Corrosion related deterioration of aging aircraft has proven to cause reduced flight availability, service lifetime, costly repairs, and if undetected, can result in potentially unsafe operating conditions. The purpose of this research is to develop, fabricate and test optical fiber-based chemical sensors for monitoring corrosion from early stages through the entire corrosion event. Although there are several preventative methods under development to address the problem of corrosion degradation, new techniques are still needed that are cost-effective and reliable to ensure an acceptable health status determination of aging aircraft and civil infrastructure. In using optical fiber-based sensors to detect corrosion precursors such as moisture, pH, nitrates, sulfates, chlorates and corrosion related metal-ion by-products the severity of the corrosive environment can be determined allowing predictive health evaluation of the infrastructure. The long period grating (LPG) element is highly sensitive to refractive index changes and with appropriate design geometry a variety of target molecules can be detected. Optical fiber long period gratings are designed to act as spectral loss elements that couple a discrete wavelength out of the optical fiber as a function of the surrounding refractive index. By applying special coating that change refractive index with absorption of target molecules to the LPG surface, it becomes a transducer for chemical measurement. Presented in this research is the incorporation of pH-sensitive hydrogels with long period gratings for the development of a fiber optic-based pH sensor. Optical fiber-based pH sensors offer numerous advantages in wastewater monitoring, blood diagnostics, bioremediation, as well as chemical and food processing. Specifically this research focuses on pH sensors that can be multiplexed with other chemical sensors for a complete chemical analysis of the corrosive environment. / Master of Science

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For the purpose of developing a new highly-sensitive and reliable fiber optical acoustic sensor capable of real-time on-line detection of acoustic emissions in power transformers, this dissertation presents the comprehensive research work on the theory, modeling, design, instrumentation, noise analysis, and performance evaluation of a diaphragm-based optical fiber acoustic (DOFIA) sensor system. The optical interference theory and the diaphragm dynamic vibration analysis form the two foundation stones of the diaphragm-based optical fiber interferomtric acoustic (DOFIA) sensor. Combining these two principles, the pressure sensitivity and frequency response of the acoustic sensor system is analyzed quantitatively, which provides guidance for the practical design for the DOFIA sensor probe and system. To meet all the technical requirements for partial discharge detection, semiconductor process technologies are applied, for the first time to our knowledge, in fabricating the micro-caved diaphragm (MCD) used for the DOFIA sensor probe. The novel controlled thermal bonding method was proposed, designed, and developed to fabricate high performance DOFIA sensor probes with excellent mechanical strength and temperature stability. In addition, the signal processing unit is designed and implemented with high gain, wide band response, and ultra low noise. A systematic noise analysis is also presented to provide a better understanding of the performance limitations of the DOFIA sensor system. Based on the system noise analysis results, optimization measures are proposed to improve the system performance. Extensive experiments, including the field testing in a power transformer, have also been conducted to systematically evaluate the performance of the instrumentation systems and the sensor probes. These results clearly demonstrated the feasibility of the developed DOFIA sensor for the detection of partial discharges inside electrical power transformers, with unique advantages of non-electrically conducting, high sensitivity, high frequency response, and immunity to the electro-magnetic interference (EMI). / Ph. D.

Sapphire fiber based temperature sensors are exceptional in their ability to operate at temperatures above 1000C and as high as 1800C. Sapphire fiber technology is emerging and the fiber is available commercially. Sapphire fiber has a high loss, is highly multi-mode and does not have a solid cladding, but it is nonetheless very useful in high temperature applications. Of the available interferometer configurations, Fabry-Perot interferometers are distinguished in their high accuracy and great isolation from sources of error. In this thesis, improvements are reported to an existing design to enhance its reliability and to reduce possible modes of failure. The existing high temperature sensor design has shown a lot of potential in the past by continuously measuring the temperature in a coal gasifier for 7 months, but its true potential has not yet been realized. The goal of this work and the work of many others is to extend the working life and reliability of high-temperature optical sapphire temperature sensors in harsh environments by exploring a solid cladding for sapphire fiber, improved fringe visibility sapphire wafers and a new sensor design. This project is supported by the National Energy and Technology Laboratory of the Department of Energy. / Master of Science

