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Due to the rapid expansion of applications of composite materials, investigations of their properties have greatly increased. Since theoretical and numerical methods have many limitations for anisotropic materials, experimental methods are sometimes the only way to answer the questions. It has been proved that moire interferometry is a powerful technique in the study of composite materials. The high sensitivity and resolution of a measurement technique is the key to determining the properties of a material which has a fine and complicated structure such as fiber reinforced composite laminates. In this paper, a carrier fringe method is introduced to increase the resolution of the fringe gradient in the moire technique. The ability of measurement is extended to the micromechanics region. High strain concentrations and the dramatic displacement variations can be determined by measuring the slopes of carrier fringes. Strain distributions across the plies (with the thickness of 125 μm) in graphite/epoxy composites and strain concentrations in the resin-rich zones (with the thickness of 10 μm) between neighboring plies are revealed by the carrier fringe technique. Three experiments are presented to show the effectiveness of the application of carrier fringes to resolve fringe gradients and obtain strains. The current moire technique is limited to the optical laboratory because it is extremely sensitive to the disturbance of the environment. A vibration with magnitude of 0.2 μm can completely wash out the contrast of a moire fringe pattern. The study has been done in moving moire interferometry off the optical table. Vibration insensitive moire systems are investigated to extend the moire technique to the tests of large structures and using testing machines for loading. Vibration problems are discussed and the new ideas for eliminating vibration effects are presented. Six representative schemes are analyzed and three of these systems are built to perform experiments in rough environments such as on a hydraulic testing machine. The results show the great success of these new systems. / Ph. D.

The objective of this study was to investigate the bending strength and failure characteristics of AS4/3501-6 and AS4/1806 graphite/epoxy angles sections as a function of processing induced defects and porosity. The angle sections were removed from 30-inch long angles fabricated at Lockheed Georgia Company with two quasi-isotropic stacking sequences, (± 45/90₂/ ∓ 45/0₂), and (± 45/90₂ ∓ 45/0₂)₃. Various degrees of porosity were introduced into the angles using four processing techniques: a standard lay-up, a solvent wipe during lay-up, moisture introduction between plies during lay-up, and a low pressure cure cycle. Two 2.5-inch wide angle sections, each with a 1.5-inch short leg and a 3.0-inch long leg, were bonded together along their long leg to form a T-shaped specimen. Bending of the T-specimen was introduced by pressing up on the underside of the flanges while holding the base of the specimen fixed. The experimental results have shown a significant effect of the processing induced defects on the failure load and bending stiffness for AS4/3501-6 specimens, but not for AS4/1806 specimens. An anisotropic analysis of the angle curved section was performed using Lekhnitskii's stress function approach. Stress and strain fields were studied and two failure criteria (Dual maximum stress and Tsai-Wu) were investigated in order to predict T-specimen failure load and failure mode. Reasonable correlation between prediction and experiments was found for the AS4/3501-6 (± 45/90₂/ ∓ 45/0₂)₃ T-specimens, but both failure criteria were found to be too conservative in predicting failure for the AS4/3501-6 (± 45/O₂/ ∓ 45/90₂)₃, T-specimens. The predicted failure modes were in good agreement with the experimental observations for both Iaminates. / Master of Science

Several damage modes, including fiber breakage, delamination, and transverse cracking, have been observed to contribute to the mechanical degradation of fiber-reinforced composite laminates. In this investigation, the effect of transverse cracking on laminate stiffness was studied. Four. glass-epoxy laminates ([0,90₃]_s, [90₃,0]_s, [0,90]_s, and [0,±45]_s) were evaluated. Two experimental test sequences were performed. In the first test sequence, longitudinal stiffness was measured at various stages of damage development. Damage development was monitored via edge replication. In the second test sequence, four laminate stiffnesses (E_xx, v_xy, G_xy, and D_yy) were measured in the undamaged and near-saturation damage states. Two analytical models were evaluated. A one dimensional shear lag model was used to predict longitudinal stiffness as a function of crack density for the [0,90₃]_s and 90₃,0]_s laminates. Correlation between theory and experiment was good. A modified laminate analysis was used to predict four laminate stiffnesses (E_xx, v_xy, G_xy, and D_yy). Except for the [0,±45]_s case, a laminate in which significant amounts of damage - s other than transverse cracking were observed, agreement between pre- · dieted and observed stiffness changes was good. / Master of Science

The results of an experimental investigation into the compressive behavior of T300-5208 graphite/epoxy plates measuring 12.70 cm by 25.40 cm and containing circular cutouts ranging to 3.81 cm are reported. Two thicknesses, 24 ply and 48 ply were chosen to differentiate between stability failures due to buckling and strength failures due to the presence of the cutout. The critical load of the 24 ply panels was found to be independent of hole size with bifurcation occurring in the two halfwave mode longitudinally and one halfwave laterally in the quasi-isotropic panels. For the orthotropic 24 ply panels, bifurcation began in the one halfwave shape in each direction but changed to the two halfwave shape before failure. Consistent post-buckling strength was exhibited by both laminate configurations. The 48 ply specimens displayed decreasing ultimate load with increasing hole diameter to approximately 50% of the no-hole panel ultimate for a diameter-to-width ratio of 0.30. The 48 ply orthotropic panels displayed a strength/stability threshold between cutout diameters of 0.3175 cm and 0.635 cm. Panels with cutout diameters below 0.3175 cm displayed buckling before failure and those with cutouts larger than 0.635 cm experienced material failure around the hole before panel collapse. The 48 ply quasi-isotropic panels showed no sign of such a threshold with failure due to the hole occurring for all hole sizes. / Master of Science

Enhancement of mechanical, thermal and hygrothermal properties of carbon fiber/vinyl ester (CFVE) composites through nanoparticle reinforcement has been investigated. CFVE composites are becoming more and more attractive for marine applications due to two reasons : high specific strength and modulus of carbon fiber and low vulnerability of vinyl ester resin to sea water. However, the problem with this composite system is that the fiber matrix (F/M) interface is inherently weak. This leads to poor mechanical properties and fast ingress of water at the interface further deteriorating the properties. This investigation attempts to address these deficiencies by inclusion of nanoparticles in CFVE composites. Three routes of nanoparticle reinforcement have been considered : nanoparticle coating of the carbon fiber, dispersion of nanoparticles in the vinyl ester matrix, and nanoparticle modification of both the fiber and the matrix. Flexural, short beam shear and tensile testing was conducted after exposure to dry and wet environments. Differential scanning calorimetry and dynamic mechanical analysis were conducted as well. Mechanical and thermal tests show that single inclusion of nanoparticles on the fiber or in the matrix increases carbon/vinyl ester composite properties by 11-35%. However, when both fiber and matrix were modified with nanoparticles, there was a loss of properties. / by Felicia M. Powell. / Thesis (Ph.D.)--Florida Atlantic University, 2012. / Includes bibliography. / Electronic reproduction. Boca Raton, Fla., 2012. Mode of access: World Wide Web.

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