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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Triboqu?mica: intera??o de insertos met?licos roscados metal-osso maxilar / Tribochemical: threaded metal inserts interaction metal-bone

Pontes, Gracilene dos Santos Aquino 26 February 2016 (has links)
Submitted by Automa??o e Estat?stica (sst@bczm.ufrn.br) on 2017-02-02T12:02:52Z No. of bitstreams: 1 GracileneDosSantosAquinoPontes_DISSERT.pdf: 15314465 bytes, checksum: 08443c4598fd6bb9ee7c3a2fcde8a8d9 (MD5) / Approved for entry into archive by Arlan Eloi Leite Silva (eloihistoriador@yahoo.com.br) on 2017-02-07T15:40:36Z (GMT) No. of bitstreams: 1 GracileneDosSantosAquinoPontes_DISSERT.pdf: 15314465 bytes, checksum: 08443c4598fd6bb9ee7c3a2fcde8a8d9 (MD5) / Made available in DSpace on 2017-02-07T15:40:37Z (GMT). No. of bitstreams: 1 GracileneDosSantosAquinoPontes_DISSERT.pdf: 15314465 bytes, checksum: 08443c4598fd6bb9ee7c3a2fcde8a8d9 (MD5) Previous issue date: 2016-02-26 / Implantes dent?rios s?o suportes ou estruturas de materiais biocompat?veis posicionados cirurgicamente no osso maxilar, abaixo da gengiva, para substituir ra?zes dent?rias, assegurando estruturalmente dentes artificiais ap?s a perda da denti??o. Desenvolveu-se um m?todo de ensaio, em laborat?rio, para analisar a resposta mec?nica de um parafuso met?lico implantado em um osso maxilar inanimado de um porco de cerca de doze meses de idade e imerso em um fluido com tr?s condi??es de pH: ?cido, b?sico e neutro. Uma solicita??o mec?nica de contato circunferencial c?clico para simular um processo mastigat?rio unidirecional foi utilizada para investigar a estabilidade dimensional da uni?o parafuso-osso em fun??o do n?mero de ciclos sob carga. Ap?s os ensaios com a presen?a de solu??o ?cida, b?sica ou neutra, analisou-se a estrutura porosa do osso maxilar su?no bem como da cabe?a do parafuso submetida ao contato metal-metal atrav?s de MEV e microan?lise por EDS. Os resultados das solicita??es triboqu?micas da uni?o parafuso-osso evidenciaram, na cabe?a do parafuso, a ocorr?ncia de desgaste abrasivo com forma??o de proa com presen?a de debris e, no osso, dano por fratura fr?gil com a presen?a de microtrincas em meio ? sua porosidade intr?nseca. As taxas de desgaste por perda m?ssica do parafuso desatarraxado ap?s cada ensaio demonstraram surpreendentemente serem menores quando resultantes dos ensaios com solu??o ?cida e b?sica, enquanto foram maiores as taxas de desgaste dos parafusos ensaiados em meio a uma solu??o neutra. O contato aqueceu em uma faixa que variou entre 0,50C at? 16,50C acima da temperatura ambiente. Assim, atribuiu-se ? a??o ?cida do fluido aquecido pelo atrito entre os contatos sobre o parafuso met?lico a forma??o de uma nanocamada passivada, respons?vel pelo menor desgaste medido. A velocidade de vibra??o global foi maior durante o running in, at? 104 ciclos, do que no regime permanente de ensaios, entre 104 e 105 ciclos, quando o contato j? se configurara como conforme. O NPS[dB], n?vel de press?o sonora seguiu esta tend?ncia. O pH do fluido continuou ?cido antes e ap?s os ensaios, embora haja migrado de 2, no in?cio, para 4, no final. Os demais permaneceram invari?veis. / Dental implants are material supports and structures biocompatible surgically positioned into the maxillary bone beneath the gums to replace tooth roots, ensuring structurally teeth substitutes after the loss of teeth. We have developed an approach in the laboratory to analyze the mechanical response of a metallic screw implanted in an inanimate jaw bone of a pig about twelve months of age and immersed in a fluid at three pH conditions: acidic, basic and neutral. A mechanical stress cyclic circumferential contact to simulate a unidirectional masticatory process was used to investigate the dimensional stability of the screw-bone junction in the number of cycles under load. After the tests on the presence of acidic, basic or neutral solution, it analyzed the porous structure of the pig maxillary bone and screw head subjected to metal-to-metal contact through MEV and EDS microanalysis. The results of tribochemical requests the screw-bone junction showed in the screw head, the occurrence of abrasive wear with bow training with the presence of debris and bone, damage by brittle fracture in the presence of microcracks in the midst of their inherent porosity. The wear rates of mass loss of undoing screw after each test showed surprisingly are lower when resulting from tests with acidic and basic solution, as were higher wear rates of the tested screws in the middle of a neutral solution. The contact heated in a band ranging from 0,5oC to 16,5oC above room temperature. Therefore, attributed to the acid action of the fluid heated by the friction between the contacts on the metal bolt the formation of a passivated nanolayer responsible for the lowest measured wear. The overall vibration velocity was higher during the running in, up to 104 cycles, than in steady-state tests, between 104 and 105 cycles, when the contact already configures as conformal. SPL [dB] Sound Pressure Level followed this trend. The pH of the acid fluid continued before and after the test, although there is migrated from 2 at the beginning, 4 at the end. The rest remained unchanged.
2