Ces dernières années, des avancées considérables ont été obtenues dans le domaine des capteurs à fibres optiques, principalement grâce à l’élan des applications industrielles, de plus en plus diverses et nombreuses (monitoring de structures, surveillance, environnement, applications médicales, ….). Cette thèse concerne le domaine des antennes acoustiques SONAR en technologie « tout-optique » Dans ce travail, nous nous sommes intéressés à l’étude d’un capteur de contrainte longitudinale à fibre optique. La modulation de phase optique induite par la contrainte est démodulée par un interféromètre adaptatif basé sur le principe de l’holographie dynamique. Cet interféromètre permet, par essence, (i) le filtrage des perturbations basse fréquence de l’environnement, (ii) un fonctionnement en régime linéaire (iii) la démodulation d’un front d’onde complexe, type speckle issu d’une fibre optique multimode. L’holographie dynamique repose sur l’interaction entre deux ondes optiques dans un milieu non-linéaire. Pour notre application, le milieu non-linéaire retenu est un modulateur spatial de lumière adressé optiquement (OASLM) à 1,55 μm. Nous présentons tout d’abord nos travaux de conception, réalisation et caractérisation de l’interféromètre adaptatif. Nous démontrons ensuite un capteur de contrainte à fibre optique basé sur cet interféromètre. Nous étudions également l’augmentation de sensibilité du capteur par l’utilisation d’une fibre optique multimode. Nous discutons finalement nos résultats et le potentiel de la technologie étudiée au regard de l’application visée. / Fiber optic sensors are a key technology for future developments with a large field of applications ranging from structure health monitoring to medical applications. Due to its high compactness, its electromagnetic immunity and the low transmission losses in the telecom window, optical fibers are very promising for underwater acoustic waves detection. We present a method relying on adaptive holographic interferometry based on two beam coupling in an optically addressed spatial light modulator (OASLM). This method allows filtering the slow phase perturbations coming from the environment directly on the sensing optical fiber. In this work, we will first introduce the OASLM operating at 1,55 μm that we have manufactured and the realization of an adaptive holographic interferometer based on this component. Moreover, we will show that it is possible to associate this demodulation method with a multimode optical fiber to reach a better sensitivity. Finally, we will focus on sensors architectures to evaluate the benefit of this technology compared to conventional techniques.

This dissertation presents the creation of slab coupled optical sensors (SCOS) for electric field sensing applications. SCOS devices utilize the benefits of an optical fiber system for high bandwidth and low electromagnetic interference. These sensors are fabricated by means of mode coupling between a small section of D-shaped optical fiber (D-fiber) with a multi-mode electro-optic slab waveguide. Electric field detection is accomplished by monitoring the behavior of the resonances, seen as transmission dips in the D-fiber transmission, as they shift with electric fields. The novelties of SCOS devices include their small compact nature, potential for sensor multiplexing and a dielectric structure allowing low electromagnetic interference. The SCOS developed in this work been used to measure fields as low as 30 V/m with 1 kHz resolution bandwidth and a high degree of linearity. Due to their compact size they are capable of placement within devices to measure interior electric fields immeasurable by other sensors that are either too large for internal placement or disruptive of the internal fields due to metallic structure. Wavelength multiplexing allows multiple sensors to be placed on a single fiber for mapping electric fields at multiple instances. As an extension, SCOS multiplexing allows the potential for 3-d field sensing by use of multiple electro-optic crystals having orthogonal orientations of the electro-optic axis. This work performs a thorough analysis of SCOS design in order to optimize sensor efficiency for its various applications. Furthermore, the straightforward fabrication process for these sensors is outlined for the development of future uses of these sensors.

