The presence of moisture in hot mix asphalt (HMA) causes loss of strength and durability of the mix, which is referred to as moisture damage. This study deals with the development of experimental methods for measuring total suction in HMA, which can be defined as the free energy state of water in HMA mixes. The total suction is related to the ability of moisture to get into the mix under unsaturated conditions; it is also related to the ability of the mix to retain moisture. Soil suction has been studied extensively. However, suction in HMA as a porous material and its relationship to moisture damage have not been studied. The development of a procedure to measure the total suction in HMA mixes is the first objective of this research. The second objective is to relate suction measurements to physical and chemical properties of the mixtures. The objectives were achieved in two phases. In the first phase, the total suction was measured in HMA specimens with different types of aggregates (limestone and granite), and with different air void distributions and aggregate gradations. The results of this phase showed that the drying test using a 60 oC temperature-controlled room is the proper setup for measuring the total suction in HMA using thermocouple psychrometers. The characteristics of suction-moisture content curves were found to be related to the air void distribution in HMA. In the second phase, total suction was measured in sand asphalt specimens. These specimens had different combinations of aggregates and binders with different bond energies and exhibited different field performance in terms of resistance to moisture damage. The suction measurements in sand asphalt specimens were used to calculate the moisture diffusion coefficient. The results revealed that water diffused into sand asphalt specimens that are known to have poor resistance to moisture damage faster than those that are known to have good resistance to moisture damage

The presence of moisture in hot mix asphalt (HMA) causes loss of strength and durability of the mix, which is referred to as moisture damage. This study deals with the development of experimental methods for measuring total suction in HMA, which can be defined as the free energy state of water in HMA mixes. The total suction is related to the ability of moisture to get into the mix under unsaturated conditions; it is also related to the ability of the mix to retain moisture. Soil suction has been studied extensively. However, suction in HMA as a porous material and its relationship to moisture damage have not been studied. The development of a procedure to measure the total suction in HMA mixes is the first objective of this research. The second objective is to relate suction measurements to physical and chemical properties of the mixtures. The objectives were achieved in two phases. In the first phase, the total suction was measured in HMA specimens with different types of aggregates (limestone and granite), and with different air void distributions and aggregate gradations. The results of this phase showed that the drying test using a 60 oC temperature-controlled room is the proper setup for measuring the total suction in HMA using thermocouple psychrometers. The characteristics of suction-moisture content curves were found to be related to the air void distribution in HMA. In the second phase, total suction was measured in sand asphalt specimens. These specimens had different combinations of aggregates and binders with different bond energies and exhibited different field performance in terms of resistance to moisture damage. The suction measurements in sand asphalt specimens were used to calculate the moisture diffusion coefficient. The results revealed that water diffused into sand asphalt specimens that are known to have poor resistance to moisture damage faster than those that are known to have good resistance to moisture damage

This thesis describes the measurement technique of fast-neutron tomography for assessing spatial distributions of steam and water in two-phase flows. This so-called void distribution is of importance both for safe operation and for efficient use of the fuel in light water reactors, which compose the majority of the world’s commercial nuclear reactors. The technique is aimed for usage at thermal-hydraulic test loops, where heated two-phase flows are being investigated under reactor-relevant conditions. By deploying portable neutron generators in transmission tomography, the technique becomes applicable to stationary objects, such as thermal-hydraulic test loops. Fast neutrons have the advantage of high transmission through metallic structures while simultaneously being relatively sensitive to the water/void content. However, there are also challenges, such as the relatively low yield of commercially available fast-neutron generators, the tendency of fast neutrons to scatter in the interactions with materials and the relatively low efficiency encountered in fast-neutron detection. The thesis describes the design of a prototype instrument, FANTOM, which has been assembled and demonstrated. The main design parameters have been optimized to achieve maximal signal count rate in the detector elements, while simultaneously reaching an image unsharpness of ≤0.5 mm. Radiographic projections recorded with the assembled instrument are presented, and the performance parameters of FANTOM are deduced. Furthermore, tomographic reconstruction methods for axially symmetric objects, which is relevant for some test loops, have been developed and demonstrated on measured data from three test objects. The attenuation distribution was reconstructed with a radial resolution of 0.5 mm and an RMS error of 0.02 cm-1, based on data recorded using an effective measurement time of 3.5 hours per object. For a thermal-hydraulic test loop, this can give a useful indication of the flow mode, but further development is desired to improve the precision of the measurements. Instrument upgrades are foreseen by introducing a more powerful neutron generator and by adding detector elements, speeding up the data collection by several orders of magnitude and allowing for higher precision data. The requirements and performance of an instrument for assessment of arbitrary non-symmetric test loops is discussed, based on simulations.

Field compaction of asphalt mixtures is an important process that influences performance of asphalt pavements; however there is very little effort devoted to evaluate the influence of compaction on the uniformity and properties of asphalt mixtures. The first part of this study evaluated relationships between different field compaction patterns and the uniformity of air void distribution in asphalt pavements. A number of projects with different asphalt mixture types were compacted, and cores were taken at different locations from these projects. The X-ray Computed Tomography (X-ray CT) system was used to capture the air void distributions in these cores. The analysis results have revealed that the uniformity of air void distribution is highly related to the compaction pattern and the sequence of different compaction equipment. More importantly, the efficiency of compaction (reducing air voids) at a point was found to be a function of the location of this point with respect to the compaction roller width. The results in this study supported the development of the "Compaction Index (CI)," which quantifies the degree of field compaction. The CI is a function of the number of passes at a point and the position of the point with respect to the compaction roller width. This index was found to correlate reasonably well with percent air voids in the pavement. The CI calculated from field compaction was also related to the slope of the compaction curve obtained from the Superpave gyratory compactor. This relationship offers the opportunity to predict field compactability based on laboratory measurements. The compaction of longitudinal joints was investigated, and recommendations were put forward to improve joint compaction. The air void distributions in gyratory specimens were related to the mixture mechanical properties measured using the Overlay and Hamburg tests. The second part of this study focused on studying the relationship between air void distribution and moisture diffusion. A laboratory test protocol was developed to measure the diffusion coefficient of asphalt mixtures. This important property has not measured before. The results revealed that the air void phase within the asphalt mixtures controls the rate of moisture diffusion. The measured diffusion coefficients correlated well with the percent and size of connected air voids. The measured diffusion coefficient is a necessary parameter in modeling moisture transport and predicting moisture damage in asphalt mixtures. The last part of this study investigated the resistance of asphalt mixtures with different percent air voids to moisture damage by using experimental methods and a fracture mechanics approach that accounts for fundamental material properties.