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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
191

Scaling Effects on Damage Development, Strength, and Stress-Rupture Life on Laminated Composites in Tension

Lavoie, J. André 04 April 1997 (has links)
The damage development and strength of ply-level scaled carbon/epoxy composite laminates having stacking sequence of [+Tn/-Tn/902n]s where constraint ply angle, T, was 0, 15, 30, 45, 60, and 75 degrees, and size was scaled as n=1,2,3, and 4, is reported in Part I. X-radiography was used to monitor damage developments. First-ply failure stress, and tensile strength were recorded. First-ply failure of the midplane 90 deg. plies depended on the stiffness of constraint plies, and size. All 24 cases were predicted using Zhang's shear-lag model and data generated from cross-ply tests. Laminate strength was controlled by the initiation of a triangular-shaped local delamination of the surface angle plies. This delamination was predicted using O'Brien's strain energy release rate model for delamination of surface angle plies. For each ply angle, the smallest laminate was used to predict delamination (and strength) of the other sizes. The in-situ tensile strength of the 0 deg. plies within different cross-ply, and quasi-isotropic laminates of varying size and stacking sequence is reported in Part II. No size effect was observed in the strength of 0 deg. plies for those lay-ups having failure confined to the gauge section. Laminates exhibiting a size-strength relationship, had grip region failures for the larger sizes. A statistically significant set of 3-point bend tests of unidirectional beams were used to provide parameters for a Weibull model, to re-examine relationship between ultimate strength of 0 deg. plies and specimen volume. The maximum stress in the 0 deg. plies in bending, and the tensile strength of the 0 deg. plies (from valid tests only) was the same. Weibull theory predicted loss of strength which was not observed in the experiments. An effort to model the durability and life of quasi-isotropic E-glass/913 epoxy composite laminates under steady load and in an acidic environment is reported in Part III. Stress-rupture tests of unidirectional coupons immersed in a weak hydrochloric acid solution was conducted to determine their stress-life response. Creep tests were conducted on unidirectional coupons parallel and transverse to the fibers, and on ±45°. layups to characterize the lamina stress- and time-dependent compliances. These data were used in a composite stress-rupture life model, based on the critical element modeling philosophy of Reifsnider, to predict the life of two ply-level thickness-scaled quasi-isotropic laminates. / Ph. D.
192

Fatigue crack propagation in AA 7050-T7451 alloy considering environment, stress ratio, rolling direction and waveform effects / Propagação de trinca por fadiga na liga AA7050-T7451 considerando o efeito do meio ambiente, razão de tensões, direção de laminação e forma de onda