Random hole optical fibers (RHOF) offer advantages over other types of microstructured optical fibers (MOFs). They are inexpensive and easy-to-make when compared to the high cost of ordered hole MOFs. They also have unique characteristics since they contain open and closed holes. The open holes contain ambient air under normal conditions and the closed holes contain residual gases from the fabrication process at certain pressure. The objective of this research work was to investigate the radiation resistance of Random Hole Optical Fibers (RHOF) for possible use as both sensing element and data transmission medium in nuclear reactor instrumentation and control applications. This work is motivated by the demand for efficient, cost effective, and safe operation of nuclear power plants, which accounts for more than 14% of the world's electricity production. This work has studied the effect of gamma irradiation on RHOF fibers by comparing their performance to that of standard solid telecommunication fibers and commercially available specialty solid fiber designed to be radiations hardened fiber. The fibers were evaluated at different absorbed dose levels: 12 mGy(Si), 350 mGy(Si), and 7200 Gy(Si) by measuring their radiation induced absorption (RIA) on-line. In the low dose test, the maximum RIA measured in untreated RHOF was approximately 8 dB while the RIA in the untreated MMF fibers reached a maximum at about 28 dB. In the high dose test, the maximum RIA measured in untreated RHOF was 36 dB while RIA in the methanol washed RHOF was only 9 dB. RHOF also demonstrated superior radiation damage recovery time over all of the other fibers tested. Based on the experimental evaluations, it was deduced that RHOFs used in this work are resistant to gamma radiation. and recover from radiation damage at a faster rate compared to other fibers tested. The radiation induced absorption (RIA) at the 1550 nm window in the RHOF fibers could be attributed to the OH absorption band tail. However, the existence of other mechanisms responsible for RIA is also postulated. Some of these mechanisms include bulk and surface defects which are related to the fabrication process and the influence of the gases confined within the RHOF microstructure. Gamma radiation resistance of RHOFs can be attributed to the lack of dopants and also possibly the inherent OH and nitrogen content. The behavior of thermally annealed RHOF and their fast recovery is in favor of this hypothesis. / Master of Science

La détection de l'hydrogène est une priorité environnementale. De nombreux capteurs à hydrogène ont déjà été développés, mais aucun d’eux ne répond aux exigences de l'industrie. Les capteurs à fibres optiques, électriquement isolés, sont d’excellents candidats pour fonctionner dans des environnements explosifs. Notre objectif est de développer un capteur à fibres optiques intrinsèque par Résonance de Plasmon de Surface pour la détection d’hydrogène. Dans cette thèse, nous étudions deux designs de capteurs à hydrogène. Le premier, basé sur la modulation d'amplitude, se compose d'une couche mince de Pd déposé sur le cœur de la fibre multimode, après avoir enlevé la gaine optique. Dans le second, basé sur la modulation de longueur d'onde, nous remplaçons la couche de Pd par un empilement de couches (Au / SiO 2 / Pd). Dans cette thèse, nous démontrons que les capteurs plasmoniques peuvent être une solution pour développer des capteurs à hydrogène fiables et rapides. Enfin, nous étudions des alliages de Mg comme matériaux sensibles à l’hydrogène afin d’optimiser la plage de détection des capteurs à hydrogène. / Hydrogen detection is an environmental priority. Numerous hydrogen sensors have been developed, but none of them meet the industry requirements. Optical fiber sensors, electrically isolated, are excellent candidates for operating in explosive environments. Our goal is to develop an intrinsic optical fiber sensor based on Surface Plasmon Resonance. In this thesis, we study two optical fiber hydrogen sensors. The first sensor, based on amplitude modulation, consists of a thin Pd layer deposited on the multimode fiber core, after removing the optical cladding. The second design, based on wavelength modulation, consists of replacing the single Pd layer by a Au/ SiO2/ Pd multilayer stack. We demonstrate in this thesis that plasmonic sensors may be a solution to develop fast and reliable fiber hydrogen sensors. Finally, we study Mg alloys as hydrogen sensitive material in order to improve the detection range of hydrogen sensors.

This thesis discusses the application of Slab Coupled Optical Fiber Sensors (SCOS) in a railgun. The specific goal of these sensors is to create an electric field profile at a specific point in the gun as the armature passes. The thesis explores the theory that powers the railgun as well as the principles of the SCOS sensors. It also elaborates on the various noise sources found throughout the detection system and concludes with a summary of the various field tests that were performed throughout this project. There are many benefits to using a railgun over traditional weapons in the field. These benefits not only include both safety and cost, but also greater overall defense capabilities. Unfortunately, the velocity skin effect (VSE) causes the current railgun designs to have limited life span through wear on the rails. In order to develop superior railguns and railgun armatures, the accurate detection of the VSE through measuring the electric field is of great interest. We used a SCOS, a small directionally precise dielectric sensor, as a small sensing area is required to be able to measure the electric fields inside of the rail gun. The actual usage of the SCOS within the railgun produced an additional set of problems that are not commonly encountered in the lab. The chief amongst these was noise from strain, RF pickup, and phase noise. This thesis also reports various methods used to reduce each of these noise sources.

