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X-Ray crystallographic structural studies on dimethyl sulfoxide and trimethylphosphine borane

Thesis (Ph.D.)--Boston University / PLEASE NOTE: Boston University Libraries did not receive an Authorization To Manage form for this thesis or dissertation. It is therefore not openly accessible, though it may be available by request. If you are the author or principal advisor of this work and would like to request open access for it, please contact us at open-help@bu.edu. Thank you. / Photographic X-ray diffraction data were used to determine the crystal and molecular structure of dimethyl sulfoxide near 5C. Of the total 868 unique X-ray reflections collected, 507 had measurable intensity, 270 were unobserved, and 91 were extinct. Near 5°C, dimethyl sulfoxide is found to be monoclinic with a = 5.303 +/- 0.005 A, b = 6.829 +/- 0.003 A, c = 11.693 +/- 0.010A, and B = 94°30' +/- 15'. The space group is P21/c with Z = 4. [TRUNCATED] / 2031-01-01

Identiferoai:union.ndltd.org:bu.edu/oai:open.bu.edu:2144/35559
Date January 1965
CreatorsThomas, Robert
PublisherBoston University
Source SetsBoston University
Languageen_US
Detected LanguageEnglish
TypeThesis/Dissertation
RightsCopyright by Robert Thomas 1965.

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