A high-temperature, high-pressure autoclave has been
adapted for use with a high-field nuclear magnetic
resonance spectrometer. The autoclave has an internal
pressure range of atmospheric pressure to 1.5 kbar and a
temperature range of 273 K to 1900 K. The autoclave is
usable in a high field (8 T) magnet with a room temperature,
76.4 mm bore. The autoclave was tested using
assorted nuclear species with resonant frequencies ranging
from 57 to 70 MHz at pressures ranging from atmospheric
pressure to 1220 bar and temperatures ranging from 273 K to
448 K. Previously, the autoclave was used in conjunction
with an iron magnet at temperatures to 1900 K and pressures
to 1.5 kbar. / Graduation date: 1997
| Identifer | oai:union.ndltd.org:ORGSU/oai:ir.library.oregonstate.edu:1957/34276 |
| Date | 13 December 1996 |
| Creators | Mullen, Corina P. |
| Contributors | Warren, William W. Jr |
| Source Sets | Oregon State University |
| Language | en_US |
| Detected Language | English |
| Type | Thesis/Dissertation |
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