<p> This dissertation focuses on the examination of the influence of sample storage conditions on the accuracy and precision of hydrocarbon composition measurements of Jet A made with GC×GC/FID and the accuracy and precision of flash point measurements of Jet A made with a Tag closed cup flash point tester. Areas of focus also include the influence of the column load value used, the S/N threshold value used, and the number of measurements made for a single sample vial on the accuracy and precision of the GC×GC/FID results. This dissertation also describes the development of an analytical method for the identification and quantitation of alkylphenols in Jet A (which are the most abundant heteroatom containing compounds in jet fuel) by using preparative high-performance liquid chromatography (prep-HPLC) and two-dimensional gas chromatography with electron ionization time-of-flight mass spectrometry (GC×GC/(+)EI TOF MS).</p>
| Identifer | oai:union.ndltd.org:purdue.edu/oai:figshare.com:article/21971357 |
| Date | 10 February 2023 |
| Creators | Brent A Modereger (14516570) |
| Source Sets | Purdue University |
| Detected Language | English |
| Type | Text, Thesis |
| Rights | CC BY 4.0 |
| Relation | https://figshare.com/articles/thesis/EFFECTS_OF_STORAGE_CONDITIONS_AND_GC_GC_FID_PARAMETERS_ON_THE_COMPOSITION_AND_FLASH_POINT_OF_JET_A_AND_THE_IDENTIFICATION_AND_QUANTITATION_OF_ALKYLPHENOLS_IN_JET_A_USING_PREP-HPLC_AND_GC_GC_EI_MS/21971357 |
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