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Syntéza a analýza kompozitních oxidových keramik v přítomnosti nekonvenčních energetických polí / Synthesis and Analysis of Composite Oxide Ceramics in Presence of Nonconventional Energetic Fields

Synthesis and bulk analysis of composite ceramic oxide materials and materials with perovskite-defect structure is presented within this work. Syntheses of these advanced ceramics materials were carroed out by using of nonconventional techniques (microwave-assisted hydrothermal synthesis and polycondensation techniques) and by conventional mechanochemical activation followed by high temperature solid state reaction. X-Ray difraction (XRD), Rietveld analysis, scaning microscopy (SEM), microalysis EDS-SEM, thermal analysis (TG), infrared spectroscopy (IR), determination of particles size and specific surface area were used for description of synthesized products. In case of perovskite system based on La-Sr-Fe-Ti-O electrochemical properties were studied. Part of work was focused on chemical analysis of synthesized composite oxide materials and decomposition hard structured products by using of nonconventional fields.

Identiferoai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:233312
Date January 2010
CreatorsBartoníčková, Eva
ContributorsLapčík, Ĺubomír, Zmeškal, Oldřich, Cihlář, Jaroslav
PublisherVysoké učení technické v Brně. Fakulta chemická
Source SetsCzech ETDs
LanguageCzech
Detected LanguageEnglish
Typeinfo:eu-repo/semantics/doctoralThesis
Rightsinfo:eu-repo/semantics/restrictedAccess

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