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Thesis (MScEng (Civil Engineering))--University of Stellenbosch, 2009. / The need for a more reliable testing procedure for the characterisation and Quality Assurance/ Control of Bitumen Stabilised Materials (BSMs), besides UCS and ITS testing, has long been recognised by the roads industry. In fact, at CAPSA 2004 and CAPSA 2007, discussions of improved test methods for granular materials, i.e. possible replacement tests for CBR procedures, were conducted in workshops. Triaxial testing for the evaluation of shear parameters is widely recognised as a reliable method of measuring these critical performance properties of granular and Bitumen Stabilised Materials (BSMs). However, the triaxial test in its current state as a research test has little chance of extensive use by practitioners and commercial laboratories, because of complexity, cost and time issues. Major adaptations to the research triaxial test are necessary, before this useful test can have a chance of being accepted by road practitioners. The main aim of this study is to investigate possibilities of developing a simple, affordable, reliable and robust test for characterizing granular and bitumen stabilized materials thus linking test outcome with in-situ performance. This is achieved through the innovative design and manufacture of a prototype triaxial cell capable of accommodating 150 mm diameter by 300 mm deep specimens. The cell is simpler than the research (geotechnical) triaxial cell and the operational protocols have been streamlined, thereby reducing the time and steps required in assembling specimens and testing them. In order to ensure the development of an appropriate triaxial cell for industry, a survey was conducted aimed at investigating currently available facilities, testing capacity and resources within civil engineering laboratories in South Africa. Findings of the survey (Appendix 4) have provided guidance with regard to the nature and sophistication of any new tests to be developed. The survey highlighted some of the limitations and lack of sophistication of the current loading frames used for CBR and UCS testing such as lack of electronic LVDTs, limited overhead space, limited loading capacity and others. Most laboratories would need to invest in new loading facilities to carry out triaxial tests. A review of the test procedure for monotonic triaxial test showed that two main factors contribute to the complexity of the research (geotechnical) triaxial cell namely, time taken to assemble the specimen accurately in the cell and secondly the inherent design of the cell which makes it water and/or air tight at relatively high pressures. The design of the Simple Triaxial Test, therefore, was aimed at overcoming the drawbacks of research triaxial test e.g. fitting a membrane to each specimen to be tested, through considerable simplification by means of a new structure design and procedure of assembly of specimen into the cell. The advantage of addressing these issues would be reduction in the number of steps required in the test procedure and therefore reduction in testing time. The design of the cell particularly was preceded by a conceptualization process that involved investigation of numerous options. Concepts such as the bottle, encapsulated-tube, bottle and sandwich concepts were considered and given reality checks. In addition, available triaxial procedures of a similar nature e.g. Texas Triaxial, were evaluated and analyzed. Ultimately, with some trials and innovation, a design was developed for a simple triaxial cell comprising a steel casing with a latex tube which is then introduced around the specimen sitting on a base plate. It is based on the ‘tube concept’ in which the specimen acts like a ‘rim’ and the cell acts like a ‘tyre’ providing confinement to the triaxial specimens for testing, within the tube. This approach eliminates the use of O-rings and membranes for the specimen and tie-rods for the triaxial cell, thus reducing testing time considerably. The overall dimensions of the cell are 244 mm diameter by 372 mm height (Appendix 5). The cell was manufactured at Stellenbosch University Civil Engineering workshop and preliminary tests were conducted under this study. Parallel tests were also conducted with the Research Triaxial Test setup at Stellenbosch University in order to determine if preliminary results obtained with the Simple Triaxial Test setup were comparable therefore providing a means of validating the data. Results of analysis of variance (ANOVA) show that variability between Simple Triaxial Test (STT) and Research Triaxial Test (RTT) results is less significant whilst that within samples of STT and RTT results is quite significant. Comparisons also show that good correlation were obtained from Reclaimed Asphalt Pavement (RAP) Hornfels + 3.3 % Emulsion + 0 % Cement mix and mixes with the G2 base course aggregate whilst completely different correlation was obtained from RAP + 3.3 % Emulsion + 1% Cement. It is evident however that the differences observed stem from material variability i.e. random variability to one degree or the other and not to the STT apparatus. It is recommended for future research that more STT versus RTT testing be done especially on a mix with known mechanical properties when compacted to a specified dry density, e.g. graded crushed stone (G1) compacted to 100% mod. AASHTO. In summary, a locally made, low cost, relatively durable triaxial cell with relatively easy and quick specimen assembly procedures has been developed. It is now possible to perform triaxial tests on 150 mm diameter by 300 mm high specimen relatively easily and quickly. However, the challenge of validating results obtained, as well as improving the manufacture process of its main component, the tube, still remains.