Cárdenas Barbosa, José Fernando 17 March 2017 (has links)
Main extrinsic and intrinsic modifiers factors of crack growth rate in AA7050-T7451 were assessed in order to provide tools for aeronautical structures designers. These tools cover most necessary information to project aircraft\'s structures using the studied alloy, under damage tolerance philosophy. The experimental methodology consisted of use CT specimens, on TL and LT rolling direction to test its behavior under different conditions of stress ratio, force waveform, and the environment. The stress ratio values were 0.1 and 0.5, the force waveform used were sine and trapezoidal or Dwell under normal air laboratory conditions and salt fog 3.5%NaCl weight in order to simulate the marine environment. In Dwell tests, results were checked with the electrical potential drop technique (DCPD) in addition to the crack opening displacement (COD) method. Using the Walker coefficients, calculated on the present research, could be projected accurately the crack propagation behavior on Paris region and do fatigue life predictions using da/dN and S-N diagrams for different stress ratio values. The corrosion environment increases both crack growth rate and ΔKth due to oxides formation on the crack path that generates a crack closure effect. Dwell carrying makes decrease the crack growth rate by decreasing the slope of the Paris line on log (da/dN) versus log (ΔK) curve, instead of shifting down the line as occurs on titanium alloys. Rolling direction change from LT to TL increase the FCG rate in both threshold and Paris region, where the rate change use to be small. / Os principais fatores modificadores extrínsecos e intrínsecos da taxa de propagação de trincas na liga AA7050-T7451 foram avaliados para fornecer subsídios para projetistas de estruturas aeronáuticas, com base na filosofía de tolerância ao dano. A metodologia experimental consistiu em ensaiar corpos de prova do tipo compact tension (CT) da liga nas direções de laminação TL e LT, para verificar seu comportamento sob diferentes razões de tensões, forma de onda e condição ambiente. Os valores de razão de tensão estudados foram 0,1 e 0,5, as formas de onda foram senoidal e trapezoidal ou de Dwell, em condições normais de laboratório, ao ar, e névoa salina 3,5% NaCl, em massa, para simular um ambiente marinho. No caso dos ensaios Dwell, os resultados foram conferidos pelo método de queda de potencial eléctrico (QPE), além do método de flexibilidade elástica. Usando os coeficientes de Walker calculados a partir dos resultados obtidos, pôde-se projetar com precisão o comportamento da propagação de trinca na região de Paris e prever a vida em fadiga usando os diagramas da/dN e S-N para diferentes valores da razão de tensões. O ambiente corrosivo aumenta tanto a taxa de propagação de trinca, quanto o valor de ΔKth por causa da formação de óxidos na trajetória da trinca, que geram um efeito de fechamento sobre a mesma. Quanto à forma de onda, verificou-se que o carregamento Dwell diminui a taxa de propagação de trinca, diminuindo a inclinação das curvas log (da/dN) versus log (ΔK) na região de Paris, ao invés de deslocá-la paralelamente como ocorre com ligas de titânio. A mudança da direção de laminação de LT para TL aumenta a taxa de propagação de trinca por fadiga (PTF) tanto na região de threshold, quanto na região de Paris, onde a mudança de taxa é pequena.
193

Design and performance of cold bent glass

Datsiou, Kyriaki Corinna January 2017 (has links)
The demand for flat glass is high and increasing significantly in the building industry as a direct result of architectural requirements for lightness, transparency and natural light. Current architectural trends require glass in curvilinear forms for smooth free-form façades. Two principal challenges arise from this: to cost-effectively produce the desired curvature and; to ensure its safe performance after exposure to ageing. The recent availability of high strength glass provides an opportunity to address the first challenge by developing cold bent glass. Cold bending involves the straining of relatively thin glass components, at ambient temperatures, and is a low energy and cost effective manner of creating curvilinear forms. However, cold bending is not yet widely established as a reliable method. The aim of this thesis is to develop the understanding of cold bent glass during the bending process and to evaluate its post-ageing performance. This thesis, firstly, investigates the mechanical response of monolithic glass plates during the cold bending process. The stability of cold bent glass is investigated experimentally by bending it in double curved anticlastic shapes. A parametric numerical analysis involves different boundary conditions, geometrical plate characteristics and bending parameters. The principal outcome is that a local instability, now termed cold bending distortion, occurs when certain displacement limits are exceeded and could degrade the optical quality of the glass. An evaluation procedure is also formulated to set limits and aid designers/manufacturers to predict the mechanical response and the optical quality of the glass. Cold bent glass is subjected to permanent bending stresses throughout its service life and therefore, its strength degradation after ageing needs to be quantified. Analytical, experimental and numerical investigations are undertaken in this thesis to identify the most effective method for estimating glass strength (evaluation of destructive tests, required number of specimens, statistical analysis methods and sub-critical crack growth). The limited availability of naturally aged toughened glass and the absence of a reliable ageing standard impede the evaluation of its aged performance. Therefore, a parametric experimental investigation of artificial ageing methods on glass is undertaken in this thesis. A procedure for the evaluation of the strength of aged glass is finally, formulated to allow the selection of artificial ageing parameters that correspond to a target level of erosion. The knowledge on artificial ageing and strength prediction acquired above is finally implemented on different types of glass to determine their strength after ageing and assess their safe use in cold bending / load bearing applications. The investigation showed that fully toughened glass has a superior performance to chemically toughened or annealed glass. Overall, the research presented in this thesis demonstrates that high quality cold bent toughened glass can be created when certain applied displacement limits are respected. These can be used as a safe, cost-effective and energy efficient replacement to the more conventional hot bent glass. However, cold bending / load bearing applications in which the stressed glass surface is exposed to ageing, require glass with a relatively high case depth such as fully toughened or bi-tempered glass.
194

