Thesis (M.S.)--University of Michigan, 2002. / Includes bibliographical references.

Thesis (Dr.)--Universidade de Sa︢o Paulo, 1968. / Includes bibliographical references.

Orientador: Mário Fernando de Góes / Dissertação (mestrado profissional) - Universidade Estadual de Campinas, Faculdade de Odontologia de Piracicaba / Made available in DSpace on 2018-08-22T14:40:39Z (GMT). No. of bitstreams: 1 Arita_CarlaHarueMartins_M.pdf: 3875036 bytes, checksum: a7eb7c2f429f80e13807b4154f6963ae (MD5) Previous issue date: 2013 / Resumo: O objetivo do estudo foi avaliar a união de cimentos à base de metacrilato à superfície de um compósito à base de silorano, com ou sem prétratamento de superfície, em teste de microtração. No total, 84 discos de resina à base de silorano (3mmX10mm) foram confeccionados, 42 discos tiveram a superfície tratada (ST) com jatos de óxido de alumínio (50?m) e os demais (42) não tiveram a ST. Os discos foram divididos em 6 grupos e foram cimentados aos pares (n=5) conforme descrição: G1 (SAM+CD)-discos sem ST com aplicação do sistema adesivo à base de metacrilato (SAM) e cimentados com cimento resinoso dual (CD); G2 (JSAM+CD)-discos com ST com aplicação do SAM e cimentados com CD; G3 (CA)-discos sem ST cimentados com cimento resinoso autoadesivo (CA); G4 (JCA)-discos com ST cimentados com CA; G5 (SAS+CD)-discos sem ST com aplicação do sistema adesivo da resina à base de silorano (SAS), foi feita a aplicação do adesivo hidrófobo seguido da aplicação do primer, e cimentação com CD; G6 (JSAS+CD)-discos com ST com aplicação do SAS e cimentados CD. Os conjuntos (disco/cimento/disco) foram armazenados em água deionizada por 24 horas. Os conjuntos foram seccionados para a obtenção de amostras em forma de palitos de (0,7 ± 0,1mm). O teste de microtração (?TBS) foi realizado à velocidade de 0,5mm/min até a fratura. Foram calculadas as médias, desvios-padrão e análise estatística (?=0,05). Foram analisados os modos de fratura. Quatro discos, de cada grupo, foram tratados, cimentados aos pares e seccionados ao meio para análise da interface de união. As médias e desvios-padrão dos grupos foram: G1=0(0); G2=47,96(9,12); G3=50,37(8,63); G4=57,07(12,01); G5=70,74(9,18); G6=59,24(9,91). A média do G1 foi inferior e estatisticamente diferente dos demais grupos, que não apresentaram diferenças estatísticas entre eles (p>0,05). A união dos materiais à base de metacrilato à superfície da resina composta à base de silorano é influenciada pelo tratamento de superfície. Em contra partida, a união de materiais à base de metacrilato fosfatado parece não ser influenciada pelo tratamento de superfície / Abstract: The aim of this in vitro study was the investigation of microtensile bond strength of low-shrinkage silorane-based composite discs (with or without pretreatment) cemented with methacylate based-cements. In total, 84 discs of silorane-based composite (3mmX10mm) were fabricated, 42 were pretreated (PT) and 42 were not (sandblasting with oxide aluminium of 50?m) and cemented in pairs. They were divided in 6 groups (n=5) as described: G1 - no PT discs with methacrylate based adhesive applied (MA) and cemented with a methacrylate based dual cure cement (DC); G2 - PT discs with MA applied and cementes with DC; G3 - no PT discs cemented with self-adhesive cement (SA); G4 - PT discs cemented with SA; G5 - no PT discs with the adhesive of silorane based composite (ASC) applied, in this group the bond was applied first followed by the primer, and cemented with DC; G6 - PT discs with ASC cemented with DC. After 24h of deionized water storage, the sets were serially sectioned into sticks (0,7 ± 0,1mm). The microtensile bond strength test (?TBS) was performed at a crosshead speed of 0,5mm/min until failure. The means were calculated and statistically analyzed (?=0,05). Modes of falure were also determined. Four discs, for each group, were PT, cemented in pairs and cut in half to interface analysis. The means and standard deviations for all groups were: G1=0(0); G2=47,96(9,12); G3=50,37(8,63); G4=57,07(12,01); G5=70,74(9,18); G6=59,24(9,91). The mean presented by group 1 was the lowest and statistically different comparing with the others, wich did not differ statistically among each other(p>0,05). The ?TBS strength of methacylated materiais was significantly influenced by the surface pretreatment. On the other hand, the ?TBS strength of methacrylate materials with phosphate groups does not seem to be influenced by surface pretreatment / Mestrado / Materiais Dentarios / Mestra em Materiais Dentários

Indiana University-Purdue University Indianapolis (IUPUI) / A method was devised to evaluate the effect of the "frozen slab" mixing technique on the physical properties of a zinc phosphate, zinc silicophosphate, hydrophosphate and polycarboxylate cement. Those properties studied were the setting time, compressive strength, tensile strength and solubility. Standardized mixing procedures were employed using predetermined powder/liquid ratios. Setting and working times were increased for all cements when mixed on glass slabs chilled to -15 c. All cements kept on the cold slab were still unset after 32 minutes. Compressive and tensile strengths were adversely affected by the "frozen slab" technique. All cements gave parallel reductions of the two strengths on the order of 20 percent except the polycarboxylate which exhibited only a 5 percent reduction in tensile strength. The polycarboxylate exhibited the highest tensile strength while its compressive strength was one half the others tested. Solubility samples were prepared and placed in 0.001M acetic acid at pH4. Solutions were changed daily and solubility was determined by the gravimetric method. The solubility of all cement was adversely affected. The zinc silicophosphate exhibited the highest and the polycarboxylate the lowest solubility of the cements tested. It was recommended that cements be mixed above the dew point and multiple mixes be used to ensure optimum physical properties.

Thesis (M.S.)--West Virginia University, 2004. / Title from document title page. Document formatted into pages; contains x, 91 p. : ill. (some col.). Vita. Includes abstract. Includes bibliographical references (p. 66-71).

Thesis (M.S.)--West Virginia University, 2001. / Title from document title page. Document formatted into pages; contains vii, 23 p. : ill. (some col.). Vita. Includes abstract. Includes bibliographical references (p. 15-21).

Thesis (M.S.)--University of Michigan, 1981.

Thesis (M.S.)--University of Michigan, 1948.

Thesis (M.S.)--University of Michigan, 1951.

Thesis (M.S.)--University of Michigan, 1981.