Yes / Understanding the chronology of Norse settlement is crucial for deciphering the archaeology of many sites across the North Atlantic region and developing a timeline of human-environment interactions. There is ambiguity in the chronology of settlements in areas such as the Northern Isles of Scotland, arising from the lack of published sites that have been scientifically dated, the presence of plateaus in the radiocarbon calibration curve, and the use of inappropriate samples for dating. This novel study uses four absolute dating techniques (AMS radiocarbon, tephrochronology, spheroidal carbonaceous particles and archaeomagnetism) to date a Norse house (the “Upper House”), Underhoull, Unst, Shetland Isles and to interpret the chronology of settlement and peat which envelops the site. Dates were produced from hearths, activity surfaces within the structure, and peat accumulations adjacent to and above the structure. Stratigraphic evidence was used to assess sequences of dates within a Bayesian framework, constraining the chronology for the site as well as providing modelled estimates for key events in its life, namely the use, modification and abandonment of the settlement. The majority of the absolute dating methods produced consistent and coherent datasets. The overall results show that occupation at the site was not a short, single phase, as suggested initially from the excavated remains, but instead a settlement that continued throughout the Norse period. The occupants of the site built the longhouse in a location adjacent to an active peatland, and continued to live there despite the encroachment of peat onto its margins. We estimate that the Underhoull longhouse was constructed in the period cal. AD 805–1050 (95% probability), and probably in cal. AD 880–1000 (68% probability). Activity within the house ceased in the period cal. AD 1230–1495 (95% probability), and most probably in cal. AD 1260–1380 (68% probability). The Upper House at Underhoull provides important context to the expansion and abandonment of Norse settlement across the wider North Atlantic region.

¹⁴C wiggle-matching was applied to two wood samples closely related to geological and archaeological events with associated dendrochronological dates, to demonstrate the accuracy of ¹⁴C dating with accelerator mass spectrometry (AMS). Wiggle-matching on charred wood with bark, excavated from a pyroclastic mud-flow deposited by the huge 10th Century eruption of the Baitoushan Volcano, revealed the eruption age as cal A.D. 935 +8/-5 with 95% confidence. This date is consistent with the eruption age of A.D. 912 to A.D. 972 estimated by dendrochronology on two wooden boards that had clear stratigraphical connections to the B-Tm tephra deposit in Japan, an ash fall layer formed by the eruption of the Baitoushan Volcano. The date is also consistent with an A.D. 937–938 date estimated by the analysis of varved sediments from Lake Ogawarako in Aomori prefecture. The other wooden board collected from the Mawaki archaeological site in Ishikawa prefecture was wiggle-matched as 783 +13/-11 cal B.C. with 95% confidence, which is consistent with the dates of 830 cal B.C. to 759 cal B.C. obtained for seven wooden poles from the same wooden structures as the wooden board. These results are highly encouraging for obtaining accurate dates on wood when dendrochronology cannot be used.

Based on Ph. D. Thesis--University of Southampton, 2002. / Includes bibliographical references.

Based on Ph. D. Thesis--University of Southampton, 2002. / Includes bibliographical references.

The assumption that prehistoric Native American land use practices had little impact on the North American landscape persists in the literature. However, recent research suggests the effects of prehistoric burning, deforestation and agriculture may potentially have been greater than previously considered. To resolve this discrepancy, quantitative estimates of changes in human population size and forest structure and composition over the course of the Holocene are needed. This thesis addresses this need by providing radiocarbon-based paleodemographic reconstructions and pollen-inferred estimates of vegetation change, as well as analyses of associations between the two at both continental and regional scales, from the late Pleistocene to the Anthropocene. One way to estimate paleodemographic change is to use the number of radiocarbon (14C) dates from a given area to study patterns of human occupation through time. A review of the literature and compilation of existing databases relevant to this method showed there is now sufficient data to study the paleodemographic history of many regions around the world. An analysis of 14C datasets from North America and Australia compared well with model-based reconstructions of past demographic growth, and provided higher frequency fluctuations in population densities that will be important for future research. Using a kernel density estimation approach, the first estimates of prehistoric population density for North America were obtained and synthesized into a series of continental-scale maps showing the distribution and frequency of 14C dates in the Canadian Archaeological Radiocarbon Database (CARD). The maps illustrated the space-time evolution of population and migration patterns, which were corroborated by independent sources of evidence. A methodology based on the statistical evaluation of cross-correlations between population and plant abundance was then developed to analyze the associations between these population estimates and plant communities derived from pollen databases. Periods of high spatial cross-correlation (positive and negative) between population and plant abundance were irregular and did not improve over time, suggesting that ancient human impacts are not discernable at a continental scale, either due to low populations or varying human land use practices. To further examine the relationship between pollen data and human land use at a regional scale, estimates of plant density and landscape openness are needed. The REVEALS (Regional Estimates of VEgetation Abundance from Large Sites) model corrects for the non-linear relationship between pollen production and plant abundance and can therefore be used to map histories of land use and land cover change. The model was applied to pollen records from lake sediments in the deciduous forest of southeastern Quebec. A preliminary analysis comparing these results to population density revealed low population during times of high Populus abundance and high population following the appearance of the mixed temperate forest suggesting a discernable human-environment association at regional scales. Overall, the results of thesis support the growing body of literature that suggests prehistoric Native Americans impacted their environments and that these impacts can be detected and quantified by integrating archaeological and paleoecological information. However, the timing, location, and intensity of human land use has changed in both space and time, suggesting regional- to local-scale analyses of human-environment interactions are most appropriate for continental North America. The methodology presented here can be used to study additional North American regions for the purpose of developing a continental history of human-environment interaction.

