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Fourier transform ion cyclotron resonance studies of dendrimers and metal porphyrin-phthalocyanine sandwich complexes.

by Lim Che Lau. / Thesis (M.Phil.)--Chinese University of Hong Kong, 1996. / Includes bibliographical references (leaves 79-84). / Title Page --- p.i / Table of Contents --- p.ii / List of Tables --- p.iv / List of Figures --- p.v / List of Schemes --- p.vii / Acknowledgments --- p.viii / Abstract --- p.ix / Chapter CHAPTER 1: --- INTRODUCTION / Chapter 1.1. --- Historical Background --- p.1 / Chapter 1.2. --- FTICR with External Ion Source --- p.2 / Chapter 1.3. --- High Mass Analysis in FTICR --- p.4 / Chapter 1.4. --- Outline of Present Work --- p.7 / Chapter CHAPTER 2: --- INSTRUMENTATION AND EXPERIMENTAL / Chapter 2.1. --- Instrumentation --- p.8 / Chapter 2.1.1 --- Ion Source --- p.10 / Chapter 2.1.1.1. --- Liquid Secondary Ion Mass Spectrometry --- p.11 / Chapter 2.1.1.2. --- Electrospray Ionization --- p.12 / Chapter 2.1.2. --- Electrostatic Ion Focusing System --- p.15 / Chapter 2.1.3. --- ICR Analyzer Cell and Magnet --- p.18 / Chapter 2.1.4. --- Data Acquisition and Handling System --- p.22 / Chapter 2.2. --- Experimental --- p.22 / Chapter 2.2.1. --- Liquid Secondary Ion Mass Spectrometry --- p.22 / Chapter 2.2.2. --- Electrospray Ionization --- p.23 / Chapter 2.2.3. --- Nozzle-Skimmer Dissociation --- p.24 / Chapter 2.2.4. --- Sustained Off-Resonance Irradiation Collision- Induced Dissociation --- p.24 / Chapter 2.2.5. --- Data Acquisition and Processing --- p.27 / Chapter 2.2.6. --- Mass Calibration --- p.27 / Chapter CHAPTER 3: --- STRUCTURAL CHARACTERIZATION OF TERPYRIDINE-BASED POLYETHER DENDRIMERS AND THEIR IRON(II) METALLOCOMPLEXES BY LIQUID SECONDARY ION MASS SPECTROMETRY AND ELECTROSPRAY IONIZATION MASS SPECTROMETRY / Chapter 3.1. --- Introduction --- p.28 / Chapter 3.2. --- Sample Preparation --- p.29 / Chapter 3.3. --- Results and Discussion --- p.30 / Chapter 3.3.1. --- Liquid Secondary Ion Mass Spectrometry Studies --- p.30 / Chapter 3.3.1.1. --- Dendrimers --- p.30 / Chapter 3.3.1.2. --- Metallodendrimers --- p.41 / Chapter 3.3.2. --- Electrospray Ionization Mass Spectrometry Studies --- p.47 / Chapter 3.4. --- Conclusions --- p.53 / Chapter CHAPTER 4: --- STUDIES OF LANTHANIDE(III) PORPHYRIN- PHTHALOCYANINE HETEROLEPTIC SANDWICH COMPLEXES USING ELECTROSPRAY IONIZATION / Chapter 4.1. --- Introduction --- p.54 / Chapter 4.2. --- Results and Discussion --- p.55 / Chapter 4.2.1. --- Molecular Weight Determination --- p.57 / Chapter 4.2.2. --- Structural Elucidation --- p.65 / Chapter 4.2.3. --- Charge-Transfer Processes --- p.72 / Chapter 4.3. --- Conclusions --- p.76 / Chapter CHAPTER 5: --- CONCLUSIONS --- p.77 / References --- p.79

Identiferoai:union.ndltd.org:cuhk.edu.hk/oai:cuhk-dr:cuhk_321526
Date January 1996
ContributorsLau, Lim Che., Chinese University of Hong Kong Graduate School. Division of Chemistry.
PublisherChinese University of Hong Kong
Source SetsThe Chinese University of Hong Kong
LanguageEnglish
Detected LanguageEnglish
TypeText, bibliography
Formatprint, ix, 84 leaves : ill. ; 30 cm.
RightsUse of this resource is governed by the terms and conditions of the Creative Commons “Attribution-NonCommercial-NoDerivatives 4.0 International” License (http://creativecommons.org/licenses/by-nc-nd/4.0/)

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