Thesis (M.S.)--University of Wisconsin--Madison, 1994. / Typescript. eContent provider-neutral record in process. Description based on print version record. Includes bibliographical references (leaves 48-50).

Thesis (Ph. D.)--University of Wisconsin--Madison, 1968. / Typescript. Vita. eContent provider-neutral record in process. Description based on print version record. Includes bibliographical references.

Thesis (Ph. D.)--Washington State University, December 2006. / Includes bibliographical references.

No description available.

Photocopy of typescript. / Digitized by Kansas Correctional Industries

LD2668 .T4 1962 K34

A consumer and a trained descriptive panel was utilized to determine liking ratings and flavor profiles, respectively, for commercial brands of pre-stirred yogurt. Once the consumer and descriptive panel data was collected, the data was combined to determine the interrelationship of these two sets of data and to determine the conditions necessary to optimize the sensory characteristics of commercial yogurt. This study was broken down into two parts: (1) evaluation by a 90 to 182 member consumer panel and an 11 member descriptive panel for 14 strawberry and 6 lemon yogurt brands, and (2) correlation of the sensory measures of sweetness and sourness, and analytical measures of sugars and acids for 14 strawberry, 12 raspberry, 6 lemon, and 17 plain yogurt brands. Large sensory differences were found between yogurts for both flavors (strawberry and lemon) by both panels. Correlation and principal component analysis (PCA) indicated that two distinct groups of descriptors contributed to the liking of the yogurts: one associated with the fruity and sweetness characteristics, and the other related to the plain yogurt and sourness descriptors. Consumers based their overall liking ratings on fruit flavor, sweetness, sourness, and a balance of sweetness/sourness liking. Males and females rated samples differently by as much as one full scale value on a 9-pt. hedonic scale. Use of PCA to relate the two panels revealed that high consumer acceptance corresponded with the PC loaded with fruity and sweet characteristics while lower consumer acceptability was noted with high loadings on PC2 which was comprised of plain yogurt, acetaldehyde, and sourness descriptors. The results from the first part of the study indicate that to produce a highly acceptable yogurt, processors should strive to provide a balance between sweetness and sourness and provide enough fruit flavor to mask plain yogurt characteristics. In the second part of this study, titratable acidity and pH were measured for all the yogurts, while sugars were measured by HPLC only for the fruit flavored yogurts. Consumer overall liking was significantly correlated with sweetness intensity, sweetness:sourness (sw:so) ratio, and the summed impact of sweetness and sourness from the trained panel for strawberry and raspberry yogurt. No correlations between analytical measures and overall liking were found for any of the yogurts. A sw:so ratio greater than 1.0 for strawberry, and .8 for raspberry and lemon appeared necessary for high consumer acceptance. Generally, it was found that the sweeter the yogurt, the higher the consumer acceptance of fruit flavored yogurt. No relationships were found for any sensory and analytical measures for predicting the overall liking of plain yogurt. However, the best predictors of consumer liking of fruit flavored yogurt were the descriptive panel ratings. / Graduation date: 1991

