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Influence of Ultra-high Temperature Process Parameters on Age Gelation of Mille ConcentrateElhilaly, Mohamed A. 01 May 1994 (has links)
The purpose of this research was to investigate the effect of ultra-high temperature process parameters on age gelation of milk concentrate. Skim milk was concentrated to 2X (volume reduction) using reverse osmosis. The milk concentrate was preheated at 75 or 90°C for 20 or 50 s and UHT-processed at 138 or 145°C for 4 or 16 s. Sterilizing methods used were direct steam injection and indirect plate heat exchanger. The samples were aseptically collected in presterilized plastic containers and stored at 15 or 35°C. At 15°C storage temperature, the steam-injected samples gelled in 5 months when 4 s UHT time was used. When UHT time was increased to 16 s, the samples gelled in 6 months.
Of the samples that were UHT processed by indirect plate heat exchanger for 4 s and stored at 15°C, all gelled after 7 months. When UHT time was increased to 16 s, all the 138°C samples gelled after 7 months as did the samples that were preheated for 50 s and UHT-processed at 138°C. The samples preheated at 75°C for 50 sand UHT-processed at 145°C gelled after 8 months, whereas at 90°C preheat temperature the samples gelled after 9 months.
The samples stored at 35°C did not gel but showed different sedimentation levels. The sediment depth in the container was always greater for the steam-injected samples. The samples that received higher heat treatments by the two processing methods had a higher sedimentation depth.
The pH decreased during storage and the extent of reduction was higher at 35°C storage temperature . Maillard browning occurred at both storage temperatures. Browning was greater in samples stored at 35°C and processed by indirect plate heat exchanger.
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Manufacture, Shelf Stability, and Acceptability of Aseptically Packaged, Unripened Soft Cheese Produced by Post-Ultra-High Temperature Acidulant Injection of Ultrafiltered Milk ConcentrateMoiseeva, Elena S. 01 May 1996 (has links)
This study investigated the manufacturing procedures and texture attributes of direct acid set of an unripened, shelf-stable cheese variety produced by the combined technologies of ultrafiltration and ultra-high temperature processing. Product evaluation included physical and chemical properties such as gel strength, syneresis, pH, moisture, protein, and fat. Whole milk was concentrated by ultrafiltration to 30, 35, and 40% total solids. Milk retentate was ultra-high temperature-processed by preheating to 65 or 77°C, sterilized at 141°C for 4 s by direct steam injection, flash cooled to approximately 62 or 72°C, homogenized in two stages at either 13.8/2.1 or 27.6/4.1 MPa, cooled to 38°C, and aseptically packaged. iv sterilized sodium chloride was aseptically added and dissolved in the ultra-filtrated and ultra-high temperature processed retentate to produce .5% final concentration. Autoclaved solutions of citric and lactic acids, or glucono-delta-lactone were added aseptically to the salted retentate to form a soft gel by lowering the pH range from 4.3 to 4.6. The coagulated retentates were stored at room temperature for 6 months. The effects of total solids, homogenization pressures, preheat temperatures, acidulants, and storage time on selected physicochemical properties of the acid gels were determined.
Taste panels evaluated selected soft cheese characteristics after 6 months' storage. No statistically significant effect of the total milk solids level on gel firmness was observed. High homogenization pressure and the interaction of high preheat temperature and homogenization pressure produced significantly firmer gel and caused less syneresis. Acidulant types influenced significantly gel strength, syneresis, appearance, and texture. Soft cheeses prepared with citric acid were firmer than those acidified with lactic acid or gluconodelta-lactone. Lactic acid samples produced more syneresis than citric acid cheese samples. Cheese samples prepared with glucono-delta-lactone had the smoothest and least grainy texture, shiny appearance, little or no wheying-off, and a gel strength intermediate between the two other acidulants.
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