Master's thesis deals with new methods of preparing catalytic materials for positive electrode of an oxygen-hydrogen fuel cell and the influence of potassium permanganate or doping agent molar mass change on theirs attributes. Further it studies the use of proper measuring methods designed to qualify theirs attributes and the presentation of achieved results. In particular methods of linear sweep and cyclic voltammetry and the processing of data using Koutecky-Levich and Tafel plot and wave log analysis. Values of half-wave and onset potential and kinetic coefficient have been measured and calculated.