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Testing and validating the improved estimation of the spectrometer-transmission function with UNIFIT 2022Hesse, Ronald, Denecke, Reinhard, Radnik, Jörg 05 January 2024 (has links)
Recent developments of X-ray photoelectron spectroscopy using excitation energies
different from the usual lab-sources Mg Kα and Al Kα, thus covering larger and different
kinetic energy ranges, require more flexible approaches for determining the transmission
function than the well-established ones using reference spectra. Therefore,
the approach using quantified peak areas (QPA) was refined allowing a more precise
estimation of the transmission function. This refinement was tested by comparing
the results obtained with the new version with former calculations. Furthermore, the
obtained transmission function was validated by comparing the results with a transmission
function using the reference spectrum of polyethylene. Additionally, an ionic
liquid was used as reference for estimating the transmission function at the energyresolved
HE-SGM beamline at BESSY II. Comparison between the measured and
stoichiometric composition shows that a transmission function was determined,
which allows a reasonable quantification.
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