International Telemetering Conference Proceedings / October 20-23, 2003 / Riviera Hotel and Convention Center, Las Vegas, Nevada / Quartz crystal is an important electronic element in the field of communication systems, computer systems, etc. It is important to precisely measure the frequency of quartz crystal unit for manufacturing. The Pi-network transmission system recommended by International Electrotechnical Commission (IEC) is generally acknowledged as a measurement technique. However it needs a precise frequency source. The frequency source must be calibrated within a regular period in the process of manufacturing. Frequency counters, time internal counters, phase comparisons, which are the most common frequency calibrations, are introduced in the paper. Nowadays GPS has also become the primary system for frequency calibration. GPS receivers provide 1 PPS (Pulse Per Second) with accuracy < 100 nanoseconds to UTC under normal conditions. Motorola UT Oncore timing GPS with time accuracy < 50ns (1 sigma) uses time RAIM algorithm to ensure the validity and reliability of measurements. The comparison between the precise 1PPS and local reference is implemented. And the phase differences are logged and read by computer. According to the values, the frequency output of DDS is coordinated. In order to reduce the phase ambiguity, local reference is divided before comparison. The calibration can be implemented at any time by GPS. Block diagrams of calibration are presented in this paper.

Nuclear quadropole spectroscopy is a modern analytical method for detecting specific solid state materials, e.g. explosives, drugs etc. It uses phenomenon of atomic nucleus called nuclear quadrupole moment. NQR method is very similar to common nuclear magnetic resonance (NMR) that is why major principles are explained using NMR. The thesis deals with basic principle of NQR, its usage for explosives detection and also detection of other chemical compounds and many other useful applications. The thesis deals with specific circuit design, techniques for sufficient sensitivity, impedance matching and circuit isolation. Practical part consists of simulations as well as designs of a few impedance transformers, pi-networks, and coils. Also experimental probe was created. In the last part, NQR workplace was assembled and a few chemical compounds were detected. These were KClO3, NaClO3 and NaNO2 . Finally minimum detectable amount of potassium chlorate as the strongest signal of these was determined.