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Methods Development for Ion Chromatography

Ion chromatography (IC) as developed by Small et. al. in 1975 has become an efficient and reliable analytical technique for simultaneous analysis of multiple ions in solution. The principle requirement prior to use the IC for an analysis is sample preparation; these include sample decomposition, solvent extraction, and trapping in case the target element is in the gas phase, etc. Solvent extractions for fluoride, chloride, sodium, ammonium, and potassium ions which are soluble in soils are described. Sample decompositions include silicate rocks using hydrofluoric acid for the determination of phosphorus; organic pesticides using lithium fusion technique for the determination of halide and cyanide ions are also described. After these sample preparation techniques, the aqueous solutions obtained were analyzed on the ion chromatograph for the analyses of the anions and cations mentioned above. Recovery and reproducibility of each technique is in general quite good and the comparison between the results obtained from the IC method and other instrumentation are given.

Identiferoai:union.ndltd.org:unt.edu/info:ark/67531/metadc330927
Date05 1900
CreatorsSupachai Maketon
ContributorsTarter, James G., Daugherty, Kenneth E., Harper, Keith J., Schwartz, Martin, Thomas, Ruthanne D.
PublisherNorth Texas State University
Source SetsUniversity of North Texas
LanguageEnglish
Detected LanguageEnglish
TypeThesis or Dissertation
Formativ, 81 leaves: ill., Text
RightsPublic, Supachai Maketon, Copyright, Copyright is held by the author, unless otherwise noted. All rights reserved.

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