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<p>Microfluidic devices using electroosmotic flows (EOFs) in microchannels have been developed and widely applied in chemistry, biology and medicine. Advantages of using these devices include the reduction of reagent consumption and duration for analysis. Moreover the velocity profile of EOFs, in contrast to the parabolic profile found in pressure-driven flows, has a plug-like profile which contributes significantly less to solute dispersion. It also requires no valve to control the flow, which is done with the appropriate application of electrical potentials, thus becomes one of the favourite techniques for sample separation. However, high potentials of several hundred volts are usually required to generate sufficient EOF. These high potentials are not practical for general usage and could cause electrical hazard in some applications. One of the possible solutions is the introduction of zeta potential modulation. The EOF in a microchannel can be controlled by the zeta potential at the liquid/solid interface upon the application of external gate potentials across the channel walls. Combined with AC EOF, it can rectify the oscillating flows and generate pressure that can be used for microfluidic pumping applications. Since the flow induced by the alternating electric field is unsteady and periodic, it is critical to visualize the flow with high spatial and temporal resolutions in order to understand fluid dynamics. A novel method to obtain high temporal resolution for high frequency periodic electrokinetic flows using phase sampling technique in micro particle image velocimetry (PIV) measurements are first developed in order to characterize the AC electroosmotic flow. After that, the principle of zeta potential modulation is demonstrated to transport particles, cells, and other micro organisms using rectified AC EOF in open microchannels. The rectified flow is obtained by synchronous zeta-potential modulation with the driving potential in the microchannel. Subsequently, we found that PDMS might not be the best material for some pumping and biomedical applications as its hydrophobic surface property makes the priming process more difficult in small microchannels and also causes significant protein adsorption from biological samples. A more hydrophilic and biocompatible material, polyurethane (PU), was chosen to replace PDMS. A polyurethane-based soft-lithography microfabrication including its bonding, interconnect integration and in-situ surface modification was developed providing better biocompatibility and pumping performance. Finally, an electroosmotic pumping device driven by zeta potential modulation and fabricated by PU soft lithography was presented. The problem of channel priming is solved by the capillary force induced by the hydrophilic surface. Its flow rate and pressure output were found to be controllable through several parameters such as driving potential, gate potential, applied frequency, and phase lag between the driving and gate potentials.</p> / Doctor of Philosophy (PhD)

Yes / This paper provides results of a comprehensive investigation into the use of waste carpet fibres for reinforcement of clay soil slopes. The interaction between laboratory scale model slopes made of fibre reinforced clay soil and surface strip footing load was examined. Results for the influence of two variables namely fibre content and distance between the footing edge and the crest of the slope are presented and discussed. Particle Image Velocimetry (PIV) technique was employed to study the deformation of the slope under the surface loading. The front side of the tank was made of a thick Perspex glass to facilitate taking accurate images during the loading stage. To study the stress induced in the slope under footing pressure, excess pore-water pressure and total stress increase were measured at predetermined locations within the slope. The results showed that fibre reinforcement increased the bearing resistance of the model slope significantly. For instance, inclusion of 5% waste carpet fibre increased the bearing pressure by 145% at 10% settlement ratio. / The post-print of this article will be released for public view when the version of record has been published by ASCE.

The mechanism by which convective heat transfer is augmented by freestream turbulence in the stagnation region was studied experimentally. Previous work has suggested that the primary mechanism for the observed augmentation is the amplification of vorticity into strong vortices which dominate the flow field near the surface. Therefore, two separate experimental investigations were performed to further study this phenomenon. In the first, the spatiotemporal convection from a heated surface was measured during the normal collision of a vortex ring. The convection was observed to increase dramatically in areas where vortices forced outer fluid through the natural convection boundary layer to the surface. Regions where fluid was swept along the surface experienced much smaller increases in convection. These observations led to the development of a mechanistic model which predicted the heat transfer based on the amount of time that fluid remained within the thermal boundary layer prior to reaching the surface. In subsequent testing, the model was able to accurately predict the time-resolved convection based solely on the transient properties of the vortex present. In the second investigation, the model was applied to the vortices which form in a stagnating turbulent flow. Three turbulence conditions were tested which changed the properties of the vortices produced. Again, the model was successful in predicting the time-resolved convection over much of the experimental measurement time. The work of designing and calibrating the heat flux sensor used is also reported. A new sensor was developed specifically for the convection research performed herein as no existing sensor possessed the required spatiotemporal resolution and underwater capabilities. Utilizing spot-welded foils of thermoelectric alloys resulted in a very robust and sensitive sensing array which was thoroughly analyzed and calibrated. In the final section, the hybrid heat flux (HHF) method is presented which significantly increases the performance of existing heat flux sensors. It is shown (both numerically and experimentally) that by combining the spatial and temporal temperature measurements from a standard sensor, the time response increases by up to a factor of 28. Also, this method causes the sensor to be insensitive to the material to which it is mounted. / Ph. D.

