A detailed metallurgical analysis was conducted to correlate microstructure to axial strain-controlled high cycle fatigue of Ti-6Al-4V forgings made from cold isostatic pressed and sintered preforms of blended element powder metallurgy (BEPM) incorporating hydrogenated titanium. Analysis included fractographic examination by SEM, microstructure examination by optical microscopy, texture examination via EBSD, chemical analysis and fatigue strain mapping via digital image correlation (DIC). From a literature review and observations of findings, factors that were of primary concern were: maximum pore diameter, primary α volume fraction, primary α width, primary α particle count, oxygen equivalency (OE) and texture of the α phase.
The primary α volume fraction was found to have the single most influential effect on fatigue, whereby decreasing volume fraction increased fatigue life. Using statistical analysis, multivariable regression analyses were performed to evaluate combinations of predictors on fatigue life. The resulting outcome of volume fraction and maximum pore diameter, having a 3.3 to 1 weighting, was the most significant at predicting the fatigue response. Improving fatigue life of forged Ti-6Al-4V made from BEPM should thus be primarily focused on microstructure refinement. It is suggested future experimentation also consider the effects of the number of primary α particles and OE when modeling fatigue strength. / Thesis / Master of Applied Science (MASc) / The mechanical properties of a metal are dictated primarily by the metal’s microstructure. The microstructure of a metal made from metal powder that has been pressed and heated to bind the powder together generally contains residual porosity. This generally leads to a reduction in metal fatigue resistance versus a metal that is pore-free.
In studying metal fatigue of a titanium alloy made from metal powder, the resistance to metal fatigue varied considerably and did not achieve the same resistance of pore-free material, despite the titanium alloy in question being nearly pore-free. This titanium alloy was studied to determine what the cause of the poor metal fatigue resistance was. Through a methodical testing program, it was determined that volume fraction of a particular crystalline phase in the microstructure was more damaging than the pores themselves.
| Identifer | oai:union.ndltd.org:mcmaster.ca/oai:macsphere.mcmaster.ca:11375/19327 |
| Date | January 2016 |
| Creators | Haynes, Noel |
| Contributors | Zurob, Hatem, Materials Science and Engineering |
| Source Sets | McMaster University |
| Language | English |
| Detected Language | English |
| Type | Thesis |
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