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Determination of Halogens in Organic Compounds by Using Sodium Fusion-Ion Chromatography Method

A sodium fusion-Ion chromatographic method for determination of fluorine, chlorine, bromine, and iodine in organic compounds is described. Seventeen organic halogen compounds and eleven mixtures were decomposed by Na fumes at 280-290°C for one hour or longer. The absorbing solutions were injected for ion chromatographic analysis using electrochemical and conductometric detectors. The arrangement of the apparatus includes the placement of the electrochemical and conductometric detectors. This method provides a mechanism providing for complete analysis for all four halogens in one ion chromatographic sample injection. Reproducibility is excellent and liquid sample handling is mentioned.

Identiferoai:union.ndltd.org:unt.edu/info:ark/67531/metadc504084
Date08 1900
CreatorsWang, Chung-Yu
ContributorsTarter, James G., Daugherty, Kenneth E.
PublisherNorth Texas State University
Source SetsUniversity of North Texas
LanguageEnglish
Detected LanguageEnglish
TypeThesis or Dissertation
Formativ, 59 leaves: ill., Text
RightsPublic, Wang, Chung-Yu, Copyright, Copyright is held by the author, unless otherwise noted. All rights reserved.

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