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Návrh a testování vhodné metodiky pro čištění povrchů preparátů in situ pro elektronovou mikroskopii pomalými elektrony / Design and Testing of methodology for in-situ sample cleaning for low voltage electron microscopy

This thesis concentrates on the methodology of semiconductor samples preparation for low voltage scanning electron microscopy. In the first part a detailed theory of sample imaging using electron beam and difference between classical scanning electron microscopy (SEM) and low voltage scanning electron microscopy (LVSEM) is described. It is given a description of a contrast formation in SEM and LVSEM and theories describing a contrast formation of differently doped semiconductors. The second part contains experimental data. The advantages and disadvantages of cleavage and focused ion beam (FIB) milling as sample preparation techniques are discussed. FIB was found as the best method for sample preparation for the analysis of precisely defined location on the sample. It is necessary to use the lowest possible FIB accelerating voltage for final polishing, ideally 1 kV.

Identiferoai:union.ndltd.org:nusl.cz/oai:invenio.nusl.cz:230351
Date January 2012
CreatorsRudolfová, Zdena
ContributorsVávra,, Ivo, Kolíbal, Miroslav
PublisherVysoké učení technické v Brně. Fakulta strojního inženýrství
Source SetsCzech ETDs
LanguageCzech
Detected LanguageEnglish
Typeinfo:eu-repo/semantics/masterThesis
Rightsinfo:eu-repo/semantics/restrictedAccess

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