Thesis (MEng)--University of Stellenbosch, 2001. / ENGLISH ABSTRACT: The use of polymer modified binders have increased drastically over the past twenty years. It is generally accepted that current empirical specification tests do not adequately characterise the improvement in binder properties when bitumen is modified with polymers. At the University of Stellenbosch, a programme was initiated to relate binder properties to asphalt mix performance. This study forms part of that programme. This study focuses on three binders and is an attempt to characterise binder properties fundamentally. The binders that were tested are: • 60/70 penetration grade bitumen • SBS modified 60/70 bitumen • Bitumen-Rubber Two rheometers were used to characterise the binder properties: • Sliding Plate Rheometer (SPR) • Dynamic Shear Rheometer (DSR) The Sliding Plate Rheometer was modified to allow testing at elevated temperatures. The modification is described in this thesis. Three types of testing were used to test the binders: • Creep tests (SPR and DSR) • Dynamic tests (Strain and Frequency Sweeps - DSR) • Flow tests (high temperature viscosity tests - DSR) The results of the tests were used to characterise differences between the binders. Shear susceptibility lines were plotted and viscosities calculated from the creep test results; Master Curves and Black Diagrams were plotted from frequency sweep results; flow test results were used to characterise high temperature behaviour. A further development in the asphalt industry is the move towards the development of performance based specifications. A programme has been initiated in this regard and this study forms part of the programme. As a step towards the development of performance based specifications filler was included in this study. BinderlFiller systems were subjected to the same test programme the binders were, to characterise the influence on binder properties of filler addition. Some of the conclusions that were drawn at the end of the study are: • Polymer modification improves binder properties related to rutting. • Filler addition does not affect binder properties negatively. • Shear rate is very important during production of asphalt mixes and construction of asphalt layers containing polymer modified binders. / AFRIKAANSE OPSOMMING: Die gebruik van polimeer gemodifiseerde bitumen het drasties toegeneem oor die afgelope twintig jaar. Dit word algemeen aanvaar dat die huidige empiriese spesifikasie toetse nie die verbetering in bindmiddeleienskappe van polimeer modifisering aanvaarbaar karakteriseer nie. 'n Program is geïnisieer by die Universiteit van Stellenbosch om 'n verband te vind tussen bindmiddeleienskappe en asfaltmengseleienskappe. Hierdie studie vorm deel van die program. Hierdie werk fokus op drie bindmiddels en is 'n poging om die bindmiddeleienskappe fundamenteel te karakteriseer. Die bindmiddels wat gebruik is in hierdie werk, is: • 60/70 penetrasiegraad bitumen • SBS gemodifiseerde 60/70 bittimen • Bitumen-Rubber Twee reometers is gebruik om bindmiddeleienskappe te karakteriseer: • Glyplaat Reometer (SPR) • Dinamiese SkuifReometer (DSR) Die glyplaat reometer is aangepas om toetse by hoër temperature te doen en die aanpassing wat gemaak is word in die tesis beskryf. Drie tipes toetse is uitgevoer om die bindmiddels mee te toets: • Kruiptoetse (SPR en DSR) • Dinamiese toetse (DSR) • Vloei toetse (DSR) Die resultate van die toetse is gebruik om die verksille tussen die bindmiddels te kwalifiseer. Verskillende grafieke en figure is getrek van die resultate om die onderskeie bindmiddels te karakteriseer. Die beweging weg van empmese spesifikasies na werkverrigting gebaseerde spesifikasies in die asfalt industrie is 'n verder nuwe ontwikkeling. 'n Program is geïnisïeer ten opsigte hiervan en hierdie werk vorm deel van die program. As 'n stap in die ontwikkeling van die werkverrigting gebaseerde spesifikasies is 'n vuIler ingesluit in die toetsprogram. Bindmiddel/vuIler stelsels is onderwerp aan dieselfde toetse waaraan die bindmiddels onderwerp is om die invloed van die vuIler op die bindmiddels te karakteriseer. Sommige van die gevolgtrekkings waartoe gekom is aan die einde van die tesis, is: • Polimeer modifisering verbeter bindmiddeleienskappe met betrekking tot wielsporing. • Die toevoeging van vuIler affekteer nie die bindmiddeleienskappe negatiefnie. • Die vervormingstempo is van groot belang wanneer asfaltmengsels gemeng en lae gebou word van mengsels wat polimeer gemodifiseerde bitumen bevat.

Thesis (MScEng (Civil Engineering))--University of Stellenbosch, 2010. / ENGLISH ABSTRACT: The research conducted in this study forms part of the Phase II process of the Bitumen Stabilized Materials (BSMs) Guideline improvement initiative. The initiative aims to address areas of concern in the cold mix design procedures for BSMs. Current road rehabilitation using the bitumen stabilization process requires testing of representative specimens as means to evaluate pavement performance over time. In order to adequately acquire specimens representative of field conditions, it is necessary to condition the materials in a process called curing. Although curing procedures have been standard in many countries on different continents, the protocols are varied and an acceptable procedure is currently not available. In order to develop an acceptable curing protocol for BSMs, both field and laboratory environments were investigated. Considering that curing takes time in the field, production of representative samples intended for laboratory testing must undergo accelerated curing in the laboratory. Given the complexities involved in achieving close correlations between field and laboratory environments, the research strived to