Hydrothermal synthesis is one of the most widely used methods for preparing nanoparticles of titanium dioxide. The process carried out at elevated temperatures and pressure, which facilitates the transformation of amorphous to crystalline titanium dioxide. Change of reaction conditions of the process (reactants concentration, temperature, time, pH, etc.) leads to change in morphology, microstructure and crystallinity of titanium dioxide nanoparticles. In this work the method of titanium dioxide preparation is briefly described. The titanium dioxide was prepared from a precursor titanium oxochloride and potassium hydroxide as the precipitating agent. Thus prepared titanium dioxide was immobilized on a glass substrate by material printing. This is a modern, highly precise and contactless method for preparing thin films. The photocatalytic activity of printed thin films of titanium dioxide was investigated by degradation of 2,6-dichlorindophenol at different irradiance. It was found that the sample prepared by hydrothermal treatment at 160 °C shows very similar photocatalytic activity to Degussa P25.
| Identifer | oai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:216821 |
| Date | January 2012 |
| Creators | Lepičová, Martina |
| Contributors | Jančovičová, Viera, Veselý, Michal |
| Publisher | Vysoké učení technické v Brně. Fakulta chemická |
| Source Sets | Czech ETDs |
| Language | Czech |
| Detected Language | English |
| Type | info:eu-repo/semantics/masterThesis |
| Rights | info:eu-repo/semantics/restrictedAccess |
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