High-pressure homogenization using a new flat valve homogenizer in combination with enzymatic digestion with a crude protease was investigated as a means of releasing Se compounds from zoological and botanical matrices prior to slurry introduction GF-AAS. Timed trials with four zoological certified reference materials (CRMs), three botanical reference materials (RMs), and a food crop indicated that Se release was quantitative after homogenization or became quantitative within 1 h of digestion at 60°C. / The same technique was employed on five animal feed samples. / A new model of homogenizer equipped with ceramic homogenizing valve was evaluated in terms of analyte metal contamination levels within the final sample dispersion. / Five animal feed samples and four wood pulp samples, were investigated for their content of Cu, Fe and Mn using high-pressure homogenization as the sample preparation technique prior to GF-AAS. Dispersions of dried animal feeds were sub-sampled reliably after 7 days of storage at 4°C. Trials on pulp samples indicated that pulps could be sub-sampled reliably after 1 day of storage. (Abstract shortened by UMI.)
| Identifer | oai:union.ndltd.org:LACETR/oai:collectionscanada.gc.ca:QMM.33386 |
| Date | January 2000 |
| Creators | Chen, Xi, 1970- |
| Contributors | Marshall, W. D. (advisor) |
| Publisher | McGill University |
| Source Sets | Library and Archives Canada ETDs Repository / Centre d'archives des thèses électroniques de Bibliothèque et Archives Canada |
| Language | English |
| Detected Language | English |
| Type | Electronic Thesis or Dissertation |
| Format | application/pdf |
| Coverage | Master of Science (Department of Food Science and Agricultural Chemistry.) |
| Rights | All items in eScholarship@McGill are protected by copyright with all rights reserved unless otherwise indicated. |
| Relation | alephsysno: 001783337, proquestno: MQ70696, Theses scanned by UMI/ProQuest. |
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