The objective of this study was to investigate, both experimentally and analytically, the stresses and deformations in angle-ply composite tubes subjected to axisymmetric thermal loading. For the theoretical portion, a generalized plane strain elasticity analysis was developed. The analysis included mechanical and thermal loading and temperature-dependent material properties. Using the elasticity analysis and a temperature range of 116 K to 450 K, stress levels were found to be high for the specific designs considered, compared to material failure levels. In addition, the use of temperature-dependent material properties was found to have a significant effect on the predicted stresses and deformations. The elasticity analysis was also used to study the effect of including a thin metallic coating on a graphite-epoxy tube. The stresses in the coatings were found to be quite high, exceeding the yield stress of aluminum. An important finding in the analytical studies was the fact that even tubes with a balanced-symmetric lamination sequence exhibited shear deformation or twist. The radial location of an off-axis ply was found to influence its effect on the overall torsional tube response. For the experimental portion, an apparatus was developed to measure torsional and axial response in the temperature range of 140 K to 360 K. Eighteen specimens were tested, combining three material systems, eight lamination sequences, and three off-axis ply orientation angles. For the twist response, agreement between analysis and experiment was found to be good. The axial response of the tubes tested was found to be greater than predicted by a factor of three. As a result of the study, it is recommended that the thermally-induced axial deformations be investigated further, both experimentally and analytically. / Master of Science

The need for sensors demonstrating both high sensitivity and electromagnetic noise immunity has prompted the development of sensing systems based on optical fiber technology. This presentation opens with a short review of fiber optic sensing methods, including a discussion of several devices developed in prominent laboratories. The theoretical and empirical results of a particular technique of distributed pressure sensing appear next. This sensing approach, aimed towards the nondestructive testing of graphite/epoxy composite structures, relies on optical time - domain reflectometry in imbedded optical fibers. The method is investigated primarily in terms of its sensitivity and its effect on the mechanical integrity of the host composite. The work concludes with a discussion of results and ideas relating to microbending sensor research, as well as the design of several novel sensing devices. / M.S.

An experimental analysis of specimens taken from a thick, filament-wound composite material pressure vessel (cylinder) was performed by testing tensile coupons with various semi-elliptical surface notches. The strength of specimens with small notches was found to be notch insensitive. The strength of specimens with larger notches depended on the size of the notch. The fracture toughness of the laminate was found by applying a general fracture-toughness parameter approach. Using this value, several approaches were employed to predict failure loads. The accuracy of the approaches depended on the size of the notches. In general, the linear-elastic fracture mechanics method overpredicted the failure strength of specimens with intermediate sized notches, but predicted failure strength accurately for specimens with large notches. A strength of materials approach accurately predicted notched strength only for specimens with small notches. Notched strength was more accurately predicted for all notch sizes using an empirical approach, with the notch area used to predict failure instead of the notch depth, which was used in the linear-elastic fracture mechanics and strength of materials approaches. / M.S.

This thesis demonstrates the use of fiber optic methods for nondestructive testing of composite materials and aluminum specimens using the acousto-ultrasound approach. A noncontact method using a hybrid interferometer is devised for measuring absolute surface acoustic wave (SAW) amplitudes. The J1..J4 spectrum analysis technique is used for calibrating the piezoelectric transducer cylinder (PZT) and JO/J2 spectrum analysis technique is used for demodulating the SAW signal from the interferometer. An extrinsic Fabry-Perot interferometric (EFPI) sensor is utilized for sensing acoustic emission, measuring speed and attenuation in aluminum and composite specimens. A broadband preamplifier is designed for amplifying signals from the EFPI sensor. Theoretical and practical minimum detectable air gap change of an EFPI sensor are calculated for the system. The directional sensitivity of the EFPI sensor to SAW is studied. / Master of Science

Results of an experimental and analytical study of the nonlinear response and failure characteristics of internally pressurized 4- to 16-ply-thick graphite-epoxy cylindrical panels are presented. Specimens with clamped boundaries simulating the skin between two frames and two stringers of a typical transport fuselage were tested to failure. Failure results of aluminum specimens are compared with the graphite-epoxy test results. The specimens failed at their edges where the local bending gradients and interlaminar stresses are maximum. STAGS nonlinear two-dimensional shell analysis computer code results are used to identify regions of the panels where the response is independent of the axial coordinate. A geometrically nonlinear one-dimensional cylindrical panel analysis was derived and used to determine panel response and interlaminar stresses. Inclusion of the geometric nonlinearity was essential for accurate prediction of panel response. Measurements of panel radius and edge circumferential displacements associated with specimen slipping were also required in the one-dimensional analysis for good correlation between analytical and experimental results. Some panels failed with significant damage in the form of tensile fiber breaks and ply delaminations preceding the ultimate pressure. Other panels failed suddenly without any apparent damage preceding the ultimate pressure. The failure usually occurred along one edge of the panel leaving the other edge intact. The damage on the panel surfaces and through-the-thickness were examined to determine the failure characteristics of the panels. Various failure criteria were applied to the stresses predicted from the one-dimensional analysis. The maximum stress failure criterion applied to the predicted tensile stress in the fiber direction agreed best with the experimentally determined first damage pressures. Results indicate that all panels tested would support applied internal pressures well above fuselage proof pressures. / Ph. D.

