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THE LIMITS & EFFECTS OF DRAW ON PROPERTIES AND MORPHOLOGY OF PAN-BASED PRECURSOR AND THE RESULTANT CARBON FIBERSEdrington, Sarah 01 January 2017 (has links)
The process, structure, and property relationship of PAN fiber as a precursor to carbon fiber was studied. The limitations of stable spinning and property improvement associated with hot draw in solution spinning were found and quantified. Conditions were varied to generated precursor fiber up to the limit of draw, from which actual samples were collected for thermal conversion to carbon fiber. Samples of PAN and subsequent carbon fiber were characterized using tensile testing and x-ray analysis. The effects of draw on modulus and break stress, as well as the orientation of the crystalline structure of both parent precursor and resultant carbon fiber were found and related back to the quantified draw limit.
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