reconcile field and laboratory material behaviour. In particular, the main objective of the research was to unify the curing protocol for BSMs, with the standardization of the curing protocol being top priority. In this study, laboratory results have confirmed that the different natures of curing mechanisms inherent in a BSM-foam and BSM-emulsion contribute to irreconcilable material behaviour(s). Results have confirmed that curing of BSM-foam is largely a function of water repulsion, with the addition of active filler dominating material performance almost immediately. Unlike BSM-foam, curing of BSM-emulsion is both a function of the breaking of emulsion during the initial phase and the gradual release of moisture with time. In this instance, BSM-emulsion material performance resembled active filler influences past the breaking of the emulsion cycle. Consequently, given the observed differences regarding material behaviour(s), the unification of the curing protocol for BSMs has not been successful. In terms of accommodation of active filler in the final curing protocol for BSMs, findings in this research have revealed that active filler’s tendency to absorb moisture in the initial stages requires longer curing time to help extract the absorbed moisture during the curing process. Although the use of active filler has an impact on curing, its inclusion in a BSM does not justify its extension in the curing time as cementation is not one of the desired properties of these materials. BSMs are primarily desirable for their flexibility in pavement structures. For this reason, active filler was omitted in the final curing protocol due to reasons of simplifying the mix design process. In conclusion, different curing protocols were tested and developed to help produce reconcilable material behaviour in both the field and laboratory environments. Through the reconciliation of key material properties such as the resilient modulus, long term equilibrium moisture conditions and shear parameters, an acceptable standardized curing protocol for BSM-foam and BSMemulsion intended for application in industrial laboratories across South Africa was successfully developed. / AFRIKAANSE OPSOMMING: Die navorsing tydens hierdie studie gedoen, vorm deel van die Tweede fase van die Bitumen Gestabiliseerde Materiale Riglyne verbeteringsinisiatief. Die inisiatief het ten doel om areas van bekommernis in die kouemengsel-ontwerp-prosedures vir Bitumen Gestabiliseerde Materiale aan te spreek. Huidige padrehabilitasie wat gebruik maak van die Bitumen Gestabiliseerde Materiale proses, vereis toetsing van verteenwoordigende monsters om sodoende plaveiselgedrag oor ‘n tydperk te evalueer. Materiale moet deur die verouderingsproses gekondisioneer word, om sodoende monsters te verkry wat akkuraat verteenwoordigend van veldtoestande is. Alhoewel verouderingsprosesse in meeste lande - op verskillende kontinente - gestandariseerd is, is die protokol verskillend en ‘n aanvaarbare prosedure is nie tans beskikbaar nie. Beide veld- en laboratoriumomgewings is ondersoek, om sodoende ‘n aanvaarbare verouderings-protokol vir Bitumen Gestabiliseerde Materiale te ontwikkel. Wanneer in ag geneem word dat veroudering in die veld tydrowend is, moet vervaardiging van verteenwoordigende monsters vir laboratoriumgebruik versnelde veroudering in die laboratoruim ondergaan. Gegee die kompleksiteite betrokke om goeie korrelasie tussen velden laboratoriumomgewings te verkry, het die navorsing daarna gestreef om die veld- en laboratoriummateriaalgedrag te verenig. Die hoofdoel van die navorsing was om die verouderingsprotokol vir Bitumen Gestabiliseerde Materiale te verenig met die stardaardisering van die verouderingsprotokol as top prioriteit. In hierdie studie het laboratorium resultate bevestig dat die verskillende aard van voorbereidings- meganismes inherent in BSM-skuim en BSM-emulsie bydra tot onversoenbare materiaalgedrag. Resultate het bevestig dat voorbereiding van BSM-skuim ’n funksie van waterrepulsie het en met die byvoeging van aktiewe vullers dominieer dit die materiaalgedrag byna onmiddelik. Anders as BSM-skuim is die voorbereiding van BSM-emulsie beide ’n funksie vir die breek van emulsie tydens die begin fase en die geleidelike vrystelling van vog oor tyd. In hierdie geval het BSM-emulsie se materiaalgedrag die invloed van aktiewe vuller getoon nadat die emulsie gebreek het. Gevolglik, weens die waargenome verskille rakende materiaalgedrag is die vereniging van die voorbereidings- protokols vir BSMs nie suksesvol nie. In terme van inagneming van aktiewe vullers in die finale voorbereidingsprotokol vir BSM’s, is deur navorsing bevind dat aktiewe vullers neig se neiging om vog te absorbeer in die beginstadia dit benodig dus ‘n langer verouderingstyd vir die ontrekking van die geabsorbeerde vog. Hoewel die gebruik van aktiewe vullers ’n impak het op die voorbereiding, reverdig dit nie die verlenging van die verouderingstyd vir die insluiting daarvan in BSM nie, siende dat sementering nie een van die gewenste eienskappe van hierdie materiaal is nie. BSMs word hoofsaaklik verkies vir sy buigsaamheid in paveiselsturkture. Om die mengselontwerp prosesse te vereenvoudig, was aktiewe vullers dus weggelaat in die finale voorbereidingsprotokol. Ter afsluiting was verskeie voorbereidings protokolle getoets en ontwikkel om te help met die vervaardiging van versoenbare materaalgedrag in beide veld-en-laboratoriumomgewings. Deur die versoening van kern materiaal eienskappe soos die elastisiteitsmodulus, lang termynewewigvog kondisies en skuifparameters, is ’n aanvaarbare gestandariseerde voorbereidingsprotokol vir BSM-skuim en BSM-emulsie bedoel vir aanwending in industriele laboratoriums regoor Suid Afrika suksesvol ontwikkel.

