A. The alcohol, 10-(4’-hydroxymethylphenyl)-1,2-benzanthracene, was prepared by the reduction or 10-(4’-carboxyphenyl)- 1,2- benzanthracene. The structure or the alcohol was proven by:
(1) Ultraviolet spectra
(2) Infrared spectra
(3) Elementary analysis
(4) Preparation or the benzoate
B. The preparation of the Grignard reagent of 10-(4’-bromophenyl)-1,2-benzanthracene was unsuccessful. An explanation of this anomaly was not discovered.
C. The Grignard reagent or 2-(1-naphthylmethyl)-chloro-benzene was prepared by the use or tetrahydrofuran and "entrainment" with methyl iodide. / M.S.
| Identifer | oai:union.ndltd.org:VTETD/oai:vtechworks.lib.vt.edu:10919/106111 |
| Date | January 1959 |
| Creators | Lewis, Claude Irenius |
| Contributors | Chemistry |
| Publisher | Virginia Polytechnic Institute |
| Source Sets | Virginia Tech Theses and Dissertation |
| Language | English |
| Detected Language | English |
| Type | Thesis, Text |
| Format | 63 leaves, application/pdf, application/pdf |
| Rights | In Copyright, http://rightsstatements.org/vocab/InC/1.0/ |
| Relation | OCLC# 26691045 |
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