DC resistance and AC conductance and capacitance have been measured under various conditions in an effort to electrically characterize and make electrical-mechanical correlations for 15 carbon black filled rubber samples. Resistance, conductance and capacitance have been monitored as functions of uniaxial compressive stress, time, temperature, and mechanical and thermal history. Capacitance and conductance have also been monitored as functions of frequency under various degrees of compressive loading and before and after specific heat treatments. A direct relationship has been found between sample • conductance and capacitance under any thermal and/or mechanical condition. This is in agreement with previous theories of conduction network formation and percolation. Various conduction mechanisms have been enumerated and an equivalent circuit of a network of lumped R-C "microelements'' has been qualitatively described. Stress, relaxation, frequency, and temperature dependences of the macroscopic parameters measured ( conductivity and capacitance) are discussed in terms of this model. / M.S.

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior / O emprego de materiais compósitos de matriz polimérica como reparo e reforço em estruturas nas indústrias do petróleo tem se tornado uma prática industrial comum. O uso destes reforços compreende desde o recobrimento de superfícies com defeitos, passantes ou não, até o reforço estrutural. Na última década, muitos estudos foram feitos para o desenvolvimento de uma metodologia alternativa para reforço e reparo de dutos com materiais compósitos. Recentemente, em 2006, o sistema ISO de normas técnicas apresentou a primeira especificação técnica de "Reparo em Compósitos para dutos das indústrias de Petróleo, Petroquímica e de Gás Natural Qualificação, projeto, instalação, testes e inspeção" ISO/PDTS 24817. O presente trabalho tem como objetivo o desenvolvimento de um sistema de reparo, utilizando materiais compósitos de matriz polimérica para o reparo e reforço estrutural de dutos e tubulações industriais, em conformidade com a Norma ISO 24817:2006. Foram desenvolvidos procedimentos para a confecção de corpos de prova destinados a ensaios mecânicos, e para aplicação do sistema de reparo. O sistema de reparo é destinado a defeitos tais como perda de espessura, amassamentos e danos transpassantes. Foi construída, em paralelo, toda a infraestrutura para a montagem de um laboratório destinado ao estudo de materiais compósitos, no Laboratório de Adesão e Aderência. São apresentados resultados de parte dos ensaios mecânicos necessários, comparação dos resultados obtidos com modelos teóricos e testes hidrostáticos. / The use of polymer matrix composites to repair and strengthen structures in the oil industry has become a common industry practice. The use of these reinforcements extends from covering surfaces with defects, through wall or not, to structural reinforcement. In the last decade, many studies have been done to develop an alternative approach to the strengthening and repairing of pipelines with composite materials. Recently, in 2006, the ISO system of technical standards presented the document technical support "Petroleum, petrochemical and natural gas industries Composite repairs for pipework Qualification, design, installation, testing and inspection" ISO/PDTS 24817. This study aims to develop a repair system using polymer matrix composite materials for repair and reinforcement of piping and pipelines in accordance with ISO 24817:2006. Procedures where developed for the confection of test specimens for mechanical testing, and application of the repair. The system is intended to repair defects such as thickness loss, gouges, and damage through wall or not. In parallel, an entire infrastructure was built for the conception of a laboratory for the study of composite materials at the Laboratory of Adhesion and Adherence. Here are presented the results of the required mechanical tests, the comparison results with theoretical models, and the hydrostatic testing.

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior / O emprego de materiais compósitos de matriz polimérica como reparo e reforço em estruturas nas indústrias do petróleo tem se tornado uma prática industrial comum. O uso destes reforços compreende desde o recobrimento de superfícies com defeitos, passantes ou não, até o reforço estrutural. Na última década, muitos estudos foram feitos para o desenvolvimento de uma metodologia alternativa para reforço e reparo de dutos com materiais compósitos. Recentemente, em 2006, o sistema ISO de normas técnicas apresentou a primeira especificação técnica de "Reparo em Compósitos para dutos das indústrias de Petróleo, Petroquímica e de Gás Natural Qualificação, projeto, instalação, testes e inspeção" ISO/PDTS 24817. O presente trabalho tem como objetivo o desenvolvimento de um sistema de reparo, utilizando materiais compósitos de matriz polimérica para o reparo e reforço estrutural de dutos e tubulações industriais, em conformidade com a Norma ISO 24817:2006. Foram desenvolvidos procedimentos para a confecção de corpos de prova destinados a ensaios mecânicos, e para aplicação do sistema de reparo. O sistema de reparo é destinado a defeitos tais como perda de espessura, amassamentos e danos transpassantes. Foi construída, em paralelo, toda a infraestrutura para a montagem de um laboratório destinado ao estudo de materiais compósitos, no Laboratório de Adesão e Aderência. São apresentados resultados de parte dos ensaios mecânicos necessários, comparação dos resultados obtidos com modelos teóricos e testes hidrostáticos. / The use of polymer matrix composites to repair and strengthen structures in the oil industry has become a common industry practice. The use of these reinforcements extends from covering surfaces with defects, through wall or not, to structural reinforcement. In the last decade, many studies have been done to develop an alternative approach to the strengthening and repairing of pipelines with composite materials. Recently, in 2006, the ISO system of technical standards presented the document technical support "Petroleum, petrochemical and natural gas industries Composite repairs for pipework Qualification, design, installation, testing and inspection" ISO/PDTS 24817. This study aims to develop a repair system using polymer matrix composite materials for repair and reinforcement of piping and pipelines in accordance with ISO 24817:2006. Procedures where developed for the confection of test specimens for mechanical testing, and application of the repair. The system is intended to repair defects such as thickness loss, gouges, and damage through wall or not. In parallel, an entire infrastructure was built for the conception of a laboratory for the study of composite materials at the Laboratory of Adhesion and Adherence. Here are presented the results of the required mechanical tests, the comparison results with theoretical models, and the hydrostatic testing.