The mechanism of heat transfer augmentation due to freestream turbulence in classic Hiemenz stagnation flow was studied experimentally for the first time using time-resolved digital particle image velocimetry (TRDPIV) and a new thin film heat flux sensor called the Heat Flux Array (HFA). Unique measurements of simultaneous, time-resolved velocity and surface heat flux data were obtained along the stagnation line on a simple, rectangular flat plate model mounted in a water tunnel facility. Identification and tracking of coherent structures in the stagnation region lends support to the theory that coherent structures experience stretching and amplification of vorticity by the mean flow strain rate upon approaching the stagnation surface. The resulting flow field in the near-wall region is comprised primarily of high strength, counter-rotating vortex pairs with decreased integral length scale relative to the imposed freestream turbulence. It is hypothesized that the primary mechanism of heat transfer augmentation is the movement of cooler freestream fluid into the heated near-wall region by these coherent structures. Furthermore, the level of heat transfer augmentation is dictated by the integral length scale, circulation strength, and core-to-surface distance of the coherent structures. To test this hypothesis, these properties were incorporated into a mechanistic model for predicting the transient, turbulent heat transfer coefficient. The model was successful in predicting the shape and magnitude of the measured heat transfer coefficient over much of the experimental measurement time. In a separate yet related set of studies, heat flux sensors and calibration methods were examined. The High Temperature Heat Flux Sensor (HTHFS) was designed and developed to become one of the most durable heat flux sensors ever devised for long duration use in high temperature, extreme environments. Extensive calibrations in both conduction and convection were performed to validate the performance of the sensor near room temperature. The measured sensitivities in conduction and convection were both very close to the predicted sensitivity using a thermal resistance model of the HTHFS. The sensor performance was unaffected by repeated thermal cycling using kiln and torch firing. Finally, the performance of Schmidt-Boelter heat flux sensors were examined in both shear and stagnation flow using two custom designed convection calibration facilities. Calibration results were evaluated using an analytical sensitivity model based on an overall sensor thermal resistance from the sensor to the heat sink or mounting surface. In the case of convection the model included a term for surface temperature differences along the boundary layer. In stagnation flow the apparent sensitivity of the Schmidt-Boelter sensors decreased non-linearly with increasing heat transfer coefficient. Estimations of the sensor's internal thermal resistance were obtained by fitting the model to the stagnation calibration data. This resistance was then used with the model to evaluate the effects of non-uniform surface temperature on the shear flow sensitivity. A more pronounced non-linear sensitivity dependence on heat transfer coefficient was observed. In both cases the main result is that convection sensitivity varies a great deal from standard radiation calibrations. / Ph. D.

The issue of the effects of free stream turbulence on the flow field over a surface-mounted prism is examined through experimental and numerical investigations. In the experimental studies, particle image velocimetry measurements are conducted in the ESM water tunnel at Reynolds number of $9,600$ and under two cases of turbulent inflow conditions. The results show that the mean flow separation, reattachment and parameters such as mean velocity, root mean square, Reynolds stresses and turbulent kinetic energy are affected by the turbulence characteristics of the incident flow. The instantaneous dynamics of the interactions between the separating shear layer and the solid wall and between the shear layer and the turbulence in the incident flow are detailed. In the numerical studies, large eddy simulations of the flow over a surface-mounted prism under two inflow conditions, namely, smooth inflow and isotropic homogeneous turbulence inflow, are performed. The use of a fifth-order scheme (CUD-II-5), which is a member of a family of Compact Upwind Difference schemes, in large eddy simulations of this flow is assessed. The performance of this scheme is validated by comparing the rate of temporal decay of isotropic turbulence with available experimental measurements for grid-generated turbulence. The results show that the spectra are sensitive to the method of flux vector splitting needed for the implementation of the upwind scheme. With van Leer splitting, the CUD-II-5 scheme is found to be too dissipative. On the other hand, using the Lax-Friedrichs vector splitting yields good agreement with experiments by controlling the level of artificial dissipation. This led us to recommend a new procedure, we denote by C6CUD5 scheme, that combines a compact sixth-order scheme with the CUD-II-5 scheme for large eddy simulation of complex flows. The simulation results, including flow patterns, pressure fields and turbulence statistics show that the CUD-II-5 scheme, with Lax-Friedricks flux vector splitting, provides high resolution of local flow structures. The results present new physical aspects of the flow topology over surface-mounted prisms. The effects of the incident homogeneous turbulence on the size of the separation region and suction pressures are determined by pointing out differences in the flow topologies between the two incident flow cases. / Ph. D.