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Radiochemical and Analytical Methods of Analysis of Radiological Dispersal Devices

<p> The events on September 11<sup>th</sup> 2001 and subsequent attacks in America and around the world have brought a renewed interest in the nation&rsquo;s security including the concern over the use of a nuclear or a radiological dispersal device (RDD). Research utilizing NAA and ICP-MS has been done in two separate projects in order to help address some of these concerns. A research assistantship from Savannah River National Laboratory was granted in order to identify the impurities and isotope ratios of <sup> 192</sup>Ir sources (chapters 2-4). An electrochemical dissolution method of the iridium was developed and used for sample preparation for ICP-MS analysis. ICP-MS analysis was then used to identify and quantify impurities and isotope ratios in iridium from various sources. The second research project has developed a series of lanthanide phosphate based nanoparticles for use as tagging and tracking agents (chapters 5-7). The composition of the nanoparticles were varied to provide a unique signature that can be rapidly and precisely measured in the field via neutron activation analysis. The nanoparticles could be used as a real-time in the field method for tracking and identifying materials such as explosives in a post detonation scenario.</p><p>

Identiferoai:union.ndltd.org:PROQUEST/oai:pqdtoai.proquest.com:13877171
Date16 April 2019
CreatorsSimmonds, Isaac D.
PublisherUniversity of Missouri - Columbia
Source SetsProQuest.com
LanguageEnglish
Detected LanguageEnglish
Typethesis

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