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Obrobitelné biokeramiky připravené metodou gelového lití / Machinable bioceramics prepared by gelcasting methodKolář, Martin January 2013 (has links)
In the diploma thesis, overviews of the existing literature focused on the gelcasting method and based on the findings were prepared aqueous slurries of zirconium oxide for gelcasting method. These suspensions were examined for the influence of the content ceramics powder, type and content of dispersants and volume of initiator on viscosity of aqueous suspensions and process of polymerization. Optimum ceramic suspension had 45 vol.% of ceramic powder which was stabilized by 0,5 weight % of dispersant Dolapix CE 64. Polymerization running at room temperature was initiated by 0,175 weight % of ammonium persufate without accelerator. Microstructure of prepared ceramic blanks and sintered bodies was compared with body prepared by isostatic pressing. For the machining tests were prepared blanks in disc-shaped.
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