The work of previous writers on the origin and propagation of solar radio noise, and particularly the correlation with visual events is reviewed, and then the construction of the author's 300 Mc/s receiver described. With a view to the author's project, absorption of electromagnetic radiation in the solar corona is quantitatively discussed, and a method for determining the intensity without absorption of a radio burst is evolved. The main project involves briefly the discovery of any possible relationship between the magnitude of a visual flare and the corrected intensity of an associated radio burst as measured at 125 Mc/s. It is concluded that no definite relation exists, but from this consideration an approximate shape of the instantaneous frequency profile of outburst elements is obtained. An extension of the theory to isolated bursts enables us to predict both this bandshape, and the velocity of an exciting agency moving radially through the corona.

The literature on isolated bursts and possible mechanisms of origin has been critically reviewed, and observations point to a mechanism involving omission of electromagnetc radiation from plasma oscillations in the solar corona excited by outward travelling disturbances. Solar noise observations on 125 Mc./s. recorded at Rhodes University during the period November 26 1957 - February 6 1958 have been analysed by the author for isolated bursts, and these observations show the same general features reported by previous investigators. In interpretation of these records particular attention has been devoted to two aspects of isolated bursts; namely the preponderance on single frequency records of double-humped bursts, and the shape of isolated burst profiles. The authors suggests that a probable explanation of double-humped bursts observed on any frequency f is that the first hump represents omission at or near the level of zero refractive index for f radiation, and that the second hump corresponds to harmonic omission at the f/2 level. Source velocities may be calculated from the time delay between the peaks and an average value of 2 x 10⁴ km./sec. was obtained from an analysis of 21 double-humped bursts. This value is in very good agreement with that deduced by Wild (1950b) from the rate of frequency drift of peak intensity of isolated bursts. Simple isolated bursts had decay profiles which are approximatley exponential in shape, and this is usually interpreted in terms of the natural decay of plasma oscillations in the medium of origin. The author has verified that the exponential function is a good fit to the observed decay profiles, but shows that a relation of the form I - ¹/n (superscript) ⋉ t (where I is intensity and t is time) fits just as well. An alternative model is suggested which would lead to an exponential-like decay profile which is not determined by the natural decay of plasma oscillations. The work concludes with some suggestions for further research.

With the increase in the application of ultra-precision manufactured parts and the absence of much participation of researchers in ultra-high precision grinding of optical glasses which has a high rate of demand in the industries, it becomes imperative to garner a full understanding of the production of these precision optics using the above-listed technology. Single point inclined axes grinding configuration and Box-Behnken experimental design was developed and applied to the ultra-high precision grinding of BK7 glass. A high sampling acoustic emission monitoring system was implemented to monitor the process. The research tends to monitor the ultra-high precision grinding of BK7 glass using acoustic emission which has proven to be an effective sensing technique to monitor grinding processes. Response surface methodology was adopted to analyze the effect of the interaction between the machining parameters: feed, speed, depth of cut and the generated surface roughness. Furthermore, back propagation Artificial Neural Network was also implemented through careful feature extraction and selection process. The proposed models are aimed at creating a database guide to the ultra-high precision grinding of precision optics.

Experience shows that the noise and sound quality in vehicles are often a recurring criticism. The bodies of modern vehicles consist predominantly of thin sheets of metal. It is hard to prevent the excitation of bending vibrations and the subsequent emission of disturbing noise while driving. The noise spectrum in a car that can be heard by the driver is from ”latent roar” to ”chattering” noise of the body and engine. In automotive vehicles damped materials, especially plastics or materials made from sheet metal and surface damping treatments, are used. Those have high internal energy losses and damp sound oscillatory systems found in the body or interior of cars. A further advantage of such treated components is that they are applied to existing components working over wide temperature and frequency ranges. Many companies provide such ”sound-absorbing compounds”. The requirements for these damping materials are high temperature-resistance, water repellence, fuel and oil-resistance and good adhesion to the base material [17]. The acoustic properties, especially the damping of the plate vibrations through rubber are of interest. the question arises how can the damping coeficient of coated metal sheets can be measured and secondly, by how much the road noise is reduced when built-in sheets are coated with a known damped material. With the Oberst Bar Test Method (named after Dr. H. Oberst) the properties are determined of the internal damping materials that can be used to simulate mechanical constructions to determine damping of larger surfaces. This method describes a laboratory test procedure for measuring the mechanical properties of damped materials. A block diagram of the test system consisting of a damped material bonded to a vibrating cantilever steel bar is shown in figure 2.1. This method is useful for testing materials such as metals, enamels, ceramics, rubbers, plastics, reinforced epoxy matrices and wood. In addition to damping measurement, the test allows for the determination of the Young’s modulus E of the material. E is calculated from the resonance frequency of a given mode and from the physical constants of the bar. By associating the damping factor with the Young’s modulus, a complex quantity is defined which is called the Complex Modulus of Elasticity. Measurements of dynamic mechanical properties are also useful in the research on the molecular structure of materials.

The graduation theses is focused on problems of emission rights. The graduation theses is describing when and where has been firstly started talking about emission rights and why, what has been developement of emission rights prices on the stock markets since their implementation in 2005 and what was the impact on the financial statements. The main part of the gradiation theses is about financial reporting. There is described a few of possible methods how to enter it in the books with concrete examples each of them. There is not missing historically first sollution of the emission rights bookkeeping, interpretation IFRIC 3.