Thesis (MScEng)--Stellenbosch University, 2013. / ENGLISH ABSTRACT: Factors influencing surface run-off of bitumen emulsions were studied in order to understand binders for use in the construction of surfacing seals. Run-off of the binder from the road surface causes an inconsistent film thickness leading to ravelling (Johannes, Hanz & Bahia n.d.) and bleeding at the upstream and downstream regions, respectively. There is currently no accepted specification for surface run-off viscosity. Practice mainly relies on empirical tests and experience. As the establishment of such a specification encompasses performance of the binder in various environments or field conditions, this study was undertaken to determine performance of the selected binder. Viscosity was kept constant by spraying the emulsion at a constant temperature and also holding the pavement temperature constant. In order to study the run-off behaviour of the binder, run-off tests were conducted at various gradients, texture depths and spray rates. Surfacing seals of various texture depths were constructed in the laboratory. Using a spray bar, the emulsion was sprayed at various spray rates. The sample surfaces were tilted to various gradients. Results portrayed the effects of the three factors (spray rate, gradient and texture depth) on the amount of runoff. An increase in the magnitude of the factors resulted in a variation in the runoff (increase or decrease). One notable finding was that the runoff from the 9.5 mm seal was less than that from the 13.2 mm seal. The other significant finding was that spray rate had the largest effect on runoff, followed by texture depth, and gradient. / AFRIKAANSE OPSOMMING: Sekere eienskappe wat oppervlakdreinering van bitumen emulsies op paaie beinvloed, is bestudeer om sodoende binders wat gebruik word in die konstruksie van die seëls beter te verstaan. Afloop van die binder vanaf die padoppervlak kan lei tot die vorming van ‘n laag met ongelyke dikte wat moontlike rafeling (Johannes, Hanz & Bahia nd) en bloeing vanuit die onderkant van die pad tot gevolg kan hê. Daar is tans geen aanvaarde spesifikasies wat hierdie verskynsels inperk nie. Konstruksie praktyk berus hoofsaaklik op empiriese toetse en ondervinding. Hierdie studie is dus onderneem om prestasie van die geselekteerde binder vas te stel. Viskositeit was konstant gehou deur die aangewende emulsie en padtemperatuur konstant te hou. Ten einde die afloopgedrag van die binder te bestudeer, is toetse uitgevoer op verskeie hellings, tekstuurdieptes en aanwendingskoerse. Seëls van die verskillende tekstuurdieptes is gebou in die laboratorium, en emulsies op hierdie oppervlaktes aangewend. Die toetsoppervlakte is gekantel om die vereiste helling te kry. Resultate vir die drie faktore wys die invloed op afloop. ‘n Toename in die grootte van die faktore het gelei tot 'n variasie in die afloop (toename of afname). Een noemenswaardige bevinding was dat die afloop van die seël van 9,5 mm minder was as dié van die seël van 13,2 mm. Belangrike bevindinge sluit ook in dat die spuitkoers die grootste invloed het op afloop, gevolg deur die tekstuur diepte en die gradiënt.

Thesis (MEng)-- Stellenbosch University, 2013. / ENGLISH ABSTRACT: Two common methods of road pavement, granular material stabilisation used in road construction throughout South Africa today include Cold in Place Recycling (CIPR) and stabilisation with cement or bitumen and an active filler to create Bitumen Stabilised Materials (BSM). As part of the updating of the South African Pavement Design Method (SAPDM) an experimental section, investigating the structural capacity of cement and lime stabilised and BSM pavement layers, was constructed and will be monitored over a two year period. As part of this study Falling Weight Deflectometer (FWD) measurements were taken on the various experimental stabilised pavement layers constructed. The FWD deflection data, measured at various time intervals over a 360 day period, forms the basis of the study presented here. The objective of this thesis was to identify typical back-calculated layer stiffnesses and their variability over time for the various in-situ recycled and stabilised base layers constructed within the experimental section. Stabiliser type, content and layer thicknesses were varied across experimental sub-sections. Trends in back-calculated stiffness of cement stabilised base layers consistently showed significant reductions in layer stiffness subsequent to construction traffic loading. Subsequent to the initial reduction in stiffness little change in stiffness was noted under normal traffic loads. Observations on the trends in back-calculated stabilised layer stiffness per material type over time indicated that seasonal moisture and temperature fluctuations have an effect on the stiffness of the pavement structure as a whole. BSM materials showed significant variability over time in-line with seasonal variability in the supporting subgrade stiffness in the southbound lane. BSM materials with 1% cement added in the northbound lane show initial stiffness reductions due to direct rainfall application however a significant increase in layer stiffness occurs up to 360 days after construction. BSMs with 2% cement in the northbound lane show significant increases in layer stiffness over the 360 day observation period. No significant difference in stiffness trend was observed between BSM emulsion a BSM foam materials. The BSM emulsion with 0.9% residual bitumen and 1% cement was observed to show rapid reduction in stiffness upon opening to traffic and reverting to stiffness values similar to an unbound material of approximately 350 MPa. Cement and lime stabilised materials showed typical post 28 –day average stiffnesses per sub-section ranging between 600 MPa and 1800 MPa. BSM foam with 1% cement added were observed to have average stiffnesses per sub-section in the range of 400MPa to 2200 MPa and BSM emulsion with 1% cement with stiffnesses between 400 MPa to 1700 MPa over the 360 day period. BSMs with 2% cement added showed stiffness ranges between 900 MPa to 4300 MPa for BSM foam and 900 MPa to 3900 MPa for BSM emulsions over the 360 day period. The spatial variability of back-calculated stiffness per sub-section of a particular stabilisation design was significant and was observed, through the Co-efficient of Variation (COV), to increase over time. The effect of the observed variability when incorporated into a pavement design scenario, requiring a design reliability of 90%, showed 50% of the pavement structure would be overdesigned by a factor of 4. With respect to the current philosophies on the development of stiffness over time of cement and lime stabilised and BSM pavement layers some useful observations were made. Cement stabilised materials correlate well with stiffness development theories predicted by previous studies. Theories relating to the stiffness development of BSMs however did not predict the levels of variability in base layer stiffness observed on the experimental section. The continued observation of the experimental section for another year will give greater insight to the stiffness trends of the stabilised materials discussed above.