[pt] Redes de Bragg em fibras ópticas (RBF) são formadas por modulações periódicas introduzidas no índice de refração do núcleo de fibras ópticas. Estes componentes comportam-se como filtros espectrais de banda passante, ou seja, quando iluminados por um sinal óptico de banda larga, refletem apenas uma fina fatia espectral de luz, cujo centro, o comprimento de onda de Bragg, é proporcional ao período espacial da modulação no índice de refração. As RBF têm encontrado aplicações importantes no sensoriamento das mais diversas grandezas, sendo hoje utilizadas em sistemas de monitoramento para vários segmentos industriais, tais como os setores de petróleo e gás, construção civil e aeroespacial, que, estima-se, respondem em conjunto por cerca de 70% destas aplicações. Em diversas situações o sensoriamento com RBF baseia-se em medidas indiretas da grandeza de interesse, sendo empregados mecanismos de transdução que transformam variações do mensurando em deformações na fibra óptica. Nestes casos, um problema que deve ser tratado com atenção é o acoplamento entre temperatura e deformação, uma vez que as RBF são sensíveis a estas duas variáveis. Não raro, a alternativa é utilizar simultaneamente duas RBF para obter-se a compensação de temperatura na medida de deformação. Este trabalho apresenta um estudo sobre deformações não homogêneas em redes de Bragg e discute aplicações de duas técnicas que podem ser utilizadas como alternativas para eliminar o efeito da temperatura no sensoriamento de deformação com apenas uma RBF. A primeira delas explora a birrefringência óptica induzida na RBF por carregamentos transversais à fibra óptica. A segunda baseia-se nos efeitos sobre o espectro refletido pela rede de Bragg quando submetida a um campo de deformações longitudinais não uniformes ao longo da direção axial da fibra óptica. No trabalho são apresentados protótipos e dispositivos que exploram tais técnicas para a medida simultânea de pressão e temperatura. Esses protótipos foram projetados com auxílio de ferramentas CAD e modelados utilizando-se o método de elementos finitos em conjunto com a teoria de modos acoplados da Rede de Bragg. As previsões obtidas utilizando-se estes modelos mostraram-se bastante próximas dos resultados das implementações experimentais dos protótipos, indicando que a metodologia de modelagem desenvolvida pode ser aplicada nos projetos de transdutores baseados nas duas técnicas estudadas. / [en] Fiber Bragg gratings (FBG) are modulations in the effective refractive index of optical fibers, introduced in a small length along the fiber core. Such components operate as narrow band reflective filters, that is, when illuminated by a broad-band light source, they reflect a narrow spectral band centered at a specific wavelength, the Bragg wavelength. This wavelength is proportional to the spatial period of the refractive index modulation. Fiber Bragg gratings have find an increasing number of applications as sensors for different quantities, and today are being employed as part of permanent, real time monitoring systems in various industrial segments. The oil and gas sector, together with civil infrastructure and aeronautics and aerospace, account for almost 70% of this applications. In a number of situations, FBG sensing is based on indirect measurements of the quantity being monitored, and a transduction mechanism is employed to transform changes in the measured quantity in strain sensed by the optical fiber. Since the FBG is sensitive to strain and temperature, proper temperature compensation is always necessary. Usually, a second grating is employed to simultaneously measure temperature and strain, performing the required compensation. This thesis presents a study on effects due to non- homogeneous strains in the Bragg grating and discusses application of two different techniques, based on these effects, to allow temperature compensated strain measurement using a single FBG. The first technique explores strain induced optical birefringence when the fiber is loaded transversely. The second technique is based on changes in the spectral shape of the light signal reflected by the grating when subjected to non homogeneous axial strain fields. Prototypes of pressure and temperature transducers based on these techniques have been developed. These prototypes have been designed by employing CAD techniques and modeled using the finite element method in conjunction with the theory of coupled modes for fiber Bragg gratings. Comparisons between results provided by theoretical models and experimental realizations of the prototypes are very close, demonstrating that the developed approach can be applied to design transducers based on the discussed techniques. Results obtained with the proposed pressure and temperature sensors are also encouraging indicating that the two techniques are suitable for industrial applications.