Numerous attempts have been made to identify the flavor compounds in Blue cheese, however, duplication of Blue cheese flavor has not yet been accomplished. Therefore, it was desirable to make a qualitative and quantitative investigation of Blue cheese flavor compounds and to study the effect of certain microorganisms on Blue cheese flavor. The aroma fraction of Blue cheese was isolated by centrifugation of the cheese and molecular distillation of the recovered fat. The volatiles were separated by gas chromatography on packed columns containing polar and nonpolar phases and by temperature programmed capillary column gas chromatography. Relative retention time data and fast scan mass spectral analysis of the capillary column effluent were used to identify compounds in the aroma fraction. Compounds positively identified were as follows: 2-pentanone, 2-hexanone, 2-heptanone, 2-octanone, 2-nonanone, 2-decanone, 2-undecanone, 2-tridecanone, 2-propanol, 2-pentanol, 2-heptanol, 2-octanol, 2-nonanol, methyl butanoate, methyl hexanote, methyl octanoate, methyl decanoate, methyl dodecanoate, ethyl formate, ethyl acetate, ethyl butanoate, ethyl hexanoate, ethyl octanoate, ethyl decanoate, ethanal, 3-methyl butanal, 2-methyl butanol, 3-methyl butanol, 1-pentanol, benzene, and toluene. Tentatively identified compounds included acetone, delta-octalactone, delta-decalactone, methyl acetate, isopropyl hexanoate, 3-methylbutyl butanoate, pentyl hexanoate, ethyl-2-methylnonanoate, isopropyl decanoate, furfural, 2-methyl propanal, methanol, ethanol, 2-phenylethanol, cresyl methyl ether, dimethylcyclohexane, diacetyl, methyl mercaptan, and hydrogen sulfide. A combination of liquid-liquid column chromatography and gas-liquid chromatography was utilized to quantitate the major free fatty acids in Blue and Roquefort cheese samples. The average concentration (mg acid/kg cheese) in three Blue cheese samples was as follows: 2:0, 826; 4:0, 1, 448; 6:0, 909; 8:0, 771; 10:0, 1,318; 12:0, 1,588; 14:0, 5,856; 16:0, 12,789; 18:0, 4,243; 18:1, 12,455; 18:2, 1,072; 18:3, 987. Roquefort cheese was found to be proportionately more abundant in 8:0 and 10:0 acids and low in 4:0 acid compared to Blue cheese. No formic, propionic, or isovaleric acid was detected in any of the cheeses tested. A quantitative procedure involving adsorption chromatography, liquid-liquid chromatography and absorption spectrophotometry was used to isolate and measure the concentration of the C₃, C₅, C₇, C₉, and C₁₁ methyl ketones in the fat of Blue and Roquefort cheese. The average methyl ketone concentration (micromoles ketone/10 g cheese fat) of five Blue cheese samples was as follows: acetone, 1.7; 2-pentanone, 5.9; 2-heptanone, 11.2; 2-nonanone, 9.3; 2-undecanone, 2. 4. Considerable variation in ketone concentration was noted between samples, but no consistent differences were observed between Blue and Roquefort cheese. One Roquefort sample contained no acetone. The annount of ketone formed during cheese curing does not depend directly on the amount of available fatty acid precursor. There appears to be a selective conversion of the 8:0, and to a lesser extent the 6:0 and 10:0, fatty acids to methyl ketones by the Penicillium roqueforti spores. The concentration of the C₅, C₇, and C₉ secondary alcohols was determined in the same cheeses used for ketone analysis. The previously measured ketones acted as internal standards and facilitated a semi-quantitative calculation of alcohol concentrations from peak areas of gas chrorriatograms. The average alcohol concentration (micromoles alcohol/10 g cheese fat) in five Blue cheese samples was as follows: 2-pentanol, 0. 3; 2-heptanol, 2. 1; 2-nonanol, 0. 8. The alcohols were present in approximately the same ratios as their methyl ketone analogs, but at much lower concentrations. A synthetic Blue cheese flavor was prepared using a blend of butterfat, dry curd cottage cheese, cream, and salt as a base. The most typical flavor was obtained using the following' compounds: the 2:0, 4:0, 6:0, and 8:0 fatty acids at two-thirds the average concentration found in cheese; twice the average concentration of the C₃, C₅, C₇, C₉, and C₁₁ methyl ketones and C₅, C₇, and C₉ secondary alcohols found in cheese: 2.0 mg/kg of base of 2-phenylethanol; 1.5 mg/kg of base of ethyl butanoate; 6.0 mg/kg of base of both methyl hexanoate and methyl octanoate. Incorporation of higher acids caused a soapy flavor. The presence of 2-phenylethanol and the esters was judged as very important in duplicating Blue cheese flavor. The mycelia of Penicillium roqueforti appear to be more active in the reduction of methyl ketones to secondary alcohols than the spores. Yeasts associated with Blue cheese are capable of reducing methyl ketones to secondary alcohols. Yeasts also may play a role in Blue cheese flavor by producing ethanol and other alcohols and certain esters. / Graduation date: 1966

No description available.

Typescript (photocopy). / Digitized by Kansas Correctional Industries