Transition metal dichalcogenides (TMDs) have displayed a host of novel physical phenomena, which opens-up promising future applications in electronics, optoelectronics, spintronics and valleytronics. However, the high defect density of 10¹² - 10¹³ cm-² in commercially available TMDs may hinder the observation of their intrinsic properties. In this thesis, the defect density of MoSe₂ and WSe₂ has been reduced by ~10x - 1000x using flux method. The reduced defect denstiy of MoSe₂ and WSe₂ enables to observe optical and electrical properties approaching their intrinsic properties.First of all, photocurrent measurements on the ultra-clean WSe₂ unveil the effect of point defects on photo-response. Substantial improvement of AC photocurrent in the ultra-clean WSe2 indicates that free carriers are likely to non-radiatively decay at atomic defects at room temperature. Then, time-resolved photoluminescence measurements on the ultra-clean MoSe₂ samples allow for direct determination of both the intrinsic (radiative) and defect-dependent (non-radiative) lifetimes of trions. In the cleanest MoSe₂, the trion quantum yield approaches unity. The long lifetime of 230 ps of trions allows direct observation of their diffusion, conclusively demonstrating that trions are free particles. Both the long radiative and non-radiative lifetime of trions can be attributed to Pauli blocking effects. Morover, transport measurements of ultra-clean WSe2 provide Hall mobility exceeding 10,000 cm²V-¹s-¹ and long mean free path over 200 nm, which are nearly three times higher than those in previous study. This improved mobility and mean free path in the ultra-clean WSe₂ indicate that the electrical properties have been limited by defect scattering. Finally, WSe₂ has been a decent platform to generate single photon emitters. However, the microscopic origin of the single photon emitter has been debated. From power- and gate-dependent photoluminescence of ultra-clean WSe₂, emerging defect bound excitons are observed, which is likely formed from the interaction between donor defects and excitons.

abstract: Acoustic emission (AE) signals have been widely employed for tracking material properties and structural characteristics. In this study, the aim is to analyze the AE signals gathered during a scanning probe lithography process to classify the known microstructure types and discover unknown surface microstructures/anomalies. To achieve this, a Hidden Markov Model is developed to consider the temporal dependency of the high-resolution AE data. Furthermore, the posterior classification probability and the negative likelihood score for microstructure classification and discovery are computed. Subsequently, a diagnostic procedure to identify the dominant AE frequencies that were used to track the microstructural characteristics is presented. In addition, machine learning methods such as KNN, Naive Bayes, and Logistic Regression classifiers are applied. Finally, the proposed approach applied to identify the surface microstructures of additively manufactured Ti-6Al-4V and show that it not only achieved a high classification accuracy (e.g., more than 90\%) but also correctly identified the microstructural anomalies that may be subjected to further investigation to discover new material phases/properties. / Dissertation/Thesis / Masters Thesis Statistics 2020

True-green wavelength emitters at 555 nm are currently dominated by III-V semiconductor-based inorganic materials. Nevertheless, due to high lattice- and thermal-mismatch, the overall power efficiency in this range tends to decline for high current density showing the so-called efficiency droop in the green region (“green gap”). In order to fill the research green gap, this thesis examines the low cost solution-processability of organometal halide perovskites, which presents a unique opportunity for light-emitting devices in the green-yellow region owing to their superior photophysic properties such as high photoluminescence quantum efficiency, small capture cross section of defect states as well as optical bandgap tunability across the visible light regime. Specifically, the mechanisms of radiative recombination in a CH3NH3PbBr3 hybrid perovskite material were investigated using low-temperature, power-dependent (77 K), temperature-dependent photoluminescence (PL) measurements. We noted three recombination peaks at 77K, one of which originated from bulk defect states, and other two from surface defect states. The latter were identified as bound-excitonic (BE) radiative transitions related to particle size inhomogeneity or grain size induced surface state in the sample. Both transitions led to PL spectra broadening as a result of concurrent blue- and red-shifts of these excitonic peaks. The blue-shift is most likely due to the Burstein-Moss (band filling) effect. Interestingly, the red-shift of the second excitonic peak becomes pronounced with increasing temperature leading to a true-green wavelength of 553 nm for CH3NH3PbBr3. On the other hand, red-shifted peak originates from the strong absorption in the second excitonic peak owed to the high density of surface states and carrier filling of these states due to the excitation from the first excitonic recombination. We also achieved amplified spontaneous emission around excitation threshold energy of 350 μJ/cm2 when optically pumped using 475 nm laser pulses, thus supporting the assignment of carrier absorption and re-excitation mentioned above. This dissertation work led to the following article: D. Priante, I. Dursun, M. S. Alias, D. Shi, V. A. Melnikov, T. K. Ng, O. F. Mohammed, O. M. Bakr, and B. S. Ooi, "The recombination mechanisms leading to amplified spontaneous emission at the true-green wavelength in CH3NH3PbBr3 perovskites", Applied Physics Letters, 106, 081902, 2015. DOI: 10.1063/1.4913463

Diploma thesis presents the description of laser induced breakdown spectroscopy (LIBS) analytical method. The possibility to decrease LIBS detection limits using double pulse LIBS (DP-LIBS) is also detailed. Properties of laser induced plasma (LIP) are discussed. Thesis describes the optimisation process of DP-LIBS setup at laser spectroscopy laboratory of Faculty of Mechanical Engineering, Brno University of Technology. Optimisation was carried out for detection of chrome in steel with respect to detection limits and ablation crater size. Optimised DP-LIBS setup is appropriate for mapping chrome distribution in steel samples.

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