Fatigue crack propagation in AA 7050-T7451 alloy considering environment, stress ratio, rolling direction and waveform effects / Propagação de trinca por fadiga na liga AA7050-T7451 considerando o efeito do meio ambiente, razão de tensões, direção de laminação e forma de onda

José Fernando Cárdenas Barbosa 17 March 2017 (has links)
Main extrinsic and intrinsic modifiers factors of crack growth rate in AA7050-T7451 were assessed in order to provide tools for aeronautical structures designers. These tools cover most necessary information to project aircraft\'s structures using the studied alloy, under damage tolerance philosophy. The experimental methodology consisted of use CT specimens, on TL and LT rolling direction to test its behavior under different conditions of stress ratio, force waveform, and the environment. The stress ratio values were 0.1 and 0.5, the force waveform used were sine and trapezoidal or Dwell under normal air laboratory conditions and salt fog 3.5%NaCl weight in order to simulate the marine environment. In Dwell tests, results were checked with the electrical potential drop technique (DCPD) in addition to the crack opening displacement (COD) method. Using the Walker coefficients, calculated on the present research, could be projected accurately the crack propagation behavior on Paris region and do fatigue life predictions using da/dN and S-N diagrams for different stress ratio values. The corrosion environment increases both crack growth rate and ΔKth due to oxides formation on the crack path that generates a crack closure effect. Dwell carrying makes decrease the crack growth rate by decreasing the slope of the Paris line on log (da/dN) versus log (ΔK) curve, instead of shifting down the line as occurs on titanium alloys. Rolling direction change from LT to TL increase the FCG rate in both threshold and Paris region, where the rate change use to be small. / Os principais fatores modificadores extrínsecos e intrínsecos da taxa de propagação de trincas na liga AA7050-T7451 foram avaliados para fornecer subsídios para projetistas de estruturas aeronáuticas, com base na filosofía de tolerância ao dano. A metodologia experimental consistiu em ensaiar corpos de prova do tipo compact tension (CT) da liga nas direções de laminação TL e LT, para verificar seu comportamento sob diferentes razões de tensões, forma de onda e condição ambiente. Os valores de razão de tensão estudados foram 0,1 e 0,5, as formas de onda foram senoidal e trapezoidal ou de Dwell, em condições normais de laboratório, ao ar, e névoa salina 3,5% NaCl, em massa, para simular um ambiente marinho. No caso dos ensaios Dwell, os resultados foram conferidos pelo método de queda de potencial eléctrico (QPE), além do método de flexibilidade elástica. Usando os coeficientes de Walker calculados a partir dos resultados obtidos, pôde-se projetar com precisão o comportamento da propagação de trinca na região de Paris e prever a vida em fadiga usando os diagramas da/dN e S-N para diferentes valores da razão de tensões. O ambiente corrosivo aumenta tanto a taxa de propagação de trinca, quanto o valor de ΔKth por causa da formação de óxidos na trajetória da trinca, que geram um efeito de fechamento sobre a mesma. Quanto à forma de onda, verificou-se que o carregamento Dwell diminui a taxa de propagação de trinca, diminuindo a inclinação das curvas log (da/dN) versus log (ΔK) na região de Paris, ao invés de deslocá-la paralelamente como ocorre com ligas de titânio. A mudança da direção de laminação de LT para TL aumenta a taxa de propagação de trinca por fadiga (PTF) tanto na região de threshold, quanto na região de Paris, onde a mudança de taxa é pequena.
195

