MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight

Description

Yes / Measurement of molecular weight is an integral part of macromolecular and polymer characterization which usually has limitations. Herein, we present the use of a bench-top 80 MHz NMR spectrometer for diffusion-ordered spectroscopy as a practical and rapid approach for the determination of molecular weight/size using a novel solvent and polymer-independent universal calibration. / Royal Society. Grant Number: URF∖R1∖180274. Engineering and Physical Sciences Research Council. Grant Numbers: EP/V037943/1, EP/V007688/1, EP/V036211/1

Links & Downloads

1. Tooley O, Pointer W, Radmall R et al (2024) MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight. Macromolecular Rapid Communications. Accepted for Publication.
2. http://hdl.handle.net/10454/19863
3. https://doi.org/10.1002/marc.202300692

Tags

Diffusion-ordered spectroscopy

Macromolecule

Molecular weight

NMR spectroscopy

Polymer

Additional Fields

Identifer	oai:union.ndltd.org:BRADFORD/oai:bradscholars.brad.ac.uk:10454/19863
Date	03 March 2024
Creators	Tooley, O., Pointer, W., Radmall, R., Hall, M., Beyer, V., Stakem, K., Swift, Thomas, Town, J., Junkers, T., Wilson, P., Lester, D., Hadleton, D.
Source Sets	Bradford Scholars
Language	English
Detected Language	English
Type	Article, Published version
Rights	© 2024 The Authors. Macromolecular Rapid Communications published by Wiley-VCH GmbH This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited., CC-BY