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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Dislocation Density-Based Finite Element Method Modeling of Ultrasonic Consolidation

Pal, Deepankar 01 August 2011 (has links)
A dislocation density-based constitutive model has been developed and implemented into a crystal plasticity quasi-static finite element framework. This approach captures the statistical evolution of dislocation structures and grain fragmentation at the bonding interface when sufficient boundary conditions pertaining to the Ultrasonic Consolidation (UC) process are prescribed. The hardening is incorporated using statistically stored and geometrically necessary dislocation densities (SSDs and GNDs), which are dislocation analogs of isotropic and kinematic hardening, respectively. Since the macroscopic global boundary conditions during UC involves cyclic sinosuidal simple shear loading along with constant normal pressure, the cross slip mechanism has been included in the evolution equation for SSDs. The inclusion of cross slip promotes slip irreversibility, dislocation storage, and hence, cyclic hardening during the UC. The GND considers strain-gradient and thus renders the model size-dependent. The model is calibrated using experimental data from published refereed literature for simple shear deformation of single crystalline pure aluminum alloy and uniaxial tension of polycrystalline Aluminum 3003-H18 alloy. The model also incorporates various local and global effects such as (1) friction, (2) thermal softening, (3) acoustic softening, (4) surface texture of the sonotrode and initial mating surfaces, and (6) presence of oxide-scale at the mating surfaces, which further contribute significantly specifically to the grain substructure evolution at the interface and to the anisotropic bulk deformation away from the interface during UC in general. The model results have been predicted for Al-3003 alloy undergoing UC. A good agreement between the experimental and simulated results has been observed for the evolution of linear weld density and anisotropic global strengths macroscopically. Similarly, microscopic observations such as embrittlement due to grain substructure evolution at the UC interface have been also demonstrated by the simulation. In conclusion, the model was able to predict the effects of macroscopic global boundary conditions on bond quality. It has been found that the normal pressure enhances good bonding characteristics at the interface, though beyond a certain magnitude enhances dynamic failure. Similarly, lower oscillation amplitudes result in a lower rate of gap closure, whereas higher oscillation amplitude results in an enhanced rate of gap relaxation at the interface. Henceforth, good bonding characteristics between the constituent foils are found at an optimum oscillation amplitude. A similar analogy is also true for weld speed where the longitudinal locations behind the sonotrode rip open when higher weld speeds are implemented in the UC machine, leading to lower linear weld density and poor bonding characteristics.
2

Využití techniky orientovaných fólií v TEM / Application of Technique of Oriented Foils in TEM

Buček, Petr January 2009 (has links)
The master’s thesis is focused on the application of the technique of oriented foils in transmission electron microscopy. Dislocation structures were identified by this technique in both phases of polycrystalline austenitic-ferritic stainless steel SAF 2507 formed during low cycle fatigue at two plastic strain amplitudes ap. In individual grains the stress axis and the Schmid factors of active slip systems were determined. In austenitic grains, the planar structures were determined at both ap. In ferritic grains, the dislocation arrangement was different for the two observed ap. Individual screw dislocations and pile-up´s of edge dislocations were found at low ap = 1x10-4. Mixture of vein and wall dislocation structures were formed at high ap = 2x10-3. Observed dislocation structures were discussed in relation with the cyclic plastic response of the duplex stainless steel.
3

Microstructure Evolution in 304L Stainless Steel Subjected to Hot Torsion at Elevated Temperature

Lu, Jian 19 September 2011 (has links) (PDF)
The current study focus on investigating a relationship between processing variables and microstructure evolution mechanism in 304L stainless steel subjected to hot torsion. The Gleeble 3800 with Mobile Torsion Unit (MTU) is utilized in the current study to conduct hot torsion test of 304L stainless steel. Samples are rotated at 1100℃ in the shear strain rate range of 0.02s-1 to 4.70s-1 and the shear strain range of 0.5 to 4. Orientation imaging microscopy (OIM) technique is used to collect and analyze the microstructure. At low strains (≤1) and strain rate (0.02s-1), average grain size remains relatively constant, but the lengths of DSs and LABs increase within grains. These are characteristics of the dynamic recovery (DRV). With increasing strain and strain rate, the lengths of DSs, LABs and HABs increase, accompanied by the decrease of average grain size. Subgrains with HAB segments are observed. These are characteristics of continuous dynamic recrystallization (CDRX). At strain rates greater than or equal to 0.94s-1, the fraction of deformation texture is about 3 times higher than that of rotated cube texture. The average grain size increases relative to that at a strain rate of 0.20s-1, accompanied by the increase of twin length per area. This indicates that grain growth take place after CDRX. Sigma phase is not observed in the current study due to the lack of static recrystallization (SRX) and the higher cooling rate.

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