Application of experimental and analytical approaches in characterizing coronary stents

Saqib, Muhammad 29 June 2023 (has links)
Coronary artery disease (CAD) affects every fifth person in the world. The gold-standard treatment for CAD is stent implantation, however, the existing therapy is not sufficient due to many reasons. For instance, in-stent restenosis, biocompatibility, controlled degradation rate, protein adsorption, and adequate endothelialization are still the main concerns. In the last two decades, the field of stent technology has been grown rapidly and many new stent types and in vitro testing methods for stent characterization have been developed to minimize the aforementioned issues. In this vicinity, there are still many unaddressed issues: i) the quantitative analysis of corrosion is conducted with simpler samples made of stent material instead of stents, in most cases due to the absence of a mathematical model to calculate the entire stent surface area (ESSA); ii) in vitro stent testing in environments that are very far from actual physiological environments; iii) Evaluation of the influence of in-vitro test conditions on coated metallic stents; iv) absence of flow-induced shear stress (FISS) corrosion model, to mention a few. This thesis presents the novel ESSA model, the fluid dynamic experimental setup with the integration of various sensors and pH control, the influence of in vitro degradation behavior of the titanium oxynitride (TiOxNy) coated stainless steel stents and anodized AZ31 samples, and the FISS corrosion model. The results show some important contributions in this field, however, there is still a huge potential for the development of promising stent characterization solutions. / Die koronare Herzkrankheit (KHK) betrifft jeden fünften Menschen auf der Welt. Der Goldstandard bei der Behandlung von KHK ist die Stent-Implantation, doch die bestehende Therapie ist aus vielen Gründen nicht ausreichend. So sind beispielsweise die Restenose im Stent, die Biokompatibilität, die kontrollierte Abbaugeschwindigkeit, die Proteinadsorption und die angemessene Endothelialisierung nach wie vor die Hauptprobleme. In den letzten zwei Jahrzehnten hat sich die Stenttechnologie rasant weiterentwickelt, und es wurden viele neue Stenttypen und In-vitro-Testmethoden zur Stentcharakterisierung entwickelt, um die oben genannten Probleme zu minimieren. In dieser Umgebung gibt es noch viele ungelöste Probleme: i) die quantitative Analyse der Korrosion wird mit einfacheren Proben aus Stentmaterial anstelle von Stents durchgeführt, in den meisten Fällen aufgrund des Fehlens eines mathematischen Modells zur Berechnung der gesamten Stentoberfläche (ESSA); ii) In-vitro-Stent-Tests in Umgebungen, die sehr weit von der tatsächlichen physiologischen Umgebung entfernt sind; iii) Bewertung des Einflusses von In-vitro-Testbedingungen auf beschichtete metallische Stents; iv) Fehlen eines FISS-Korrosionsmodells (flow-induced shear stress), um nur einige zu nennen. In dieser Arbeit werden das neuartige ESSA-Modell, der strömungsdynamische Versuchsaufbau mit der Integration verschiedener Sensoren und pH-Kontrolle, der Einfluss des In-vitro-Degradationsverhaltens der mit Titanoxynitrid (TiOxNy) beschichteten Edelstahlstents und anodisierten AZ31-Proben sowie das FISS-Korrosionsmodell vorgestellt. Die Ergebnisse zeigen einige wichtige Beiträge in diesem Bereich, jedoch gibt es noch ein großes Potenzial für die Entwicklung von vielversprechenden Lösungen zur Charakterisierung von Stents.
196

Performance characterisation of duplex stainless steel in nuclear waste storage environment

