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Spectrophotometric determination of aluminium oxide, calcium oxide and iron (III) oxide in Portland cement.

Shu King-hung. / Thesis (M.Phil.)--Chinese University of Hong Kong, 1993. / Includes bibliographical references (leaves 80-81). / ABSTRACT --- p.1 / Chapter CHAPTER I. --- INTRODUCTION --- p.3 / REFERENCES --- p.6 / Chapter CHAPTER II. --- BRIEF REVIEW OF THE ANALYTICAL METHODS USED / Chapter 1. --- Spectrophotometry --- p.8 / Chapter 2. --- Derivative spectrophotometry --- p.9 / Chapter 3. --- Atomic absorption spectrometry --- p.12 / Chapter 4. --- X - Ray fluorescence --- p.12 / REFERENCES --- p.14 / Chapter CHAPTER III. --- SIMULTANEOUS DETERMINATION OF ALUMINIUM OXIDE AND IRON (III) OXIDE / Chapter 1. --- Introduction / Review of the reported methods --- p.15 / Determination of aluminium and iron with / 8-hydroxyquinoline --- p.18 / Chapter 2. --- Experimental --- p.21 / Chapter 3. --- Results and discussion / Determination of iron --- p.28 / Determination of aluminium --- p.38 / Chapter 4. --- Conclusion --- p.52 / REFERENCES --- p.53 / Chapter CHAPTER IV. --- RAPID DETERMINATION OF CALCIUM OXIDE / Chapter 1. --- Introduction --- p.56 / Chapter 2. --- Experimental --- p.62 / Chapter 3. --- Results and discussion --- p.66 / Chapter 4. --- Conclusion --- p.79 / REFERENCES --- p.80 / FIGURES / Chapter II-1 --- Attenuation of a beam of radiation by an absorbing solution --- p.8 / Chapter II-2 --- Gaussian curve and its first to fourth derivatives --- p.11 / Chapter III-l --- Effect of pH on the extraction of metals with8- hydroxyquinoline --- p.19 / Chapter III-2 --- "Normal absorbance spectra of the metal - oxinates: A1 (5ppm), Fe (5ppm)" --- p.20 / Chapter III-3 --- Effect of pH on the determination of iron (5ppm) --- p.29 / Chapter III-4 --- Calibration curve for the determination of iron (III) by spectrophotometry at 580 nm --- p.33 / Chapter III-5 --- "The first derivative spectra of metal-oxinates A1: 5ppm, Fe : 5ppm" --- p.39 / Chapter III-6 --- "The second derivative spectra of metal-oxinates, A1: 5ppm, Fe : 5ppm" --- p.39 / Chapter III-7 --- "Normal absorption spectra of the metal-oxinates : A1(5 ppm), Ti (5 ppm)" --- p.41 / Chapter III-8 --- Effect of pH on the determination of aluminium --- p.43 / Chapter III-9 --- Calibration curve for the determination of aluminium by second derivative spectrophotometry at 390 nm --- p.47 / Chapter IV-1 --- "Effect of pH on the development of colour of Ca- GBHA complex. Ca : 1.2 ppm, wavelength : 530 nm" --- p.68

Identiferoai:union.ndltd.org:cuhk.edu.hk/oai:cuhk-dr:cuhk_319196
Date January 1993
ContributorsShu, King-hung., Chinese University of Hong Kong Graduate School. Division of Chemistry.
PublisherChinese University of Hong Kong
Source SetsThe Chinese University of Hong Kong
LanguageEnglish
Detected LanguageEnglish
TypeText, bibliography
Formatprint, v, 81 leaves : ill. ; 30 cm.
RightsUse of this resource is governed by the terms and conditions of the Creative Commons “Attribution-NonCommercial-NoDerivatives 4.0 International” License (http://creativecommons.org/licenses/by-nc-nd/4.0/)

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