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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Structural and dielectric properties of V2O5 addition on Bi5Ti3FeO15 ceramic matrix / Estudo das propriedades dielÃtricas e estruturais do Bi5Ti3FeO15 adicionado de V2O5

Francisco Andrà Andrade de Aguiar 08 January 2016 (has links)
O Bi5Ti3FeO15 foi sintetizado pelo mÃtodo de ReaÃÃo no Estado SÃlido (RES) e posteriormente adicionado de V2O5 (PentÃxido de VanÃdio) objetivando melhorar suas propriedades dielÃtricas. Para as anÃlises estruturais foram utilizadas as seguintes tÃcnicas: DifraÃÃo de Raios-X (DRX), Microscopia EletrÃnica de Varredura (MEV), Espectroscopia de DispersÃo de Energia de Raios-X (EDS), Espectroscopia Raman e Infravermelho (IV). Para o estudo das propriedades dielÃtricas do material em radiofrequÃncia e em microondas, foram empregadas, respectivamente, a Espectroscopia de ImpedÃncia (EI) e o mÃtodo de Hakki e Coleman. A tÃcnica de DRX foi utilizada para identificar a fase BFT pura, bem como as duas novas fases originadas a partir da adiÃÃo de V2O5: Bi4V1.5Fe0.5O10.5 e Bi2Ti2O7. As alteraÃÃes na morfologia dos grÃos e a resposta dielÃtrica foram atribuÃdas à presenÃa destas fases secundÃrias. Em radiofrequÃncia verificou-se que a adiÃÃo de V2O5 aumentou a permissividade dielÃtrica e reduziu os valores de tangente de perda, resultados semelhantes aos obtidos em microondas. Ressonadores DielÃtricos foram fabricados como um protÃtipo para antena monopolo. Os valores de frequÃncia de funcionamento da antena variaram entre 2,4 GHz e 3,1 GHz. Jà os valores de coeficiente de temperatura da frequÃncia ressonante (f) variaram de -330 a -192 ppm/ÂC. Assim sendo, a cerÃmica BFT adicionada de V2O5, pode ser utilizada em dispositivos de microondas, como telefones mÃveis, por exemplo. / The Bi5Ti3FeO15 (BFT) was synthesized by the solid state reaction method (SLR) and then added by V2O5 (vanadium pentoxide) to improve its dielectric properties. For the structural analyses the following technics were used: X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), Raman and infrared spectroscopy. For the dielectric propeties of the material at radiofrequency and microwave ranges, impedance spectroscopy (IS) and the Hakki-Coleman methods were used respectively. The XRD technique was used to identify the BFT phase as well as the two new ones (Bi4V1.5Fe0.5O10.5 and Bi2Ti2O7). Changes in the grain morphology and the dielectric response were assigned due to the presence of these secondary phases. The V2O5 addition increased the dielectric permittivity and reduced the loss tangent values at radiofrequency range; similar results were obtained at microwave. The Dielectric resonators (DR) were fabricated as a prototype for monopole antenna. The antenna operating frequency (2.4 - 3.1 GHz) and temperature coefficient of resonance frequency (τf) (from -330 to -192 ppm/ÂC) changed as a function of V2O5 concentration in the DR. Thus, BFT ceramics added by V2O5 are good candidates to be used for microwave devices as cell mobile phones, for example.

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