Thesis (PhD)--Stellenbosch University, 2014. / ENGLISH ABSTRACT: The increased use of reclaimed asphalt (RA) in Bitumen Stabilised Materials (BSMs), shortcomings in the existing design guidelines and manuals and ongoing developments in the concepts and understanding of these materials require further research into the fundamental properties and behaviour of BSMs. The state-of-the-art of foamed bitumen techniques is reviewed in the literature study. Current best practices in the design of BSMs and pavements incorporating such materials are also included in this literature study. Shortcomings and areas for further improvement of the design practice have been identified. With new environmental legislation, the importance of BSM technology including RA as an environmentally-friendlier and more sustainable construction technique is set to increase in the coming years. Changes in the behaviour of materials and failure mechanisms of BSM mixes are long-term phenomena. This implies that the study of the physico-chemical and mechanical properties of the mixes with increasing amount of RA is vital. Therefore, fundamental understandings of moisture damage and thermo-physical characteristics, which are related to material properties, are required. The main objective of this study is to advance BSM technology by assessing the influence of the selected materials on durability behaviour, temperature distribution and long-term performance in all phases of application (i.e. mix design, construction, and in-service condition). This study begins with a comprehensive literature review of research dealing with the interactions between RA and mineral aggregates. The properties of RA and mineral aggregates were reviewed. This was followed by a review into the mechanical properties of BSM-foam mixes with high percentage of RA and its durability performance. Factors influencing the temperature gradient of BSMs were then identified. Achieving a better understanding of the fundamental performance properties and temperature influence on the behaviour of BSMs with high percentage of RA is one of the key factors of this research, with a view to using the extended knowledge for improvements to current mix design and structural design practices. Finally, the fundamental theories on thermo-conductivity and the mechanical properties of the BSM were used to create a relationship between temperature and mechanical properties in a pavement section. A laboratory testing programme was set up to study the properties and behaviour of BSMs and to establish links with the compositional factors, i.e. the type of binder used, the percentage of RA in the mix and the addition of a small amount of cement as active filler. BSMs were blended in three different proportions of RA and good quality crushed stone materials: 100% RA (with 2 % bitumen content), 50% RA and 50% G2 Hornfels crushed stone (with 2.1% bitumen content) and 100% G2 (with 2.3 % bitumen content). Tri-axial testing was carried out to determine shear parameters, resilient modulus and permanent deformation behaviour, while brushing testing was carried out to determine the possible durability performance of the BSMs. The mixture durability in terms of moisture damage was investigated. Temperature data were collected and a model to accurately simulate the temperature distribution in the BSMs was identified and proposed for further investigation and validation. It was found from the laboratory temperature data collected in this study that the temperature gradient varied according to the depth of the BSMs. A considerable part of the efforts of this study were dedicated to characterise and model the temperature distribution in a pavement section, taking into account the mechanical properties and performance of the BSMs at different temperature layers. The study provides an insight into fundamental mechanical performance, material durability properties, and the thermal capacity and conductivity of the BSM-foam mixes with high percentage of RA. This will assist in improving the current procedure for selection, combining and formulation of the mix matrices for BSMs. In addition, the study provides guidelines that will enable practitioners to confidently understand the relationship between temperature gradient and mechanical behaviours of BSM-foam pavement section. The specific durability-related issues addressed in this study are substance for future research. / AFRIKAANSE OPSOMMING: Die toenemende gebruik van herwonne asfalt (Engels: reclaimed asphalt (RA)) in bitumen gestabiliseerde materiaal (Engels: Bitumen Stabilised Materials (BSMs)), tekortkominge in die bestaande ontwerpriglyne- en handleidings en deurlopende verbeteringe in die konsepte en begrip van hierdie material vereis verdere navorsing oor die fundamentele eienskappe en gedrag van BSM. In die literatuurstudie word die huidige stand van kennis van die ontwerp van skuimbitumentegnieke ondersoek. Die literatuurstudie dek ook die huidige beste praktyke in die ontwerp van BSM en plaveisels wat hierdie materiale insluit. Tekortkominge en areas van verdere verbetering in die ontwerppraktyke is geïdentifiseer. Onlangse omgewingswetgewing verhoog die belangrikheid van BSM tegnologie, insluitend RA, as ‘n meer omgewingsvriendelike en volhoubare konstruksie-tegniek. Hierdie faktor sal in die toekoms al hoe belangriker word. Die verandering in die gedrag van materiaal en die falingsmeganismes van BSM mengsels is langtermynverskynsels. Dit impliseer dat die studie van die fisio-chemiese en meganiese eienskappe van mengsels met toenemende verhoudings van RA van kardinale belang is’n Fundamentele begrip van die vogskade en temo-fisiese eienskappe, wat verwant is aan die materiale se eienskappe, word vereis. Die primêre doelwit van die studie is die bevordering van BSM tegnologie deur die invloed van die geselekteerde materiale op duursaamheid, temperatuurverspreiding en langtermyn gedrag in al die fases van toepassing (mengselontwerp, konstruksie en in-dienstoestand) te bepaal. Die verhandeling begin met ‘n omvattende literatuuroorsig van navorsing oor die interaksie tussen RA en mineraalaggregate. Die eienskappe van RA en die mineraalaggregate word bespreek. Dit word gevolg deur ‘n oorsig van die meganiese eienskappe van die BSM-skuimbitumenmengsels met ‘n hoë persentasie RA en die duursaamheidgedrag daarvan. Faktore wat die temperatuurgradient van BSM beïnvloed word dan aangetoon. ‘n Beter begrip van die fundamentele gedragseienskappe en die invloed van temperatuur op die gedrag van BSM met ‘n hoë persentasie RA is een van die sleutelfaktore van hierdie navorsing. Dit het ten doel om die uitgebreide kennis te gebruik om huidige mengselontwerp en strukturele ontwerppraktyke te verbeter. Laastens is die fundamentele teorie van termogeleiding en die meganiese eienskappe van BSM gebruik om ‘n verhouding tussen temperature en meganiese eienskappe in ‘n plaveiselsnit te ontwikkel. ‘n Laboratoriumtoetsprogram is opgestel om die eienskappe en gedrag van BSM te bestudeer en om verwantskappe tussen samestellende faktore soos die tipe bindmiddel gebruik, die persentasie RA in die mengsel en die toediening van klein hoeveelhede sement as aktiewe vuller te bepaal. BSM is in drie verskillende verhoudings van RA en goeie gehalte gebreekte klipmateriaal vermeng: 100% RA met 2 % bitumen, 50% RA en 50 % G2 Hornfels gebreekte klip met 2.1 % bitumen en 100% G2 met 2.3 % bitumen. Drie-assige druktoetse is gebruik om skuifsterkteparameters, elastiese modulus en permanente vervormingsgedrag te bepaal. Borseltoetse is gebruik om die duursaamheidgedrag van BSM te bepaal. Die mengsels se duursaamheid is ook in terme van vogskade ondersoek.

