Orientadores: Marcelo Giannini, Pascal Magne / Tese (Doutorado) - Universidade Estadual de Campinas, Faculdade de Odontologia de Piracicaba / Made available in DSpace on 2018-08-21T22:55:10Z (GMT). No. of bitstreams: 1 Carvalho_AdrianaOliveira_D.pdf: 96375930 bytes, checksum: 98085bf2a4f1941f9510f1ba4c7d0a85 (MD5) Previous issue date: 2013 / Resumo: Objetivos: Comparar a resistência à fadiga (RFAD) e à fratura (RFRA), o modo de falha e o desgaste do antagonista em contato com os diferentes designs de coroas CAD/CAM utilizadas para restaurar molares tratados endodonticamente/TE ou não, fabricadas em cerâmica feldspática/FEL, dissilicato de lítio/DL ou resina nano cerâmica/RNC e fixadas com cimento resinoso auto-adesivo. Materiais e Métodos: Para os capítulos um e dois, 90 molares foram preparados e restaurados com coroas com espessura de 1,5mm ou 0,7mm respectivamente, em FEL, DL ou RNC. Para os capítulos três e quatro, outros 90 molares tiveram a porção coronária removida (nível da junção cemento-esmalte), foram TE e restaurados utilizando três diferentes designs de núcleo de preenchimento em resina composta/NPRC (4-mm de altura, 2-mm ou sem núcleo de preenchimento/endocrown) associados a coroas em RNC ou DL respectivamente. Para o capítulo cinco, grupos dos capítulos um (RNC/1,5mm e DL/1,5mm), três (NPRC de 4-mm de altura/RNC) e quatro (NPRC de 4-mm de altura/DL) foram combinados. Todas as coroas do estudo foram confeccionadas pelo sistema CAD/CAM Cerec 3 e cimentadas com o cimento RelyX Unicem II Automix. As coroas em FEL e DL foram previamente condicionadas com ácido fluorídrico e silanizadas. As coroas em RNC, assim como os dentes preparados foram apenas jateados. Todas as restaurações foram submetidas ao teste de RFAD com um carregamento cíclico isométrico aplicado por uma esfera de resina composta. O carregamento começou com cargas de 200N (5.000x) seguidos por estágios de 400, 600, 800, 1000, 1200 e 1400N a um máximo de 30.000 ciclos cada. Os espécimes foram submetidos ao carregamento até a fratura ou por no máximo 185.000 ciclos. Os espécimes que resistiram a todos os ciclos foram novamente testados axialmente até a falha ou até uma carga máxima de 4.500N. Os espécimes foram classificados quanto ao modo de falha em: catastrófica, possivelmente reparável e reparável. Os grupos foram comparados utilizando uma análise de sobrevida para o teste de RFAD e t-test ou ANOVA para o teste de RFRA. Comparações Post hoc também foram utilizadas para comparar os diferentes grupos. Resultados: A taxa de sobrevida das coroas sobre os molares não TE foram: 80% (RNC/1,5mm), 6,6% (RNC/0,7mm), 93,3% (DL/1,5mm), 13,2% (DL/0,7mm), 6,6% (FEL/1,5mm) e 0% (FEL/0,7mm). A RFRA das coroas com 1,5mm de espessura foi: 3122N-RNC, 3237N-DL e 2500N-FEL. As coroas cimentadas sobre molares TE tiveram taxa de sobrevida e RFRA respectivamente de: 53%/2969N (RNC-4mm de altura), 100%/3181N (DL-4mm de altura), 87%/2794N (RNC-2mm de altura), 93%/3759N (DL-2mm de altura), 87%/2606N (RNC-endocrown) e 100%/3265N (DL-endocrown). No teste de RFAD houve falha catastrófica apenas para as coroas confeccionadas em RNC-4mm. Após o teste de RFRA todos os espécimes falharam catastroficamente. As coroas em RNC induziram menor desgaste aparente ao antagonista. Conclusão: Apenas as coroas FEL-0,7mm não sobreviveram além da máxima força mastigatória humana. Para os dentes não TE, as coroas em DL e RNC com espessuras de 1,5mm tiveram o melhor desempenho mecânico. Para os molares TE, uma maior carga para fratura foi requerida com o uso de coroas em DL-2mm. O tratamento endodontico não teve influência sobre a RFAD de molares restaurados com coroas CAD/CAM de DL, mas diminuiu a performance das RNC / Abstract: Objectives: To evaluate the fatigue resistance, load-to-failure, failure mode and antagonistic wear in contact with different designs of full CAD/CAM crowns made of feldspathic ceramic/FEL, lithium disilicate/LD or resin nano ceramic/RNC. These prosthetic materials were used to restore endodontic treated molars or not, using a simplified cementation process. Materials and Methods: Chapters One and Two used 90 molars, which had a standardization of full crown preparation and teeth were restored using crown made of FEL, LD and RNC with thickness of 1.5mm or 0.7mm, respectively. Chapters Three and Four used 90 molars decoronated at the level of CEJ, endodontically-treated and restored using three different Filtek Z100 adhesive core build-ups designs (4-mm-build-up; 2-mm-build-up; and no buildup/ endocrown preparation) combined to crowns made of RNC and LD, respectively. For Chapter Five, groups of Chapters One (RNC/1,5mm and LD/1,5mm), Three (4-mm-build-up/RNC) and Four (4-mm-build-up/LD) were combined. All molars were restored using the Cerec 3 CAD/CAM system and cemented with RelyX Unicem II Automix cement. FEL and LD restorations were conditioned by hydrofluoric acid etching and silanated. RNC restorations as well as all preparations were treated only with airborne-particle abrasion. All restorations were submitted to cyclic isometric loading applied through a composite resin hemi-sphere. The cyclic loading started with a load of 200N (x5000 cycles), followed by stages of 400, 600, 800, 1000, 1200, and 1400N at a maximum of 30,000 cycles each. Specimens were loaded until failure or for a maximum of 185,000 cycles. Survived specimens were axially loaded until failure or to a maximum load of 4,500N. After load tests, the specimens were analyzed for the failure mode: "catastrophic" tooth/root failure, "possibly reparable" failure and "reparable" failure. Groups were compared using the life table survival analysis (fatigue test) and the t-test, one-way or two-way ANOVA for the survived samples loaded to failure. Pairwise post hoc comparisons were used to compare the different groups. Results: The survival rates for the vital teeth were: 80% (RNC - 1.5mm), 6.6% (RNC - 0.7mm), 93.3% (LD - 1.5mm), 13.2% (LD - 0.7mm), 6.6% (FEL - 1.5mm) and 0% (FEL - 0.7mm). Post-fatigue load-to-failure for 1.5mm crowns ranged between 3122N (RNC), 3237N (LD) and 2500N (FEL). The survival rate and post-fatigue load to failure for non-vital teeth were 53% / 2969N (4mm - RNC), 100% / 3181N (4mm - DL), 87% / 2794N (2mm - RNC), 93% / 3759N (2mm - DL), 87% / 2606N (endocrown - RNC) e 100% / 3265N (endocrown - LD), respectively. There were only catastrophic failures for 4mm-build-up RNC during the fatigue test. All of specimens in the load-to-failure test exhibited non-restorable catastrophic fractures. Crowns made of RNC seemed to generate the least amount of antagonistic wear. Conclusions: FEL crowns with 0.7mm of thickness didn't survive beyond the maximum masticatory forces. RNC and LD crowns with 1.5mm thick had the best performance on vital teeth. LD crowns combined with short build-ups (2mm) were associated to highest loads to failure. Endodontic treatment did not influence the fatigue resistance of molars restored with LD CAD/CAM complete crowns but decreased the performance of RNC crowns / Doutorado / Materiais Dentarios / Doutora em Materiais Dentários

