Thesis (M.S.)--Ohio University, March, 1994. / Title from PDF t.p.

published_or_final_version / Industrial Engineering / Master / Master of Philosophy

In this research, the effects of gas composition, elapsed time of reaction and temperature on scale formation and descaling of low carbon steel were investigated and results were discussed from the viewpoint of the phase composition of the scales, oxidation rates, oxidation mechanisms, adhesion, fracture mechanics, porosity and residual scale. / The phase composition and morphology of scales grown under conditions similar to those of reheating furnaces were analyzed. Low carbon steel was oxidized over the temperature range 1000-1250°C in gas mixtures of O 2-CO2-H2O-N2, O2-H 2O-N2 and O2-CO2-N2. The mole fraction of each phase, wustite (FeO), magnetite (Fe3O 4) and hematite (Fe2O3) was determined by the direct comparison method Two types of scales were observed. The first type was a crystalline scale with an irregular outer surface composed mostly of wustite, and a negligible amount of magnetite. The second type was the classical three-layer scale composed of wustite, magnetite and hematite. In general, the experiments showed that the furnace atmosphere, oxidation time and temperature influence the phase composition of the scales. / Low carbon steel was oxidized in air over the temperature range 600-1200°C for 120 s to approximate the formation of secondary and tertiary scale in hot rolling. The mole fraction of wustite, magnetite and hematite was determined by the direct comparison method The phase composition of the scales changed with temperature and time. During the initial 30 s of oxidation, wustite was the predominant phase in the temperature range 800-1200°C, and as oxidation proceeded, the percentages of magnetite and hematite increased. In addition, the texture of the scales was investigated by orientation imaging microscopy (OIM); it was found that temperature influences the texture of the scales. The experiments indicated that 850°C is the ideal temperature for the finishing mill in order to reduce surface defects and work roll wear. / The adhesion of scales formed in air on low carbon steel in continuous heating and isothermal conditions was investigated with a four-point bending test. The separation (crack) always occurred inside the scale indicating that the strength of the scale is lower than the strength of the scale/steel interface. It was found that scale adhesion is related to scale porosity, blister formation and stresses acting in the scale. A spallation process was observed when cooling from 800°C to room temperature. The microscopic observations revealed that spallation followed route 1 "strong interface and weak oxide." / Low carbon steel was oxidized over the temperature range 1050-1250°C in O2-CO2H2O-N2 gas mixtures in order to study the hydraulic descaling process. The oxidation times were 15-120 min. and the scales were 130-2000 mum thick. The experimental parameters were chosen to approximate scale formation under conditions similar to those of reheating furnaces. In the hydraulic descaling tests, two modes of scale removal were observed. In the first mode, observed in classical three-layer scales that developed an inner porous layer with low or medium porosity, the horizontal undercutting occurred at the boundary of the inner porous layer and dense scale. The second mode was observed in classical three-layer scales that developed an inner porous layer with high porosity and in crystalline scales. In the second mode, the horizontal undercutting occurred at the first plane of large pores relative to the scale/steel interface. In general, the experiments showed that scale morphology controlled the removability of scale.

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Thesis (Ph. D.)--Florida State University, 2005. / Advisor: Dr. Hamid Garmestani, Florida State University, College of Engineering, Dept. of Mechanical Engineering. Title and description from dissertation home page (viewed Sept. 29, 2005). Document formatted into pages; contains xiii, 101 pages. Includes bibliographical references.

Thesis (Ph. D.)--Ohio State University, 1986. / Includes vita. Includes bibliographical references (leaves 170-179). Available online via OhioLINK's ETD Center.

The objective of this investigation was to determine the influence of work roll cooling on roll thermal behavior. The investigation has been conducted utilizing a previously developed computer model [1]. Three industrial operations were evaluated and features of an optimum configuration have been identified. The magnitude of the thermal zone near the roll surface within which the cyclic temperature variation is confined has been evaluated for different roll cooling conditions. A two dimensional thermal model of a work roll has been developed to predict the thermal field inside the roll, based on which the thermal crown of the roll was calculated under an assumption of axi-symmetric deformation. The heat transfer equation was solved by the numerical finite difference method, the Alternating Direction Implicit (ADI) method. This method makes it possible to solve the problem on a personal computer making it suitable for industrial application due to the minimum requirements of computer storage and time. Also because the thermal model simulates operating conditions including the cooling configuration it is of value in studying a variety of industrial rolling conditions. The influence of roll spray arrangement, roll gap heat transfer and mill pacing on roll thermal crown has been investigated. / Applied Science, Faculty of / Materials Engineering, Department of / Graduate

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Thesis (Ph. D.)--Ohio University, November, 2002. / Title from PDF t.p. Includes bibliographical references (leaves 164-171).