Thesis (MScEng)--Stellenbosch University, 2014. / ENGLISH ABSTRACT: This research investigates the flexibility and the performance properties of bitumen stabilised materials under the influence of mix variables. The laboratory testing consisted of two main phases. During the first phase (mix design), the strength and the flexibility of the mixes were assessed through ITS (Indirect Tensile Strength), UCS (Unconfined Compressive Strength), displacement at break, strain at break and fracture energy. The second phase consisted of a series of triaxial tests done to assess the performance properties (shear strength: cohesion and angle of internal friction; and stiffness: resilient modulus) of the mixes. The mineral aggregates used in this study were milled from different locations of the R35, near Bethal. This was a blend of granular material (dolerite, from various locations of the existing base and subbase layer of the R35) and Reclaimed Asphalt (RA) milled from the existing surfacing. During the mix design phase, two types of bituminous binders were used (bitumen emulsion and foamed bitumen) at bitumen content ranges of 2%, 2.4% and 2.8% each. Two types of active filler were used separately and in combination at a proportion of 1% and 2%. Finally, specimens were tested in wet and dry conditions for each mix combination. During the triaxial testing phase, only the optimum bitumen content of 2.4% was used, both for bitumen emulsion and foamed bitumen, with only cement as active filler in a proportion 1% and 2%. The specimens were tested at different ranges of densities and saturation levels. The flexibility of the mix was assessed through the fracture energy, the strain and the displacement at break parameters. An analysis of variance (ANOVA) was conducted on the data to assess the significance of experimental variables on this property. This property was found to be very sensitive to bitumen and cement content added to the mix. When assessing the combined effect and the significance of the variables on the flexibility of the mixes, it was found that fracture energy is mostly influenced by the cement content, followed by the bitumen content, then the type of treatment and finally the testing condition. However, the level of significance was not in the same order for the other two parameters (displacement and strain at break). It was also found that the combined effect of some independent variables (cement content + testing condition, type of treatment + cement content + bitumen content) had a significant effect on the fracture energy and the strain at break respectively. From the ITS and UCS tests, an increase in strength was noticed with the increase of cement content. On the other hand, the increase in bitumen content led to a decrease in strength of the material. The statistical analysis on the ITS and UCS values show that the independent variable with the most significant effect on the ITS is the cement content, followed by the testing conditions, then the bitumen content and finally the type of treatment. The combined effect of cement content + bitumen content was found to be significant both for ITS and UCS. In the second phase triaxial tests were performed in order to evaluate the performance properties of the mixes. It was found that the increase of the active filler content significantly improves the shear strength of the material. It was also found that at a fixed cement content, specimens tested at low density and/or high level of saturation show low shear strength. The Mr-θ model was used to model the resilient modulus of the mixes and the model coefficients used to evaluate the effect of experimental variables on the resilient modulus. It was found that the resilient modulus of the mixes increases as the bulk stress increases. This confirms the stress dependent behaviour of bitumen stabilised materials. The analysis show that increasing the percentage of active fillers content results in a significant increase in the resilient modulus values. An increase in relative density also resulted in an increase in the resilient modulus of the mixes, while the opposite effect was observed with the increased of the saturation level. Besides the engineering properties and the mechanical test parameters, other parameters such as the Tensile Strength Ratio (TSR) was calculated in order to evaluate the moisture sensitivity of the mixes. Weakening due to moisture was found to be more predominant in the mixes with less active filler. In addition, bitumen emulsion mixes were found to have a better resistance to moisture weakening effects compared to foamed bitumen. In addition, a comparison between the rapid curing and the accelerated curing was done. Higher ITS and UCS results were obtained for specimens cured using long term curing compared to specimens cured using the accelerated curing method. In conclusion, flexibility is an important property of bitumen road construction material (bitumen stabilised material include) however, it is not an easy property to measure. Although, displacement/strain at break and fracture energy from ITS and UCS were