Thesis (M.S.)--Youngstown State University, 1972. / Typescript. Includes bibliographical references (leaf 85).

M.Ing. (Electrical and Electronic Engineering) / Please refer to full text to view abstract

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For the induction heating process of bi-metallic tubes, the inner tube of alloy-layer is much easier to cause a lot of defects of cavities due to the fact that heating power, maximum temperature value and the time frame of temperature retention were chosen improperly. This research focuses on the effect of maximum temperature value and the time frame of temperature retention on the micro-structure and defects of cavities of the Nickel-based alloy-layer. The experiments of this study are divided into two parts. In the domain of the experiment in simulation fashion, Nickel-based alloy powders were put into the specimens of AISI 4140 steel. Radio Frequency (RF) oven were used to smelt Nickel-based alloy powders in the vacuum conditions over the maximum temperature range of 920~1180¢Jrespectively. After that, the time frame of temperature retention was conducted from 0 to 10 minutes. Then, the furnace-cooling went down to 700¢J then air-cooling down to the room temperature. Nickel-based alloy-layer, microstructure, component analysis, defects of cavities of the interface between Nickel-based alloy-layer and steels, and diffusion of interfaces were analyzed using optical microscopes (OM) and scanning electron microscopes (SEM). From the experiments, it was found that Nickel-based alloy-layer consisted of £^-Ni¡BCrB¡BCr7C3 over the maximum temperature range of 920~1050¢Jwhether temperature retention is performed or not. According to the findings of metallographic observation, the increase of coarsening and the reduction of the capacity of CrB and Cr7C3 become more obvious as maximum temperature value and the time frame of temperature retention become large. In addition, the whitening layer (diffusion zone) formed between the interface of alloy-layer and steels become much wider as maximum temperature value and the time frame of temperature retention become large. Secondly, the field experiment method was also applied in this paper. The tube rich in Nickel-based alloy powders was heating to analyze induction coil in various conditions: heating power (200~285KW), maximum temperature value (1020~1040¢J), the time frame of temperature retention (10, 30, 50sec), and the rotating speed (1000~1300rpm). The results of the experiments indicated that the surface of the alloy-layer cause defects of vermicular cavities since the volume of liquid cannot fill out the crack of cavities completely due to lower temperature when there is insufficient time; too long periods of the time frame of temperature retention lead to the tough and huge dendrites to obstacle the flowing of liquid and the solidification of shrinkage cavity. According to the observation of the microstructure, the larger the maximum temperature value and the time frame of temperature retention were, the more the dendrites formed. The formation of dendrites causes not only the uneven distribution of hardening phase of CrB and Cr7C3 of the alloy-layer but also the reduction of hardness of the alloy-layer. The dendrites are typically formed from the interface to the surface of the alloy-layer. Besides that, the alloy-layer mainly consists of £^-Ni, Ni3B, Ni3Si, CrB, and Cr7C3 via X-ray Diffraction (XRD). Among them, the main hardening phases are CrB and Cr7C3 which is the main reason that the alloy-layer has high-level hardness. As maximum temperature value and the time frame of temperature retention become large, the whitening layer (diffusion zone) was formed between the interface of alloy-layer become much wider because the faster the elements of the based materials (tube) diffused and the wider the intermetallic compound formed among the interfaces. After heated for 800 seconds over the temperature range of 750~1030¢J, iron element was diffused all over the alloy-layer. The increase of coarsening and the reduction of the capacity near interface and interface become more obvious as maximum temperature value and the time frame of temperature retention become large.

Nickel-based super alloys are widely employed in the aerospace industry due to their high- temperature strength and high corrosion resistance. Because of the special application, the superficial residual stress of the super alloy is mandatory to 100% compressive stress according to the Federal Aviation Administration (FAA) regulations. In manufacturing of nickel-based super alloy components, grinding processes are necessarily applied as the final material removal step for achieving the stringent tolerance and surface finish requirements. During the traditional grinding process of Nickel based alloy, due to the thermal effect, tensile residual stress might be generated on the surface of the alloy. It's critical to transfer the tensile residual stress to compressive one which benefits on the fatigue life of alloy. In the thesis, a novel technology is developed to generate the superficial compressive residual stress with the method of embed a subsurface heating layer inside the workpiece to regulate the distribution of temperature field very before mechanical process. The residual stress might be reduced much, even transfer to compressive stress after combining the thermal effect. The numerical model will be built in the thesis including the induction model, heat transfer model, grinding heat model. Effects of different parameters on final subsurface heating layer will be studied including the coil parameters, concentrator parameters, coolant parameters, feed rate and also electromagnetic field properties such as the skin effect, proximity effect and slot effect. The thesis creates a system combining induction heating and cooling processes to regulate the temperature distribution in subsurface area that will be used for further stress analysis.

