Title: Study of ultrafine-grained materials prepared with different methods of severe plastic deformation Author: RNDr. Tomáš Krajňák Department: Department of Physics of Materials, Faculty of Mathematics and Physics, Charles University in Prague Supervisor: Doc. RNDr. Kristián Máthis, PhD., Department of Physics of Materials, Faculty of Mathematics and Physics, Charles University in Prague Abstract: Interstitial free steel with ultrafine-grained (UFG) structure was prepared by high-pressure torsion (HPT). The development of the microstructure as a function of the number of HPT turns was studied at the centre, half-radius and periphery of the HPT-processed disks by X-ray line profile analysis (XLPA), positron annihilation spectroscopy (PAS) and electron microscopy. The dislocation densities and the dislocation cell sizes determined by XLPA were found to be in good agreement with those obtained by PAS. The evolution of the dislocation density, the dislocation cell and grain sizes, the vacancy cluster size, as well as the high-angle grain boundary (HAGB) fraction was determined as a function of the equivalent strain. It was found that first the dislocation density saturated, then the dislocation cell size reached its minimum value and finally the grain size got saturated. For very high strains after the...
Identifer | oai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:350058 |
Date | January 2015 |
Creators | Krajňák, Tomáš |
Contributors | Mathis, Kristián, Hadzima, Branislav, Kalvoda, Ladislav |
Source Sets | Czech ETDs |
Language | Czech |
Detected Language | English |
Type | info:eu-repo/semantics/doctoralThesis |
Rights | info:eu-repo/semantics/restrictedAccess |
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