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Gas Chromatography Micro-Chip with High Temperature Interface and Silk Screen HeatersVilorio, Carlos R. 11 August 2020 (has links)
There has been substantial market demand for a portable Gas Chromatography (GC) system. Throughout the years, much progress has been made on fabricating a micro system that works as well as a benchtop system. Unfortunately, even though many substrates, channel types, channel widths, temperature control systems, and interface solutions have been attempted, existing versions of the micro-GC still fall short of the ideal. This thesis presents the design, fabrication, and testing of a silicon based micro-GC column that presents a solution for interfacing and heating of the chip. A polyimide resin is used to create a durable high temperature low thermal mass interface with the chip, while a silk screen method is demonstrated for easy printing of heaters. Chromatogram results are shown in both Temperature Program and Thermal Gradient runs.
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