Ornek, Cem January 2016 (has links)
The majority of UK’s intermediate level radioactive waste is currently stored in 316L and 304L austenitic stainless steel containers in interim storage facilities for permanent disposal until a geological disposal facility has become available. The structural integrity of stainless steel canisters is required to persevere against environmental degradation for up to 500 years to assure a safe storage and disposal scheme. Hitherto existing severe localised corrosion observances on real waste storage containers after 10 years of exposure to an ambient atmosphere in an in-land warehouse in Culham at Oxfordshire, however, questioned the likelihood occurrence of stress corrosion cracking that may harm the canister’s functionality during long-term storage. The more corrosion resistant duplex stainless steel grade 2205, therefore, has been started to be manufactured as a replacement for the austenitic grades. Over decades, the threshold stress corrosion cracking temperature of austenitic stainless steels has been believed to be 50-60°C, but lab- and field-based research has shown that 304L and 316L may suffer from atmospheric stress corrosion cracking at ambient temperatures. Such an issue has not been reported to occur for the 2205 duplex steel, and its atmospheric stress corrosion cracking behaviour at low temperatures (40-50°C) has been sparsely studied which requires detailed investigations in this respect. Low temperature atmospheric stress corrosion cracking investigations on 2205 duplex stainless steel formed the framework of this PhD thesis with respect to the waste storage context. Long-term surface magnesium chloride deposition exposures at 50°C and 30% relative humidity for up to 15 months exhibited the occurrence of stress corrosion cracks, showing stress corrosion susceptibility of 2205 duplex stainless steel at 50°C.The amount of cold work increased the cracking susceptibility, with bending deformation being the most critical type of deformation mode among tensile and rolling type of cold work. The orientation of the microstructure deformation direction, i.e. whether the deformation occurred in transverse or rolling direction, played vital role in corrosion and cracking behaviour, as such that bending in transverse direction showed almost 3-times larger corrosion and stress corrosion cracking propensity. Welding simulation treatments by ageing processes at 750°C and 475°C exhibited substantial influences on the corrosion properties. It was shown that sensitisation ageing at 750°C can render the material enhanced susceptible to stress corrosion cracking at even low chloride deposition densities of ≤145 µm/cm². However, it could be shown that short-term heat treatments at 475°C can decrease corrosion and stress corrosion cracking susceptibility which may be used to improve the materials performance. Mechanistic understanding of stress corrosion cracking phenomena in light of a comprehensive microstructure characterisation was the main focus of this thesis.
197

An Analysis of Microstructure and Corrosion Resistance in Underwater Friction Stir Welded 304L Stainless Steel

Clark, Tad Dee 30 June 2005 (has links) (PDF)
An effective procedure and parameter window was developed for underwater friction stir welding (UWFSW) 304L stainless steel with a PCBN tool. UWFSW produced statistically significant: increases in yield strengths, decreases in percent elongation. The ultimate tensile strength was found to be significantly higher at certain parameters. Although sigma was identified in the UWFSWs, a significant reduction of sigma was found in UWFSWs compared to ambient FSWs. The degree of sensitization in UWFSWs was evaluated using double loop EPR testing and oxalic acid electro-etched metallography. Results were compared to base metal, ambient FSW, and arc welds. Upper and lower sensitization localization bands were identified in the UWFSWs. Although higher sensitization levels were present in UWFSWs compared to the arc weld, ambient FSW, and heat treated base metals, the UWFSWs were found less susceptible to corrosion than arc welds due to the subsurface location of the sensitization bands. A SCC analysis of UWFSWs relative to base metal and arc weldments was performed. U-bends were exposed to two 3.5% NaCl cyclic immersion experiments at 21 °C and 63 °C for 1000 hours each. A tertiary test was conducted in a 25% NaCl boiling solution. The UWFSW u-bends were no more susceptible to SCC than base metal in the cyclic immersion tests. In the boiling NaCl test, the SCC of the UWFSWs showed significant improvement over the SCC of arc welds. Arc u-bends cracked entirely within the weld bead and HAZ, while SCC in the UWFSWs showed no cracking localization.

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