Desgaste corrosivo-cavitativo-erosivo de um a?o-carbono em meio aquoso com fra??es de sal (NaCl), CO2 e particulados s?lidos (SiO2) / Corrosive-cavitative-crosive wear of a carbon steel in aqueous medium with salt (NaCl), CO2 and solid particulates (SiO2) fractions

Silva, Fernando Nunes da 27 August 2012 (has links)
Made available in DSpace on 2014-12-17T14:58:19Z (GMT). No. of bitstreams: 1 FernandoNS_DISSERT.pdf: 5044327 bytes, checksum: 66e88407297dda873c6a6d882b6de312 (MD5) Previous issue date: 2012-08-27 / Conselho Nacional de Desenvolvimento Cient?fico e Tecnol?gico / A batch of eighty-four coupons of low carbon steel were investigated at laboratory conditions under a corrosive, cavitative-corrosive (CO2) and corrosive-erosive (SiO2 + CO2) in an aqueous salt solution and two levels of temperature. The following measurements were made on Vickers (HV0,05, HV0,10, HV0,20) Microhardness tests at three levels of subsurface layer. A turbulent flow collided on the cylindrical sample, with and without mechanical stirring and gas bubbling, with and without fluid contamination by solid particles of SiO2, at two temperatures. Surface Roughness and Waviness, under two conditions "as received, after machining" and "after worn out", as well as gravimetric and electrochemical parameter were measured on the two opposite generatrices of each cylindrical sample, on the flow upstream (0?) and downstream (180?) by Profilometry, Mass Variation and Linear Polarization Resistance (LPR). The results of the Microhardness and Surface Texture of all coupons were subjected to statistical comparison, using the software Statgraphics? Centurion XVI, 95% statistical certainty, and significant differences were observed in some arrays of measurements. The corrosive wear rate measured by LPR and mass variation shown to be sensitive to the presence of bubbles and hydrodynamic fluctuations inside the cell, considering the temperature and contamination of corrosive fluid by solid particles. The main results of visual inspection relative to some topologies of the surface damages involving different mechanisms that were seen to give explanation for some fluctuations in wear rates of the steel experimentally investigated / Um lote de oitenta e quatro corpos-de-prova (CP) de a?o AISI 1018 foi investigado em laborat?rio sob solicita??es corrosivas, cavitativo-corrosivas (CO2) e erosivocorrosivas (SiO2+CO2) em meio aquoso salino e a duas temperaturas. Foram realizados ensaios de microdureza Vickers a tr?s n?veis de subsuperf?cie (HV0,05, HV0,10, HV0,20). Um fluxo agitado colidiu contra os CPs, em todas as condi??es de ensaio, sem e com agita??o mec?nica e borbulhamento de g?s, sem e com contamina??o do fluido por part?culas s?lidas de SiO2, nas duas temperaturas estudadas. A rugosidade e ondula??o superficial, nas condi??es como recebidos, ap?s usinagem e ap?s desgastados , bem como medi??es gravim?tricas e eletroqu?micas foram realizadas em duas geratrizes opostas de cada corpo-deprova, a montante (0?) e a jusante (180?), atrav?s das t?cnicas de perfilometria, varia??o m?ssica e resist?ncia de polariza??o linear (RPL). Os resultados da microdureza e da textura superficial em todos CPs foram submetidos ? compara??o estat?stica, utilizando-se o software Statgraphics? Centurion XVI e, com 95% de certeza estat?stica, diferen?as significativas foram observadas em alguns grupos de medidas. As medidas das taxas de desgaste corrosivo, por RPL e por varia??o m?ssica, demonstraram serem sens?veis ? presen?a de bolhas e ?s flutua??es hidrodin?micas no interior da c?lula, consideradas a temperatura e a contamina??o do fluido corrosivo por part?culas s?lidas. Apresentam-se, tamb?m, os principais resultados da inspe??o visual em que se evidenciam algumas topologias do dano superficial nas geratrizes a 0? e a 180?, involvendo diferentes mecanismos que foram presenciados, para justificar algumas flutua??es nas taxas de desgaste do a?o em estudo

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