No / The advances of the polymer melt flow-induced crystallization behaviour and its influence on mechanical properties of high density polyethylene (HDPE) in micron injection (MI) were studied in the present paper. Analysis of mechanical performance, including yield stress and elongation at break, for samples adopted from different regions in a molded plaque showed that a higher injection speed, a higher mold temperature and a longer cooling time could effectively enhance the yield stress but negatively promoted the ductility. Then, the mechanisms of such variation of mechanical performance and the factors affecting it were investigated by means of differential scanning calorimetry (DSC), scanning electron microscopy (SEM) and polarized light microscopy (PLM). The super high shear rate during cavity feeding in MI molding not only induced a typical three-layered structure but also developed a highly oriented fibrously morphological structure in the skin layer. However, such fully oriented morphology was much negative in the interlayer and even could not be observed in the core layer. The results from SEM and PLM observations indicated that the orientation morphology varied significantly through the plaque's cross-section and thickness of the each layer changed with the process parameters and geometric position, and finally led to variation of the mechanical performance.

The presented diploma thesis focuses on flow-induced vibrations of a tube. The main aim and benefit is the analysis of tube stiffness in contact with the other one and the following use of obtained values and characteristics in CFD simulations. The work can be divided into three parts. The first part is about the current state of knowledge of flow-induced vibrations. It introduces the basic mechanisms of vibration and methods for their suppression. The second part deals with the determination of stiffness of defined geometry tube including the collision with the other tube. The final part demonstrates and evaluates the application of obtained characteristics in CFD simulations.

Coronary artery disease (CAD) affects every fifth person in the world. The gold-standard treatment for CAD is stent implantation, however, the existing therapy is not sufficient due to many reasons. For instance, in-stent restenosis, biocompatibility, controlled degradation rate, protein adsorption, and adequate endothelialization are still the main concerns. In the last two decades, the field of stent technology has been grown rapidly and many new stent types and in vitro testing methods for stent characterization have been developed to minimize the aforementioned issues. In this vicinity, there are still many unaddressed issues: i) the quantitative analysis of corrosion is conducted with simpler samples made of stent material instead of stents, in most cases due to the absence of a mathematical model to calculate the entire stent surface area (ESSA); ii) in vitro stent testing in environments that are very far from actual physiological environments; iii) Evaluation of the influence of in-vitro test conditions on coated metallic stents; iv) absence of flow-induced shear stress (FISS) corrosion model, to mention a few. This thesis presents the novel ESSA model, the fluid dynamic experimental setup with the integration of various sensors and pH control, the influence of in vitro degradation behavior of the titanium oxynitride (TiOxNy) coated stainless steel stents and anodized AZ31 samples, and the FISS corrosion model. The results show some important contributions in this field, however, there is still a huge potential for the development of promising stent characterization solutions. / Die koronare Herzkrankheit (KHK) betrifft jeden fünften Menschen auf der Welt. Der Goldstandard bei der Behandlung von KHK ist die Stent-Implantation, doch die bestehende Therapie ist aus vielen Gründen nicht ausreichend. So sind beispielsweise die Restenose im Stent, die Biokompatibilität, die kontrollierte Abbaugeschwindigkeit, die Proteinadsorption und die angemessene Endothelialisierung nach wie vor die Hauptprobleme. In den letzten zwei Jahrzehnten hat sich die Stenttechnologie rasant weiterentwickelt, und es wurden viele neue Stenttypen und In-vitro-Testmethoden zur Stentcharakterisierung entwickelt, um die oben genannten Probleme zu minimieren. In dieser Umgebung gibt es noch viele ungelöste Probleme: i) die quantitative Analyse der Korrosion wird mit einfacheren Proben aus Stentmaterial anstelle von Stents durchgeführt, in den meisten Fällen aufgrund des Fehlens eines mathematischen Modells zur Berechnung der gesamten Stentoberfläche (ESSA); ii) In-vitro-Stent-Tests in Umgebungen, die sehr weit von der tatsächlichen physiologischen Umgebung entfernt sind; iii) Bewertung des Einflusses von In-vitro-Testbedingungen auf beschichtete metallische Stents; iv) Fehlen eines FISS-Korrosionsmodells (flow-induced shear stress), um nur einige zu nennen. In dieser Arbeit werden das neuartige ESSA-Modell, der strömungsdynamische Versuchsaufbau mit der Integration verschiedener Sensoren und pH-Kontrolle, der Einfluss des In-vitro-Degradationsverhaltens der mit Titanoxynitrid (TiOxNy) beschichteten Edelstahlstents und anodisierten AZ31-Proben sowie das FISS-Korrosionsmodell vorgestellt. Die Ergebnisse zeigen einige wichtige Beiträge in diesem Bereich, jedoch gibt es noch ein großes Potenzial für die Entwicklung von vielversprechenden Lösungen zur Charakterisierung von Stents.

The aim of the dissertation thesis is the control of the tube bundle on the cyclic fatigue caused by the flow past tube bundle. Fatigue due to flow is caused by flow-induced vibrations. Examined vibrations are caused by the mutual interaction of two phases (solid and liquid). The present work is focused mainly on the interaction of tube bundles with fluid. The current level of knowledge in this field allows to predict mainly static respectively quazi-static loading. These predictions are based on methods of comparing key vibration variables such as frequencies, amplitudes or speeds (see TEMA [1]). In this way, it is possible to determine quickly and relatively precisely the occurrence of a vibrational phenomenon, but it is not possible to quantitatively assess the effect of these vibrations on the damage of to the tube beam and to predict its lifespan, which would require the determination of the temperature field and the distribution of forces from the fluid on the beam. The aim of the work is to evaluate the-state-of-the-art, to perform a numerical simulation of the flow of fluids in the area of shell side under the inlet nozzle. Current methods of numerical analyses very well solve this problem, but at the expense of computing time, devices and expensive licences. The benefit of this work is the use of user-defined function (UDF) as a method for simulating interaction with fluid and structure in ANSYS Fluent software. This work places great emphasis on using the current state of knowledge for verifying and validation. Verifying and validation of results include, for example, experimentally measured Reynolds and Strouhal numbers, the drag coefficients and for example magnitude of pressure coefficient around the tube. At the same time, it uses the finite element method as a tool for the stress-strain calculation of a key part on tube such as a pipe-tube joint. Another benefit of this work is the extension of the graphical design of heat exchanger according to Poddar and Polley by vibration damages control according to the method described in TEMA [1]. In this section, the author points out the enormous influence of flow velocity on both the tube side and the shell side for design of the heat exchanger to ensure faultless operation. As an etalon of damage, the author chose a heat exchanger designated 104 from the Heat Exchanger Tube Vibration Data Bank [3]. With this heat exchanger, vibrational damage has been proven to be due to cutting of the tubes over the baffles. The last part outlines the possibilities and limits of further work.