Master of Science / Department of Chemical Engineering / J.R. Schlup / The curing reaction for the amine epoxy resin system of phenyl glycidyl ether (PGE) with metaphenylene diamine (mPDA) was investigated using two-dimensional correlation spectroscopy in the near-infared region (2DNIR). Synchronous and asynchronous correlation maps were generated using 2Dshige© software. The characteristic NIR band assignments were made, including the identification of new peaks for the O-H combination band in the 4825-4750 cm[superscript]-1 region and the CH stretching vibration overtone at 6018 cm[superscript]-1. Finally, the data suggests the reaction proceeds as follows: the appearance of the OH groups and C-H backbone vibrations occurs before the primary amine reactions and epoxide rings disappear.
| Identifer | oai:union.ndltd.org:KSU/oai:krex.k-state.edu:2097/13838 |
| Date | January 1900 |
| Creators | Hollock, Michael R. |
| Publisher | Kansas State University |
| Source Sets | K-State Research Exchange |
| Detected Language | English |
| Type | Report |
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