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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Characterization of non-metallic inclusions according to morphology and composition : A comparison of two different steels before and after turning

Gram, Tove, Vickerfält, Amanda January 2015 (has links)
Investigation of non metallic inclusions in two different steels from Sandvik was made before and after turning. After dissolving the non-metallic inclusions by electrolytic extraction the particles were analysed manually or by INCA feature. This was referred to as 3D analysis. INCA feature analysis without extraction of particles was also performed, this was referred to as 2D analysis. The aim of the report was to a make a characterization of non-metallic inclusions with respect to chemical composition, aspect ratio, size and shape. The aim was also to compare different investigation methods. Samples were prepared and investigated. It was obtained that inclusions with sulphur content was elongated and crushed during the turning process. Broken sulphides were detected in one of the steels, and broken oxysulphides in the other steel in the electrolytically extracted chips created by turning. The first steel, steel 1, mainly contained sulphide and oxysulphide inclusions, and steel 2 mainly contained oxysulphides. The aspect ratio obtained by 2D analysis of the sulphide inclusions in steel 1 before turning showed similar results to the electrolytic extracted inclusions measured by hand. The aspect ratio increased with the length of the inclusion. However the deviation of data obtained by the 2D analysis was larger than deviation from the extracted particles measured by hand. The reason for this was assumed to be that the 2D method was not able to analyse the true shape of the inclusions e.g. if inclusions were partly concealed by metal matrix. In analysis of steel 2 the average aspect ratio decreased for oxides and increased for oxysulphides after turning. The chemical composition of inclusions did not change after the turning process for neither of the steels. Copper was detected in the electrolytic extracted inclusions, however not in the 2D investigation by SEM. This is an interesting topic for future research.
2

Nitrogen Without Oxygen : The effect of ferroalloys added after vacuum treatment on cleanliness of nitrogen-alloyed tool steel

Nilsson Hultén, Leo January 2021 (has links)
Nitrogen-alloyed tool steel is made at Uddeholms AB by adding high-nitrogen ferroalloy after vacuum degassing where introduced impurities are hard to remove. In this thesis two types of high-nitrogen ferrochromium are compared, a solid version and a powder cored wire. They are examined in crossection and 16 samples from four charges are examined with Pulse Distribution Analysis as well as systematic microscopy of polished cross sections. The PDA results missed smaller spinel inclusions shown in previous research to be detrimental. The wire form shows promise but more charges need to be evaluated before a conclusion is drawn. / Kvävelegerat verktygsstål tillverkas hos Uddeholms AB genom tillsats av kväverika ferrolegeringar efter vakumavgasning, och orenheter som introduceras i detta steg är svåra att avskilja. I den har uppsatsen jämförs två typer av kväverikt ferrokrom varav en i form av stycken och en i form av tråd med pulverkärna. De undersöks i tvärsnitt och totalt 16 prov från fyra charger undersöks med PDA (pulsfördelningsanalys) och systematisk mikroskopering i tvärsnitt. Resultaten från PDA missade mindre inneslutningar av spinell vilka tidigare har visat sig problematiska. Trådformen verkar lovande men fler charger behöver undersökas för att kunna dra en definitiv slutsats.

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