The thesis was focused on preparation of bioceramic composite materials containing Ca-phosphates and zirconia fibers using electrophoretic deposition. A series of experiments were aimed at determining the appropriate composition of the suspensions. High-energy milling was used for preparing deposits with good physical and mechanical properties using EPD. The influence of milling time, the amount of monochloroacetic acid in isopropanol slurry indifferent electrolyte LiCl and ZrO2 were evaluated on the course deposition and the resulting properties of the deposits. Influence of sintering temperature, the milling time and the fiber content of ZrO2 on the chemical and structural composition was determined by X-ray analysis, measurement of density and structural analysis using a scanning electron microscope. Mechanical and bioactive properties of sintered deposits were determined depending on the milling time and content of ZrO2 fibers.
| Identifer | oai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:231718 |
| Date | January 2014 |
| Creators | Sláma, Martin |
| Contributors | Drdlík, Daniel, Cihlář, Jaroslav |
| Publisher | Vysoké učení technické v Brně. Fakulta strojního inženýrství |
| Source Sets | Czech ETDs |
| Language | Czech |
| Detected Language | English |
| Type | info:eu-repo/semantics/masterThesis |
| Rights | info:eu-repo/semantics/restrictedAccess |
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