able to give us some indications on the main factors governing the flexibility of bitumen stabilised materials (the bitumen and active filler content), more accurate and adequate tests are required to evaluate the parameter. / AFRIKAANSE OPSOMMING: Die buigsaamheid en gedragseienskappe van bitumen gestabiliseerde materiale was getoets om sodoende die invloed van verskeie mengselveranderlikes te evalueer. Die ondersoek het uit twee fases bestaan. Tydens die eerste fase (mengfase) is die sterkte en buigsaamheid deur middel van indirekte treksterkte toetse (ITS), onbegrensde druksterkte toetse (UCS), verplasing – en vervorming by breekpunt sowel as breek-energie toetse gedoen en ondersoek. Die tweede fase het bestaan uit ʼn reeks drie-assige triaksiaal toetse. Triaksiaaltoetse is uitgevoer om die gedragseienskappe soos die skuifsterkte, kohesie, hoek van interne wrywing, styfheid en weerstand modulus te ondersoek. Die gemaalde mineraal-aggregaat wat in hierdie ondersoek gebruik is, was verkry op verskeie areas van die R35, geleë naby Bethal. Die materiaal is ʼn mengsel van granulêre materiaal (van die bestaande kroonlaag en stutlaag van die pad) en herwonne asfalt (RA). Tydens die mengontwerp fase is twee tipes bitumen gebruik naamlik bitumenemulsie en skuimbitumen in hoeveelhede van 2%, 2.4% en 2.8%. Twee tipes aktiewe vulstof (hoeveelhede van onderskeidelik 1% en 2%) was saam met elk van die verskeie bitumen-hoeveelhede gebruik. Proefstukke van elk van hierdie mengsel kombinasies is onder beide nat en droë kondisies getoets. Tydens die tweede fase, is slegs die optimum binder inhoud (2.4%) gebruik vir beide emulsie- en skuimbitumen, gekombineer met 1% en 2% aktiewe vulstof. Proefstukke was getoets by ʼn reeks van verskillende digthede en versadigingvlakke. Die buigsaamheid was ondersoek deur middel van breek-energie, vervorming en die verplasing by breekpunt. ʼn Analise van variasie (ANOVA) is uitgevoer op die toetsdata om sodoende die te evalueer of die veranderlikes beduidend is ten opsigte van buigsaamheid. Daar is gevind dat die buigsaamheideienskap sensitief is vir beide bitumen en sement inhoud. Met assessering van die gekombineerde effek en betekenis van die veranderlikes op die buigsaamheid van die mengsels, is daar gevind dat die hoogste beduidende veranderlike t.o.v breek-energie die sement inhoud is, gevolg deur die bitumeninhoud, tipe behandeling en laastens die toetskondisie. Die orde van belangrikheid verskil vir die ander twee parameters (verplasing en vervorming by breekpunt). Daar is ook gevind dat die gekombineerde effek van sommige veranderlikes (sement inhoud en toets kondisie, tipe behandeling en sement inhoud tesame met bitumen inhoud) ook beduidend was t.o.v breek-energie en vervorming by breekpunt. Vanuit die ITS en UCS toetse was daar ʼn toename in sterkte waargeneem soos die sementinhoud toeneem. Aan die anderkant, het ʼn toename in bitumeninhoud ‘n afname in sterkte veroorsaak. Die statistiese analise van ITS en UCS resultate, toon dat die grootste beduidende onafhanklike t.o.v ITS waardes ook die sement inhoud was, gevolg deur toets kondisies die grootste effek, bitumen inhoud en die tipe behandeling. Die gekombineerde effek van sementinhoud en bitumeninhoud, was betekenisvol vir beide ITS en UCS. Drie-assige triaksiaaltoetse was uitgevoer om die gedragseienskappe van die mengsels te evalueer. Daar is gevind dat die toename in sement inhoud, die skuif sterkte van die materiaal grootliks verbeter. By ʼn konstante sementinhoud, wys toetsresultate van proefstukke wat getoets is by lae digthede en hoë vlakke van versadiging, lae skuif sterkte. Die Mr – θ model was gebruik om die veerkragsmodulus van die mengsels te moduleer en die modelkoëffisiënte is gebruik om die effek van eksperimentele veranderlikes op die weerstand modulus te evalueer. Met toename in die omhullende spanning is ‘n toename in die veerkragsmodulus waargeneem, wat bevestig dat die gedrag van bitumen gestabiliseerde materiale spannings afhanklik is. ʼn Toename in die sement en relatiewe digtheid het ʼn merkwaardige toename in die veerkragsmodulus tot gevolg gehad, terwyl die teenoorgestelde waargeneem is met toename in versadigingsvlakke. Buiten die ingenieurseienskap en meganiese toetsfaktore, is ander faktore (soos die trekspanning verhouding) bereken om die vogsensitiwiteit van die mengsels te evalueer. Mengsels met laer sement inhoud het groter verswakking ervaar met blootstelling aan water. Bitumenemulsie proefstukke toon beter weerstand teen water as skuimbitumen. Vergelyking tussen versnelde en korttermyn nabehandelingsprosedure van proefstukke, toon hoër ITS en UCS waardes vir die versnelde nabehandelingsprosedure prosedure. Buigsaamheid is ‘n belangrike eienskap van bitumen in padkonstruksie materiale (insluitend bitumen gestabiliseerde materiale), maar word moeilik gemeet. Alhoewel verplasing/vervorming by breekpunt en breek energie, bepaal vanaf ITS en UCS, ‘n indikasie toon van die hooffaktore (binder en sement) wat buigsaamheid van bitumen gestabiliseerde materiaal beïnvloed, word meer akkurate toetse benodig om die eienskap te ondersoek.

