Identification of an acetyl disulfide derivative in the synthesis of thiosialosides

Description

No / The first report of the formation of an acetyl disulfide sialoside during the synthesis of thioglycosides is described. This compound is a by-product in the synthesis of the 2-thioacetyl sialoside commonly used in thioglycoside preparation. Our investigations into the identification of this novel disulfide are described.

Links & Downloads

1. Ribero Morais, G., Oliveira, I.P.F., Humphrey, A.J. and Falconer, R.A. (2009). The first report of the formation of an acetyl disulfide sialoside during the synthesis of thioglycosides is described. This compound is a by-product in the synthesis of the 2-thioacetyl sialoside commonly used in thioglycoside preparation. Our investigations into the identification of this novel disulfide are described.. Carbohydrate Research. Vol. 345, No. 1, pp. 160-162.
2. http://hdl.handle.net/10454/4614
3. https://doi.org/10.1016/j.carres.2009.10.017

Tags

Disulfide

Thiosialosides

Chromatography

Magnetic Resonance Spectroscopy

Additional Fields

Identifer	oai:union.ndltd.org:BRADFORD/oai:bradscholars.brad.ac.uk:10454/4614
Date	January 2009
Creators	Ribeiro Morais, Goreti, Oliveira, Inês P.F., Humphrey, Andrew J., Falconer, Robert A.
Source Sets	Bradford Scholars
Language	English
Detected Language	English
Type	Article, No full-text in the repository