Submitted in full compliance with the requirements for the Master of Health Science Degree: Dental Technology, Durban University of Technology, Durban, South Africa, 2017. / Background Shade matching is a challenging aspect of aesthetic dentistry (Vichi et al., 2011). For a long time, aesthetically pleasing prostheses have been achieved using the porcelain-fused-to-metal crown whereby the metal is masked with an opaque layer and then consecutive layers of veneering ceramic are built up (McLean, 1979). The growing popularity of all-ceramic restorations has created a need for an understanding of its colour characteristics in preference to porcelain fused to metal restorations. The study aims to assist dental technicians in making a more informed decision when choosing an all-ceramic system in terms of colour stability. Objectives The objectives were to identify colour changes of the zirconia after each firing cycle and defining if there are any microstructural changes in the zirconia cores after subsequent firing. Methods This is a quantitative study with a sample size of eighteen which was used for each experimental group. Green state zirconia blocks from Cercon (Dentsply DeguDent, USA), Lava (3M ESPE,USA), and Zirkon Zahn (Zirkonzahn Gmbh, Bruneck, Italy) were trimmed, finished and sintered to a final thickness of 0.5mm according to the manufacturers’ instructions. Each sample group was obtained directly from the manufacturer. In each group, nine specimens were shaded and nine were unshaded. The colour of each specimen was recorded before being exposed to firing cycles. This data formed the control group. All specimens were subjected to three firings and spectrophotometer reading. After each firing, SEM analysis was done after one and three firings. There was a total of thirty six specimens x three firings; n = 108. The raw data for the statistical analysis was obtained from the spectrophotometer readings recorded after the firings (n=108). The data of the study was analyzed using the SPSS version 22.0. The data were compared among the three groups using Pearsons chi square tests, where the data of the firings were measured as a binary or nominal variable, and using t-tests where a measured normally distributed variable was compared. The general linear model (GLM) looked at combinations of the variables and their effects on the dependant variable. The Multivariate tests table indicates the actual result of the one-way MANOVA. Results The Cercon results for both the control and experimental groups reveal the same result patterns and was maintained before and after firing. Lava also revealed the same results before and after firing, however, the cores in the control group differed in colour. The Zirkon Zahn system proved to be the least stable in colour. Conclusion This study supports the hypothesis that colour differences would occur relative to the number of firings for shaded zirconia. It can be concluded that Cercon displayed the most stable results in terms of colour. The acumen gained in this study may better assist dental technicians in their selection of an all-ceramic zirconia system. / M

Thesis (M.S.)--University of Michigan, 1984.

Thesis (Doctoral)--Bayer. Ludwig-Maximilians-Universität München, 1935.

Thesis (M.S.)--University of Michigan, 2001. / Includes bibliographical references.

Thesis (M.S.)--West Virginia University, 2005. / Title from document title page. Document formatted into pages; contains viii, 57 p. : ill. (some col.). Vita. Includes abstract. Includes bibliographical references (p. 34-39).

Thesis (M.S.)--University of Michigan, 1984.

Thesis (M.S.)--University of Michigan, 1985.

Thesis (Ph. D.)--University of Southern California, 1999. / eContent provider-neutral record in process. Description based on print version record. Includes bibliographical references.

Thesis (Ph. D.)--University of Southern California, 1999. / eContent provider-neutral record in process. Description based on print version record. Includes bibliographical references.