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Preparation and characterization of halide-doped perovskite-type catalysts for oxidative dehydrogenation of ethane.

by Chan Ying. / Thesis (M.Phil.)--Chinese University of Hong Kong, 2001. / Includes bibliographical references. / Abstracts in English and Chinese. / Abstract --- p.i / 摘要 --- p.iii / Acknowledgements --- p.iv / Table of contents --- p.v / List of Tables --- p.ix / List of Figures --- p.xii / Chapter Chapter 1 --- Introduction / Chapter 1.1 --- Introduction --- p.1 / Chapter 1.2 --- Literature review of the ODE reaction over different catalysts --- p.4 / Chapter 1.2.1 --- The alkali metal and the alkaline earth metal oxide catalysts --- p.4 / Chapter 1.2.2 --- Rare earth oxide catalysts --- p.5 / Chapter 1.2.3 --- Transition metal oxide catalysts --- p.6 / Chapter 1.3 --- Perovskite-type oxide catalysts --- p.7 / Chapter 1.3.1 --- The structure of perovskites oxide --- p.7 / Chapter 1.3.2 --- Preparation method of perovskites oxide --- p.8 / Chapter 1.3.3 --- Literature review of perovskites oxide catalysts --- p.9 / Chapter 1.4 --- ODE mechanism --- p.11 / Chapter 1.5 --- Factors affecting the catalytic performance of catalysts --- p.12 / Chapter 1.6 --- surface and bulk characterization of perovskites-type oxide catalysts --- p.13 / Chapter 1.7 --- Objective of this research project --- p.15 / Reference --- p.15 / Chapter Chapter 2 --- Instrumentation / Chapter 2.1 --- Introduction --- p.20 / Chapter 2.2 --- Assessment catalytic performance --- p.20 / Chapter 2.3 --- "Brunauer, Emmett and Teller (BET)" --- p.23 / Chapter 2.3.1 --- Theory --- p.23 / Chapter 2.3.2 --- Experimental --- p.25 / Chapter 2.4 --- X-ray Diffraction (XRD) --- p.25 / Chapter 2.4.1 --- Theory --- p.25 / Chapter 2.4.2 --- Instrumentation --- p.26 / Chapter 2.5 --- X-ray Photoelectron Spectroscopy (XPS) --- p.28 / Chapter 2.5.1 --- Basic principles --- p.28 / Chapter 2.5.2 --- Qualitative analysis --- p.29 / Chapter 2.5.2.1. --- Chemical shift peaks --- p.29 / Chapter 2.5.2.2. --- Auger peaks --- p.30 / Chapter 2.5.2.3. --- Shake-up satellites --- p.30 / Chapter 2.5.3 --- Quantitative analysis --- p.31 / Chapter 2.5.3.1 --- Surface sensitivity and sampling depth --- p.31 / Chapter 2.5.3.2 --- Atomic concentration determination --- p.31 / Chapter 2.5.4. --- Instrumentation --- p.32 / Chapter 2.5.4.1 --- Ultra-high Vacuum --- p.32 / Chapter 2.5.4.2 --- Sample Introduction System --- p.33 / Chapter 2.5.4.3 --- X-ray Source --- p.33 / Chapter 2.5.4.4 --- Data processing --- p.34 / Chapter 2.6 --- O2-Temperature Programmed Desorption (02-TPD) --- p.37 / Chapter 2.7. --- Halogen Analysis --- p.37 / Chapter 2.7.1 --- The Determination of Chloride by Fajans Method --- p.37 / Chapter 2.7.2. --- The Determination of Fluoride Content by ISE Fluoride Electrode --- p.38 / Chapter 2.8. --- The Determination of Mn Concentration --- p.38 / Reference --- p.39

Identiferoai:union.ndltd.org:cuhk.edu.hk/oai:cuhk-dr:cuhk_323396
Date January 2001
ContributorsChan, Ying., Chinese University of Hong Kong Graduate School. Division of Chemistry.
Source SetsThe Chinese University of Hong Kong
LanguageEnglish, Chinese
Detected LanguageEnglish
TypeText, bibliography
Formatprint, xiv, 123 leaves : ill. ; 30 cm.
RightsUse of this resource is governed by the terms and conditions of the Creative Commons “Attribution-NonCommercial-NoDerivatives 4.0 International” License (http://creativecommons.org/licenses/by-nc-nd/4.0/)

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