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Neutron radiography is well suited to non-invasive imaging of water within metal containers. The goal of this work is to determine if neutron radiography can be used to image water freezing within a 1.6mm diameter capillary tube with the ultimate goal of observing this phenomena within fuel cells. In this work, radiography was completed at the Thermal Neutron Imaging Facility in the Nuclear Engineering Teaching Lab at The University of Texas at Austin. The source of neutrons was a TRIGA Mark II nuclear research reactor capable of 1.1 MW steady state power, which creates a neutron flux at the neutron imaging plane in beam port 5 of 5×10^6 neutrons/cm^2s. A scintillation screen and CCD camera are utilized to obtain digital radiographs, in which differences in pixel intensity are related to differences in neutron attenuation. An image processing algorithm was developed in Matlab to extract necessary data from each image, analyze water column images, and compare one to another. Also, a neutron flux model was implemented in Matlab in order to understand how a non-unidirectional neutron flux will affect final results. Raw image intensities of the water column in liquid and solid form were found to differ from expectations by at most 12.0% and 13.3%, respectively from the predictions of the Matlab flux model. A difference in pixel intensity comparing liquid water to solid water data is apparent and quantified. A ratio of pixel intensity for the ice image to the water image at full thickness of the water column is expected to be 1.038. Experimental results find a maximum ratio of 1.027, 1.1% off from expectations. / text

by Chan Yiu Nam. / Chinese title: / Includes bibliographical references / Thesis (M.Phil.) -- Chinese University of Hong Kong, 1983

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<p> Neutron radiography has the ability to differentiate between gas and liquid in twophase flow due both to the density difference and the high neutron scattering probability of hydrogen. Previous studies have used dynamic neutron radiography - in both real-time and high-speed - for air-water, steam-water and gas-liquid metal two-phase flow measurements. Radiography with thermal neutrons is straightforward and efficient as thermal neutrons are easier to detect with relatively higher efficiency and can be easily extracted from nuclear reactor beam ports.</p> <p> The quality of images obtained using neutron radiography and the imaging speed depend on the neutron beam intensity at the imaging plane. A high quality neutron beam, with thermal neutron intensity greater than 3.0xl06 n/cm2-s and a collimation ratio greater than 100 at the imaging plane, is required for effective dynamic neutron radiography up to 2000 frames per second.</p> <p> The primary objectives of this work are: (1) tu optimize a neutron radiography facility for dynamic neutron radiography applications and (2) to investigate a new technique for three-dimensional neutron radiography using information obtained from neutron scattering. </p> <p> In this work, neutron transport analysis and experimental validation of a dynamic neutron radiography facility is studied with consideration of real-time and high-speed neutron radiography requirements. A beam port based dynamic neutron radiography facility, for a target thermal neutron flux of l.Oxl07 n/cm2-s, has been analyzed, constructed and experimentally verified at the McMaster Nuclear Reactor.</p> <p> The neutron source strength at the beam tube entrance is evaluated experimentally by measuring the thermal and fast neutron fluxes using copper activation flux-mapping technique. The development of different facility components, such as beam tube liner, gamma ray filter, beam shutter and biological shield, is achieved analytically using neutron attenuation and divergence theories. Monte-Carlo simulations (using MCNP-4B code) are conducted to confirm the neutron parameters along the beam path and at the imaging plane. Good agreement between the analytical and the numerical values for the thermal neutron flux at the imaging plane to within 5% has been achieved. The MCNP simulations show that neutron back scattering, due to the presence of the back-wall biological shielding and the beam catcher, have an insignificant effect on the thermal neutron flux at the imaging plane, however, the epithermal and fast neutron fluxes have increased by 4-11 %.</p> <p> Experimental results show that the thermal neutron flux is nearly uniform over an imaging area of 20.0-cm diameter. The thermal neutron fl11x ranges from 1.0x 107 - 1.26x10 7 n/ cm2 -s at a reactor operating power of 3. 0 MW. The measured value for the neutron-to-gamma ratio is 6.0x 105 n/cm2-μSv and the Cadmium-ratio is observed to be 1.22. These values promote real-time neutron radiography with relatively high neutron attenuating materials such as light water and high-speed neutron radiography with relatively low neutron attenuating materials such as heavy water and Freon type fluids with a minimal contrast degradation resulting from non-thermal neutron content of the beam.</p> <p> A dynamic neutron radiography system has been developed and modified to obtain less neutron damage to the low-light level video camera. The system is used to visualize air-water two-phase flow in a natural-circulation loop to examine the dynamic capabilities of the radiography facility. Measurements of bubble velocity, void fraction, and phase distribution are successfully made. Single frames (-33 ms) of neutron images were captured using the dynamic neutron radiography system for air-water two-phase flow. The system was able to resolve single bubbles interfaces with an image spatial resolution of approximately 0.44 mm.</p> <p> Thermal neutron detectors are placed at the periphery of the neutron beam to detect neutrons scattered by a non-flowing two-phase object placed on a turntable to simulate motion of the gas phase. The results show the potential ability to use neutron scattering technique to provide two-dimension neutron radiography with additional information to the third dimension.</p> / Thesis / Doctor of Philosophy (PhD)

Neutron radiography is a non-destructive analysis tool that complements X-ray transmission radiography. The use of neutrons provides the ability to image the interior of an object that has a metal core of steel or lead that would shield the interior from X-ray inspection. Neutron tomography is the use of a set of images of a single sample taken at various angles to produce a three dimensional rendition of the sample that greatly increases the effectiveness of neutron radiography as a non-destructive testing tool. A neutron radiography and tomography system has been built at the 1.1 MW TRIGA Mark II nuclear research reactor at The University of Texas at Austin in the Nuclear Engineering Teaching Lab. The Texas Neutron Imaging Facility is located on beam port five of the reactor and is housed in a shielding cave made of concrete to minimize radiation dose to users. The system itself integrates a sample positioning system and neutron sensitive camera through the use of a control code written in National Instruments Labview software. The code was written to increase the efficiency of the imaging process and to provide flexibility in the system. Precise sample positioning and timing of image acquisition provided by the code allows for the collection of data that can be used in computed tomography. The system has produced results in the form of radiographs and 3-D reconstructions of sample objects. / text

Thesis (Ph. D.)--University of Texas at Austin, 2004. / Supervisor: Steven Biegalski. Vita. Includes bibliographical references. Also available from UMI.

Thesis (Ph. D.)--University of Texas at Austin, 1998. / Vita. Includes bibliographical references (leaves 209-211). Available also in a digital version from Dissertation Abstracts.

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