This thesis reports an investigation into the design of converters for induction heating systems based upon resonant switch mode power converter techniques. The proposed three phase unity power factor induction heating system consists of two stages of power conversions. The important requirements for each stage of the power conversion of a typical induction heating system working from a three-phase supply are identified. A wide range of power converters which fulfil these requirements are compared and evaluated. From the evaluation, the most applicable converter topologies are selected. Each selected converter class is investigated in great detail to outline their advantages and disadvantages. The first stage consists of a push-pull buck converter connected to a unity power factor rectifier stage. This stage converts the three phase AC mains supply to a required DC value. The second stage, which converters the DC into AC is a single ended resonant inverter system. Analysis of the converters has been made and the design procedure has been formulated. The design procedure allows a strenuous design of each resonant converter for particular converter applications. The final converter design has been simulated using the circuit simulation software packages Design Architect and Accusim to verify the results of analysis. The most important design and construction achievements can be summarised as follows: I A novel push-pull buck quasi-resonant converter with a three-phase rectifier stage has been built and tested. At its maximum operating frequency of 40kHz, the prototype converter delivers an output power of 500W. The converter draws nearly sinusoidal currents from the three-phase mains supply and has an input power factor approaching unity. A secondary stage resonant converter provides AC for the induction heater coil. This AC current flowing in the induction coil creates an alternating electromagnetic field for the workpiece. An induction heating coil has been designed and built by using electrical equivalent coil design method. A novel control strategy was developed to provide output power control. Both converter and inverter stage of the system are operated in the zero-current switching condition. The use of this technique allows higher switching frequencies and provides low switching losses. The full design details are presented along with simulation and practical results. The simulation and practical performance results presented show good correlation with theoretical predictions.

M.Ing. (Electrical And Electronic Engineering) / The metals manufacturing industry is the link between the mining industry, where the ore is mined, and the manufacturing industries, where metals are utilized to create a wide range of products. Melting processes.are used in the manufacturing of metals from the ore, of which induction melting is one of the possible melting processes. In this study the improvement of induction melting of metals is investigated. A new topology for an induction melting furnace is proposed, and this topology is thoroughly investigated. The induction melting process is influenced by certain user-controlled variables as well as the electromagnetic layout of the furnace. In this study, the influence of these variables on the performance of the furnace are investigated through finite element simulations and insight is also gained into the influence of the electromagnetic layout of the system. An experimental induction melting furnace is described in this study, investigated and compared to the predictions from the simulations. Improvements from structural, thermal and measuring viewpoints are also investigated and implemented.

Doctor of Philosophy / Department of Chemistry / Viktor Chikan / Semiconducting nanoparticles have emerged in the past few decades as an interesting material with great potential in various interdisciplinary applications such as light-emitting devices, solar cells and field-effect transistors, mostly notably for their size-dependent electronic structure and properties. Manipulation of their electronic-optical characters through defects control is one of the most important approaches towards realization of these applications. This thesis focuses on understanding the role of defects, including their impact on carrier density and conductivity at both room and elevated temperature, their impact on growth kinetics of colloidal nanoparticles and new opportunities for dopant control. To achieve these goals, colloidal CdSe quantum dots are doped with gallium atoms and important changes in electronic and optical properties of the material are reported, which shows a significant impact on the growth kinetics of quantum dots, and reveals clues about the mechanism of the gallium dopant incorporation into the CdSe. It is shown that the gallium doping significantly impacts the conductivity of CdSe thin film made of the quantum dots as well as the photoluminescence and chemical reactivity of the quantum dots, in agreement with the expected n-type character. P3HT/CdSe hybrid cells are constructed with Ga-, In- and Sn-doped CdSe QDs, demonstrating high conductivity and stronger electronic coupling which leads to enhanced charge separation and transport efficiency, both essential for hybrid inorganic-organic solar cells. This work also demonstrates a novel heating method that can drastically improve size distribution control of colloidal nanoparticle synthesis. Sub-2-nm ultra-small CdSe QDs are prepared with the induction (magnetic) heating and show excellent agreement of its emission profile compared with natural sunlight. The impact of extreme high heating rate on the development of more accurate nucleation and growth theories are also discussed. Finally, this study also investigates the stabilization of charges from intrinsic defects by looking for altered blinking behaviors of CdSe nanorods (NRs) under different polar environments. TMOS-PTMOS gradient films are prepared with infusion withdrawal dip-coating technique. Although no significant differences are observed of the fluorescence statistics of these NRs, permanent bleaching induced by exciting laser light is discovered, which significantly lowers raw blinking spot count and increases the “off” time of these fluorophores.

Thesis (B.S.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science; and, (B.S.)--Massachusetts Institute of Technology, Dept. of Mechanical Engineering, 1977. / MICROFICHE COPY AVAILABLE IN ARCHIVES AND ENGINEERING. / Includes bibliographical references. / by Martin Frederick Schlecht. / B.S.

Thesis. 1976. M.S.--Massachusetts Institute of Technology. Dept. of Electrical Engineering and Computer Science. / Microfiche copy available in Archives and Engineering. / Includes bibliographical references. / M.S.