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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Estudo de sistemas v?treos para infiltra??o em alumina / Study of glass system to alumina infiltration

Queiroz, Jos? Renato Cavalcanti de 14 September 2007 (has links)
Made available in DSpace on 2014-12-17T14:06:48Z (GMT). No. of bitstreams: 1 JoseRCQ.pdf: 1649143 bytes, checksum: 51cca0511bbe445cfdc5a7308f841ccf (MD5) Previous issue date: 2007-09-14 / The system in-Ceram Alumina, produced by VITA, consists in a technique of prepare of a substructure of ceramics to dental crowns. First burning is made in the alumina decanted by slip casting process under a stone die that reproduces the tooth prepared to receive a crown. In a second burning, alumina is infiltrated by vitreous system, giving to this set a high mechanic resistance. In this work, it s made a study of the composition of a new infiltrating material more used nowadays, giving to alumina desirable mechanics proprieties to its using like substructure of support to ceramic s crown used in the market today. The addition of Lanthanum oxide (frit A) and calcium oxide (frit B) was made in attempt to increase the viscosity of LZSA and to reduce fusion temperature. The frits were put over samples of alumina and took to the tubular oven to 1400?C under vacuum for two groups (groups 1 and 2). For another two groups (groups 3 and 4) it was made a second infiltration, following the same parameters of the first. A fifth group was utilized like group of control where the samples of pure alumina were not submitted to any infiltrating process. Glasses manifested efficient both in quality and results of analysis of mechanic resistance, being perfectly compatible with oral environment in this technical requisite. The groups that made a second infiltration had he best results of fracture toughness, qualify the use in the oral cavity in this technical question. The average of results achieved for mechanic resistance to groups 1, 2, 3, 4 and 5 were respectively 98 MPa, 90 MPa, 144 MPa, 236 MPa and 23 MPa / O sistema In-Ceram Alumina, fabricado pela VITA, consiste numa t?cnica de confec??o de uma infra-estrutura cer?mica para coroas dentais. Uma primeira queima ? realizada na alumina depositada pelo processo de slip casting sob um troquel de gesso que reproduz o dente preparado para receber a coroa. Numa segunda queima, a alumina ? infiltrada por um sistema v?treo, conferindo a este conjunto uma elevada resist?ncia mec?nica. Neste trabalho procurou-se estudar a composi??o de um novo material infiltrante baseado no sistema Li2O ZrO2 SiO2 Al2O3 (LZSA) com adi??o de La2O3 ou CaO, a fim de substituir o material importado mais usado atualmente (In-Ceram glass da Vita Zahnfabrik), proporcionando a alumina as propriedades mec?nicas desej?veis para seu emprego como infra-estrutura de suporte ?s coroas puras de cer?mica utilizadas na odontologia, diminuindo custos frente a esse sistema oferecidos hoje no mercado. O acr?scimo de ?xido de lant?nio (frita A) e ?xido de c?lcio (frita B) foi realizado na tentativa de aumentar a viscosidade do LZSA e diminuir a sua temperatura de fus?o. As fritas foram depositadas sobre amostras de alumina e levadas ao forno tubular a 1400?C sob v?cuo em dois grupos (1 e 2). Para outros dois grupos (3 e 4) foi realizada uma segunda infiltra??o, seguindo os mesmo par?metros da primeira. Um 5? grupo foi utilizado como grupo controle onde as amostras de alumina pura n?o foram submetidas a qualquer processo infiltrat?rio. Os vidros se mostraram eficazes tanto na qualidade da infiltra??o como nos resultados das an?lises de resist?ncia mec?nica. Os grupos que foram submetidos ? dupla infiltra??o obtiveram melhores resultados de resist?ncia mec?nica, sendo perfeitamente compat?veis com o meio oral nesse quesito t?cnico. A m?dia dos resultados obtidos para resist?ncia mec?nica para os grupos 1, 2, 3, 4 e 5 foram respectivamente 98 MPa, 90 MPA, 144 MPA, 236 MPa e 23 MPa

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