Non-intrusive acoustic thermometry using an acoustic impulse generator and two microphones is developed and integrated with tomographic techniques to reconstruct temperature contours. A low velocity plume at around 450 °F exiting through a rectangular duct (3.25 by 10 inches) was used for validation and reconstruction. 0.3 % static temperature relative error compared with thermocouple-measured data was achieved using a cross-correlation algorithm to calculate speed of sound. Tomographic reconstruction algorithms, the simplified multiplicative algebraic reconstruction technique (SMART) and least squares method (LSQR), are investigated for visualizing temperature contours of the heated plume. A rectangular arrangement of transmitter and microphones with a traversing mechanism collected two orthogonal sets of acoustic projection data. Both reconstruction techniques have successfully recreated the overall characteristic of the contour; however, for the future work, the integration of the refraction effect and implementation of additional angled projections are required to improve local temperature estimation accuracy. The root-mean-square percentage errors of reconstructing non-uniform, asymmetric temperature contours using the SMART and LSQR method are calculated as 20% and 19%, respectively. / Master of Science / Computational tomography is an approach to reconstruct the cross-sectional planar image of a 3D object. This technique is widely used in the medical field using x-rays to visualize cross-sections of internal organs. Along with x-rays, acoustic rays can also be utilized with tomographic techniques. The speed of sound travelling through a gaseous medium, such as air, is depended on the density, humidity, and temperature of the medium. Using this relationship, the temperature of the medium can be calculated with known speed of sound, density, and humidity. The speed of sound can be found using the distance and time of flight of the acoustic ray using transmitter and microphones. Since the effect of density and humidity of the medium on speed of sound is relatively insignificant, those values were assumed to be constant. In this research, the acoustic temperature measuring technique using the speed of sound relationship was applied and validated, then the technique was integrated with tomography using two projection angles. A rectangular duct (3.25 by 10 inches) with a heated air at around 450 °F exiting the duct was tested. The calculated temperature from acoustics was compared with values measured with thermocouples. After the acoustic temperature measuring technique was validated, multiple acoustic rays arranged in two orthogonal projections were setup. The speed of sound values from the acoustic rays were utilized to reconstruct the temperature distribution of the duct exit using two tomographic reconstruction methods: LSQR and SMART. Both reconstruction techniques have captured overall contour of the temperature. More projection angles and sound refractive properties will be utilized in the future to overcome the limitations of detailed reconstruction.