No description available.

Archaeological bones are usually dated by radiocarbon measurement of extracted collagen. However, low collagen content, contamination from the burial environment or museum conservation work have previously lead to inaccurate results, especially for old bones, compromising the ability to reconstruct reliable past chronologies. It is reported, for example, that up to 70% of Palaeolithic radiocarbon dates on bones are likely to be underestimates of the real age, blurring the picture of modern human dispersals and Neanderthal extinction. In this thesis, a method for isolating and radiocarbon dating the collagen amino acid hydroxyproline is described. Hydroxyproline consists of about 10% of bone collagen but is not found in significant amounts elsewhere in nature. The hydroxyproline dating method uses a mixed-mode (i.e. ion-exchange combined with hydrophobic chemistry), semi preparative HPLC methodology. The amino acids do not require derivatisation, and no organic solvents are used, thereby avoiding addition of carbon. The hypothesis of this thesis is that the hydroxyproline can be used as a bone specific biomarker, improving dating accuracy and making it possible to obtain radiocarbon determinations where previously it has been impossible. It was calculated that on average 3.3±1.4μg of contaminant carbon are added to each sample in the process of isolating the hydroxyproline, a low level suitable for 14C dating. It was investigated whether a deliberately contaminated bone and 'naturally' contaminated archaeological bones, yielding erroneous dates when dated using the normal pretreatment method, could be dated accurately using this method. In addition, a hydroxyproline date was obtained for a bone with too little surviving collagen to be dateable by the bulk collagen method. Finally, using the hydroxyproline dating method, the earliest direct ages for the presence of anatomically modern humans on the Russian Plain were obtained. The method proved to be a powerful tool that can help resolve longstanding archaeological questions.

Zuni Salt Lake (ZSL) is a large maar in the Red Hill-Quemado volcanic field located in west-central New Mexico in the southwestern USA. Stratigraphic analysis of sections in and around the maar, coupled with optically stimulated luminescence (OSL) and accelerator mass spectrometry (AMS) C-14 dating, indicate that ZSL volcanic activity occurred between similar to 13.4 and 9.9 ka and was most likely confined to a <= 500-year interval sometime between similar to 12.3 and 11.0 ka. The basal volcanic unit consists of locally widespread basaltic ash fallout interpreted to represent a violent or wind-aided strombolian eruption tentatively attributed to Cerro Pomo, a scoria cone similar to 10 km south of ZSL. Subsequent eruptions emanated from vents near or within the present-day ZSL maar crater. Strombolian eruptions of multiple spatter and scoria cones produced basaltic lava and scoria lapilli fallout. Next, a phreatomagmatic eruption created the maar crater and surrounding tephra rim and apron. ZSL eruptions ended with strombolian eruptions that formed three scoria cones on the crater floor. The revised age range of ZSL is younger and more precise than the 190-24 ka 2-sigma age range derived from previous argon dating. This implies that other morphologically youthful, argon-dated volcanoes on the southern margin of the Colorado Plateau might be substantially younger than previously reported.

Rivers are a significant source of particulate and dissolved organic carbon (POC, DOC) into inland waters and coastal systems and provide a fundamental linkage between the terrestrial, oceanic, and atmospheric carbon reservoirs. Recent studies have examined the relationship between the quantity and form (POC vs. DOC) of carbon delivered to the aquatic system; however, little is known about the age of POC and DOC exported and how the radiocarbon age may vary with latitude, topographic gradient, vegetation, and land use. I provide the first global synthesis of published radiocarbon values of POC and DOC (∆14C). Inclusion of DOC and POC parameters (µM, δ13C, ∆14C) reveal significant driving forces of DOC (µM), latitude, and elevation (m) as capable of explaining 25% of the variability in DO14C in rivers and POC (µM) and latitude accounting for 15% of the variability in PO14C. When δ13C of DOC and POC and latitude were incorporated with ∆14C of DOC observations, 61% of the variability in DOC age was explained revealing the necessity to include dissolved and particulate fractions of organic carbon to yield the most robust predictive models. This study found a global trend of increasing age of DOC and increasing δ13C of DOC and POC with increasing latitude. My study suggests future research should incorporate both particulate and dissolved OC parameters along with elevation, vegetation, land cover, and climate zones to increase understanding of what drives the age of carbon exported in riverine systems.

Radiocarbon content in tree-rings can be an excellent proxy of the past incoming cosmic ray intensities to the Earth. Although such past cosmic ray variations have been studied by measurements of 14C contents in tree rings with ≧10 year time resolution for the Holocene (1), there are few annual 14C data. There is a little understanding about annual 14C variations in the past with the exception of a few periods including the AD774-775 annual 14C excursion (2). Here, we report the result of 14C measurements using the bristlecone pine tree rings for the period from 5490 BC to 5411 BC with 1-2 year resolution, and a finding of an extraordinarily large 14C increase (20‰) from 5481 BC to 5471 BC (the 5480 BC event). The 14C increase rate of this event is much larger than that of the normal Grand Solar Minima. We propose the possible causes of this event are a special phase of grand solar minimum, or a combination of successive solar proton events and a normal grand solar minimum.