Thesis (MScEng)--Stellenbosch University, 2014. / ENGLISH ABSTRACT: Surface seals are widely used in South Africa. There are a number of reasons which include affordability, versatility and durability. There are, however, in some cases problems with stone loss that can lead to a shortened lifespan of the pavement. The loss of aggregate chippings in surface seals poses a major problem in the seal pavement industry. This study aims to identify the influencing factors that lead to these adhesive failures as well as to find optimum combinations of binders and aggregates at various conditions. Various binders commonly used in South African surface seal construction will be tested using the Bitumen Bond Strength (BBS) test method. The binders used in the study include 80/100 penetration grade bitumen, elastomer modified bitumen, bitumen rubber, elastomer modified emulsion and cationic rapid setting emulsion. Aggregates used in the study include dolerite, granite and quartzite. The test samples were cured and tested at two temperatures, 15 °C and 35 °C. The samples were also cured for 2, 6 and 24 hours respectively. The study tackles a wide range of variables in order to obtain a good understanding of adhesion properties of surface seals used in South Africa. Tests were repeated at least once to ensure repeatability and in some cases up to four repeats were performed. The loading rate at which the tests were performed had a significant influence on the BBS results. This rate varied which complicated the process of comparing the results. It was therefore decided to unify the loading rates. The BBS results exposed the difference between hot applied binders and emulsions. The former having significant stronger adhesion properties. It was also confirmed by the results that temperature plays a key role in the BBS results due to the visco-elastic properties of bitumen. These influences will be discussed along with others such as aggregate types and curing times. The type of failure is also discussed. Failure can either be adhesive or cohesive, the former being a failure between the aggregate and the binder while the later refers to a failure in the binder itself. The results of other students will also be discussed and compared to the results of this study. These include results of predecessors that tested emulsions as well as results from tests done on fractured aggregate surfaces and precoated aggregates. This study showed very similar results as these from other students, except for tests done with emulsions. It was discovered that the method of curing of the emulsions must be adapted to ensure proper curing of the emulsions. It was found that aggregates did not influence the BBS properties to the same extent as temperature and binder application type. The BBS results of hot applied binders also did not significantly increase as the curing time increased, but the results of emulsions showed some increase. However, the emulsions needed more time to cure properly. / AFRIKAANSE OPSOMMING: Oppervlak seëls word algemeen gebruik in Suid-Afrika. Daar is verskeie redes hiervoor waaronder bekostigbaarheid,veelsydigheid en duursaamheid. Daar is egter in sommige gevalle probleme met klipverlies wat kan lei tot n verkorte leeftyd. Hierdie klipverlies ontstaan as gevolg van verskeie redes of kombinasies daarvan. Die studie beoog om hierdie faktore wat die adhesie eienskappe beïnvloed te identifiseer sowel as om optimum kobinasies van bindmiddels en klipsoorte te bewerkstellig by verkeie kondisies. ‘n Verskeidenheid van bindmiddels wat algemeen in Suid-Afrika gebruik word, word in die studie getoets met die Bitumen Bond Sterkte (BBS) toets metode. Die bindmiddels wat in die studie gebruik word sluit 80/100 penetrasie graad bitumen, elastomeer gemodifiseerde bitumen, bitumen rubber, elastomeer gemodifiseerde emulsie en kationiese snel settende emulsie. Die klipsoorte wat vir die studie gebruikword is doleriet, graniet en kwartsiet. Hierdie gesteentes word algemeen in die praktyk gebruik. Die toets monsters word ook by twee temperature gekuur en getoets. Hierdie temperature is 15 °C en 35 °C. Die toets monsters word ook onderskeidelik vir 2, 6 en 24 uur gekuur. Die studie ondersoek 'n wye verskeidenheid van veranderlikes om sodoende 'n goeie begrip van adhesie eienskappe van die oppervlak seëls wat in Suid-Afrika gebruik word te verkry. Elke toets was ten minste een maal herhaal om herhaalbaarheid te verseker. Sommige toetse was tot 4 keer herhaal. Die belasting tempo van die toetse het ‘n beduidende uitwerking op die BBS resultate as gevolg van die visko-elastiese eienskappe van bitumen. Hierdie tempo het gewissel en dit moeilik gemaak om die resultate te vergelyk. Daarom was daar besluit om die tempo van die toetse te verander na ‘n gelykvormige tempo. Daar was ‘n duidelike verskil in BBS resultate van die warm toegepaste bindmiddels en die emulsies. Die warm bindmiddels het baie hoër BBS resultate gelwer. Dit was ook bevestig in die resultate dat temperatuur ‘n beduidende rol speel in die BBS. Hierdie invloede sal bespreek word tesame met ander, soos klipsoorte en kuring tye. Die tipe versaking word ook bespreek. Versaking kan plaasvind as gevolg van adhesie of cohesie, waar adhesie versaking 'n versaking is tussen die klip en die bindmiddel terwyl cohesie versaking verwys na 'n versaking in die bindmiddel self. Die uitslae van die ander studente sal ook bespreek word en vergelyking word met die resultate van hierdie studie. Dit sluit die resultate van voorgangers in wat emulsies getoets het sowel as die resultate van toetse wat gedoen is op gebreekte klipoppervlaktes en bitumen behandelde klippe. Hierdie studie het baie soortgelyke resultate getoon as dié van ander studente, behalwe vir die toetse wat gedoen was met emulsies. Daar is vasgestel dat die metode van kuring van die emulsies moet aangepas word om behoorlike kuring van die emulsies te verseker. Daar is ook gevind dat klipsoorte nie die BBS eienskappe in dieselfde mate as temperatuur en bindmiddel toepassingstipe beïnvloed het nie. Die BBS resultate van warm aangewende bindmiddels het ook nie aansienlik verhoog soos die kuringstyd toegeneem het nie, maar die resultate van emulsies het wel 'n toename getoon. Die emulsies het wel meer tyd nodig gehad om behoorlik te kuur.