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Optimalizace chemické analýzy vybraných složek materiálů historických uměleckých děl / Optimization of chemical analysis of selected components in material of historical artworks

The simplification of the historical pieces of work samples' treatment is described in the dissertation. The recent methods have been inappropriate therefore, modification of the treatment was necessary. The dammar and copal resin, important restoration materials, were used in the experiment. HPLC-MS, HPLC-ELSD, GC-FID, GC-MS and pyrolysis GC- MS were applied. The concentration of fatty acids in the historical sculpture was determined by GC-MS, and it was compared to the content of fatty acids inside an egg. For identification of monosaccharide in the gum, GC-MS (hexamethyldisilazan, trimethylchlorsilan, and pyridine) is the suitable method. GC-MS determines the same composition of dammar resin as stated in the cited sources. The simple process for the samples' treatment was designed.

Identiferoai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:338227
Date January 2014
CreatorsPekař, Martin
ContributorsČabala, Radomír, Hudeček, Jiří
Source SetsCzech ETDs
LanguageCzech
Detected LanguageEnglish
Typeinfo:eu-repo/semantics/masterThesis
Rightsinfo:eu-repo/semantics/restrictedAccess

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